Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/

or distribution, of this document and its contents are strictly prohibited unless expressly authorized in

writing by Lurgi. Offenders are liable for damages. All rights, including but not limited to all proprietary
Rev. 0a
rights in relation to patents, utility models and/or other industrial property rights, are reserved.
Lurgi Process DS Cover Sheet.xls

00
Revision

Case-Name:
All
Sheet

Normal Case
Name

Project Name
PuWa
Date
Prepared, Revised
04/10/2015
DiS
Name
Checked
CS
Name

Project No.
Cover
Process

Date
Approved
04/10/2015
06-T-0110
Process Data Sheet

Index of Revisions
Methanol Water Column

IFI
Status

Document No.
Issued for Information

Printed by / date / time:

1 / 8
Sheet / of

/
Remark, kind of revision

/
00
Q.L. Revision
CONFIDENTIAL
 Process

Process Data Sheet

Column-Reactor Sections

01 Item Number Unit Number 06

06-T-0110
writing by Lurgi. Offenders are liable for damages. All rights, including but not limited to all proprietary
or distribution, of this document and its contents are strictly prohibited unless expressly authorized in

Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/

02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.

03 Designation Methanol Water Column

04
05 Number required 1
06 Orientation vertical
07 Total volume ft
08 Total height ft 111
09
10 Cyclic loading No
11 Column Sections
12 Section number
13 Section description Section I
14 Medium Methanol Water
15 Volume ft
16 Height ft 111
17 Inner diameter in 76.00
18 Density lb/ft
19 Op. temp. max. / min. F 291.72 / 214.66 / / /
20 Op. pres. max. / min. psi [a] 59.32 / 53.51 / / /
21 Des temp. max./min./vac. F 345 / 3 / / / / / / /
22 Des pres. max./min./vac. psi[g] 75 / / FV / / / / / /
23 Corrosive components
24 Sour gas service (acc. Lurgi Std. Spec.) no
25 H 2 -partial pressure psi [a] @ F @ F @ F @ F
26 Material CS
27 Corrosion allowance in 0.2
28 Lining
29 Cladding
30 Heat treatment No
31 Process Internals
32 49 / Sieve Tray / / /
33 SS
34
35 / / / /
36
37
38 / / / /
Internals number / type
39
Material
40
41 / / / /
42
43
44 / / / /
45
46
47 Insulation Yes Heat, external
48 Remarks: row 17) To be finally decided by tray manufacturer / contractor
3
row 18) Only applicable if density > 1000 kg/m (62.43 lb/ft3)
Rows 06) and 18) to be finally decided by tray manufacturer / Vendor

General Notes:
Lurgi Process DS Column-Reactor Sections.xls

1) For Tray design use information provided in "General Notes for column ".
2) Refer General Notes for equipments .

Line revised under Rev. No.

Project Name Project No. Document No. Sheet / of Revision

Rev. 0a

2 / 8 00
Case-Name: Normal Case Printed by / date / time: / /
 Process

Process Data Sheet

Nozzle

01 Item Number Unit Number 06

06-T-0110
writing by Lurgi. Offenders are liable for damages. All rights, including but not limited to all proprietary
or distribution, of this document and its contents are strictly prohibited unless expressly authorized in

Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/

02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.

03 Description Methanol Water Column

04
05 Table of Nozzles
06 Item No req NPS Rating Facing Designation
07 in
08 N1 1 2 Impure Water Outlet to 06-P-0109A/B
09 N2 1 10 Impure Water Outlet to Reboiler 06-E-0120
10 N3 1 10 Nozzle for Spare reboiler
11 N4 1 18 Impure Water Inlet from Reboiler 06-E-0120
12 N5 1 18 Nozzle for Spare reboiler
13 N6 1 6 Live Steam Injection
14 N7 1 1) Min flow line from Pump 06-P-0109
15 N8 1 2 LP N2 Utility
16 N9 1 2 Demin Water Inlet from 06-E-0121A/B, Spare
17 N10 1 2 Demin Water Inlet from 06-E-0121A/B
18 N11 1 2 Methanol Water Inlet from 06-P-0107A/B
19 N12 1 4 Pure Methanol Inlet from 06-P-0110A/B
20 N13 1 14 Methanol Vapour Outlet to 06-T-0109
21 V1 1 2 Vent
22 D1 1 2 Drain
23 P1 1 2 Pressure Transmitter
24 T1-7 7 2 Temperature Nozzle
25 L1A/B 2 2 Level Gauge
26 L2A/B 2 2 Level Transmitter
27
28
29 M1-5 5 24 Manhole
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54 Remarks: Rating and Facing according pipe-class
1) Nozzle sizes for Pump minimum circulation lines to be finalised durig Detail Engineering.
2) Inlet Nozzle size to be checked by Internals Vendor
Lurgi Process DS Nozzle.xls

Line revised under Rev. No.

Project Name Project No. Document No. Sheet / of Revision

Rev. 0a

3 / 8 00
Case-Name: Normal Case Printed by / date / time: / /
 Process

Process Data Sheet

Sketch

01 Item Number Unit Number 06

06-T-0110
writing by Lurgi. Offenders are liable for damages. All rights, including but not limited to all proprietary
or distribution, of this document and its contents are strictly prohibited unless expressly authorized in

Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/

02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.

03 Description Methanol Water Column

04
05 N 13
06 V1

07 T.L.
48"

08
ID 7 6"
M5
09 N 12 1
14x16"= 224"

10 N o te:
11 1 ) D is ta n c e m u s t b e c h e c k e d d u rin g
d e ta il e n g in e e rin g a c c o rd in g to d e s ig n o f
12 R e b o ile r 0 6- E- 0 1 2 0
420"

13 15
14 2 ) M a te ria l fo r fla n g e d p ip e (2 ") a n d b lin d fla n g e (3 ")
M4
36"

is S S 3 0 4L
15
16 3 ) In le t d e v ic e to b e d e s ig n e d b y in te rn a ls
7x16"= 112"

16 T7 ve n d o r / c o n tra c to r
17
18
19 23 T6
20
36"

21
68"

N1 1
2x16"= 32"

22 24
23 T5 p lu g - in n o z zle s
24 26
36"

25 N1 0
26 M3
2)
27 27
2x16"= 32"
T.L.-T.L. 111'

28 T4
29 29
30
32"

31 N9
32 30 T3
6x16"= 96"

2)
33
34
35 36
T2
36"

36
M2
12x16"= 192"
844"

37 37
38
39
40 49
P1
41 N8
42 N7
1)

M1
70"

43 N6
44
N4 3) N5
45
46 L 1 B, L 2 B T1
47
340"

48
49 L 1 A, L 2 A
10"

50 V o rte x B re a k e r
T. L.
51
Min. required for

52
53 N2 N3
54
piping

N1
55 D1
56
Lurgi Process DS Sketch.xls

57

Line revised under Rev. No.

Project Name Project No. Document No. Sheet / of Revision

Rev. 0a

4 / 8 00
Case-Name: Normal Case Printed by / date / time: / /
 Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/

or distribution, of this document and its contents are strictly prohibited unless expressly authorized in

writing by Lurgi. Offenders are liable for damages. All rights, including but not limited to all proprietary
Rev. 0a
rights in relation to patents, utility models and/or other industrial property rights, are reserved.
Lurgi Process DS Sketch.xls

57
56
55
54
53
52
51
50
49
48
47
46
45
44
43
42
41
40
39
38
37
36
35
34
33
32
31
30
29
28
27
26
25
24
23
22
21
20
19
18
17
16
15
14
13
12
11
10
09
08
07
06
05
04
03
02

Case-Name:
420" 01 Item Number

To E- 0121

Normal Case
214" 68"

N5

N1

D1

Project Name
N3
NLL
HLL
06-T-0110

ID76"
T- 0110
Tray1

Project No.
Sketch
Process

N4

48" 90 "
Unit Name
Description

N2
Unit Number
Process Data Sheet

79" 116 "

Document No.
E- 0120
06

Printed by / date / time:

Rectisol

ID36"
Methanol Water Column

/
5 / 8
Sheet / of

/
96" 99"

Line revised under Rev. No.

00
Revision
 Process

Process Data Sheet

Tray

01 Item Number Unit Number 06

06-T-0110
writing by Lurgi. Offenders are liable for damages. All rights, including but not limited to all proprietary
or distribution, of this document and its contents are strictly prohibited unless expressly authorized in

Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/

02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.

03 Designation Methanol Water Column

04
05 Column section number
06 Column section designation Top Section Top Section Middle Section
07 Top Bottom Top
08 Tray No. from to 1 23 1 23 24 26
09 Operating data of decisive tray No. 1 23 24
10 Operating pressure psi [a] 53.52 56.16 56.42
11 Medium Methanol / Water Methanol / Water Methanol / Water
12 Operating temperature t op F 214.66 226.53 236.34
Vapour to tray

13 Normal load lb/h 52782.18 48061.48 43966.87

14 Required load min. max. % 70 130 70 130 70 130
15 Molecular weight lb/lbmol 31.99 29.92 28.12
16 Density @ t op lb/ft 0.25 0.24 0.22
17 Dynamic viscosity @ t op cP 0.01 0.01 0.01
18 Compressibility factor Z = pV / RT 0.949 0.949 0.95
19 Medium Methanol / Water Methanol / Water Methanol / Water
C 214.66 221.83 226.53
Liquid from tray

20 Operating temperature
21 Normal load lb/h 45306.22 48247.92 44601.13
22 Required load min. max. % 70 130 70 130 70 130
23 Density @ t op lb/ft 43.37 44.39 45.62
24 Dynamic viscosity @ t op
cP 0.25 0.25 0.24
25 Surface tension dyn/cm 15.69 21.63 27.16
26 Allowable pressure drop per tray psi 0.11 0.11 0.11
27 Allowable level in the downcomer in
28 Allowable hold-up time in the downcomer min
29 Allowable leakage rate per tray lb/h
30 Allowable flooding factor % 80 80 80
31 Foaming factor (system factor) 1.00 1.00 1.00
32 Column inside calculated in 76.00 50.00 50.00
33 diameter selected in
34 Type of tray Sieve Sieve Sieve
35 Tray spacing in 16.00 16.00 16.00
36 Number of passes 1 1 1
37 Tray SS SS SS
Material

38 Valve
39 Bubble or tunnel caps
40
41 Remarks: row 8, 9) Count from top
row 32, 35) To be stated by tray manufacturer
Internals to be installed into the column/vessel through manhole.
Maximum recommended downcomer inlet velocity: 0.39 ft/s
Maximum recommended downcomer clear liquid backup: 50%, I.e. 0.5 (TS + h_weir)
TS: Tray Spacing
h_weir: Outlet Weir Height

General Notes:
1) Potential fouling service use big sieve holes, preferably between 1" to 1.2" (i.e. 25mm - 30mm) diameter.
Lurgi Process DS Tray.xls

Line revised under Rev. No.

Project Name Project No. Document No. Sheet / of Revision

Rev. 0a

6 / 8 00
Case-Name: Normal Case Printed by / date / time: / /
 Process

Process Data Sheet

Tray

01 Item Number Unit Number 06

06-T-0110
writing by Lurgi. Offenders are liable for damages. All rights, including but not limited to all proprietary
or distribution, of this document and its contents are strictly prohibited unless expressly authorized in

Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/

02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.

03 Designation Methanol Water Column

04
05 Column section number
06 Column section designation Bottom Section Bottom Section
07 Top Bottom
08 Tray No. from to 27 49 27 49
09 Operating data of decisive tray No. 27 49
10 Operating pressure psi [a] 56.68 59.32
11 Medium Methanol / Water Methanol / Water
12 Operating temperature t op F 257.57 291.83
Vapour to tray

13 Normal load lb/h 36503.78 26269.89

14 Required load min. max. % 70 130 70 130
15 Molecular weight lb/lbmol 24.51 18.02
16 Density @ t op lb/ft 0.19 0.14
17 Dynamic viscosity @ t op cP 0.01 0.01
18 Compressibility factor Z = pV / RT 0.96 0.97
19 Medium Methanol / Water Methanol / Water
F 236.34 291.72
Liquid from tray

20 Operating temperature
21 Normal load lb/h 37138.04 26904.14
22 Required load min. max. % 70 130 70 130
23 Density @ t op lb/ft 48.37 54.79
24 Dynamic viscosity @ t op
cP 0.24 0.19
25 Surface tension dyn/cm 36.87 49.45
26 Allowable pressure drop per tray psi 0.11 0.11
27 Allowable level in the downcomer in
28 Allowable hold-up time in the downcomer min
29 Allowable leakage rate per tray lb/h
30 Allowable flooding factor % 80 80
31 Foaming factor (system factor) 1.00 1.00
32 Column inside calculated in 76.00 76.00
33 diameter selected in
34 Type of tray Sieve Sieve
35 Tray spacing in 16.00 16.00
36 Number of passes 1 1
37 Tray SS SS
Material

38 Valve
39 Bubble or tunnel caps
40
41 Remarks: row 8, 9) Count from
row 32, 35) To be stated by tray manufacturer
Internals to be installed into the column/vessel through manhole.
Maximum recommended downcomer inlet velocity: 0.39 ft/s
Maximum recommended downcomer clear liquid backup: 50%, I.e. 0.5 (TS + h_weir)
TS: Tray Spacing
h_weir: Outlet Weir Height

General Notes:
1) Potential fouling service use big sieve holes, preferably between 1" to 1.2" (i.e. 25mm - 30mm) diameter.
Lurgi Process DS Tray.xls

Line revised under Rev. No.

Project Name Project No. Document No. Sheet / of Revision

Rev. 0a

7 / 8 00
Case-Name: Normal Case Printed by / date / time: / /
 Process

Process Data Sheet

Nozzle Stream Table

01 Item Number Unit Number 06

02 06-T-0110 Unit Name Rectisol
writing by Lurgi. Offenders are liable for damages. All rights, including but not limited to all proprietary
or distribution, of this document and its contents are strictly prohibited unless expressly authorized in
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/

03 Designation Methanol Water Column

rights in relation to patents, utility models and/or other industrial property rights, are reserved.

04
05 Case Normal Case
06 Nozzle-ID N1 N2 N4 N10
07 Nozzle designation Impure Water Outlet to Impure Water Outlet to Impure Water Inlet from Demin Water Inlet from
08 06-P-0109A/B Reboiler 06-E-0120 Reboiler 06-E-0120 06-E-0121A/B
09 Stream no. 404
10 Internal stream no. 404 404A 404B 413
11 Stream designation Impure Water Impure H2O Impure H2O Impure Water
12 from 06-T-0110 to Reboiler 06-E-0120 from Reboiler 06-E-0120 from 06-T-0110
13 Phase Liquid Liquid Mixed Liquid
14 Total flow lbmol/h 35.21 16167.26 16167.26 24.86
15 Total flow lb/h 634.26 291334 291334 447.82
16 Liquid Vapour Liquid Vapour Liquid Vapour Liquid Vapour
17 Vol. flow ft/h 11.58 - 5317.28 - 4605.47 - 8.08 -
18 Norm. vol. flow 10^6 scf/day - - - 13.31 -
19 Mass flow lb/h 634.26 291334 264999 26335 447.82
20 Mole flow lbmol/h 35.21 35.21 14705.83 1461.43 24.86
21 Molweight lb/lbmol 18.02 18.02 18.02 18.02 18.02
22 Eff. density lb/ft 54.79 54.79 57.54 0.14 55.45
23 Spec. heat cap. Btu/(lb F) 1.02 1.02 1.03 0.56 1.02
24 Viscosity cP 0.19 0.00 0.19 0.01 0.20
25 Ther. conductivity (Btu/h)/(ft F) 0.40 0.40 0.40 0.02 0.40
26 Mole fraction fraction 1.00 1.00 0.91 0.09 1.00
27 Mass fraction fraction 1.00 1.00 0.91 0.09 1.00
28 Temperature F 291.72 291.72 293 277.47
29 Pressure psi [a] 59.32 59.32 59.32 81.77
30
31 Nozzle-ID N11 N12 N13
32 Nozzle designation Methanol Water Inlet from Pure Methanol Inlet from Methanol Vapour Outlet to
33 06-P-0107A/B 06-P-0110A/B 06-T-0109
34 Stream no. 403
35 Internal stream no. 402 358 403
36 Stream designation Methanol Water Pure Methanol Methanol Water Column
37 from 06-P-0107A/B to 06-T-0110 Ovhd to 06-T-0109
38 Phase Liquid Liquid Vapour
39 Total flow lbmol/h 242.62 1419.38 1651.64
40 Total flow lb/h 7662.39 45369.35 52845.30
41 Liquid Vapour Liquid Vapour Liquid Vapour Liquid Vapour
42 Vol. flow ft/h 176.22 - 1046.59 - - -
43 Norm. vol. flow 10^6 scf/day - - - 15.04 -
44 Mass flow lb/h 7662.39 45369.35 52845.30
45 Mole flow lbmol/h 242.62 1419.38 1651.64
46 Molweight lb/lbmol 31.58 31.96 32.00
47 Eff. density lb/ft 43.47 43.35 0.25
48 Spec. heat cap. Btu/(lb F) 0.799 0.79 0.39
49 Viscosity cP 250.00 0.25 0.01
50 Ther. conductivity (Btu/h)/(ft F) 0.104 0.10 0.01
51 Mole fraction fraction 1.00 1.00 1.00
52 Mass fraction fraction 1.00 1.00 1.00
53 Temperature F 217.45 215.14 214.66
Lurgi Process DS Nozzle Stream Table.xls

54 Pressure psi [a] 87.02 70.00 53.52

55 Remarks:

Line revised under Rev. No.

Project Name Project No. Document No. Sheet / of Revision

Rev. 0a

8 / 8 00
Case-Name: Normal Case Printed by / date / time: / /