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NaOH Titration Data and Analysis

This document presents the results of an experiment investigating the reaction between sodium hydroxide (NaOH) and ethyl acetate (Et(Ac)) in a continuous stirred tank reactor (CSTR) under various flow rates. The results show that increasing the flow rate of NaOH and Et(Ac) decreases the residence time and increases the conversion rate. Across six trials at different flow rates, the conversion rates ranged from 93.8% to 96.9% while the residence times decreased from 0.672 to 4.082 minutes as the flow rates increased. A graph of residence time versus conversion shows an inverse relationship between the two variables.

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85 views2 pages

NaOH Titration Data and Analysis

This document presents the results of an experiment investigating the reaction between sodium hydroxide (NaOH) and ethyl acetate (Et(Ac)) in a continuous stirred tank reactor (CSTR) under various flow rates. The results show that increasing the flow rate of NaOH and Et(Ac) decreases the residence time and increases the conversion rate. Across six trials at different flow rates, the conversion rates ranged from 93.8% to 96.9% while the residence times decreased from 0.672 to 4.082 minutes as the flow rates increased. A graph of residence time versus conversion shows an inverse relationship between the two variables.

Uploaded by

ahmad pidot
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd

RESULT

No. Flow Flow rate Total Residenc Inlet Outlet Conversion Reaction Rate of volume
rate of of Et(Ac) flow rate e time,τ conductivit conductivit , X (%) Rate Reaction, of NaOH
NaOH (mL/min) of (min) y (ms/cm) y (mS/cm) Constant,K -rA titrade
(mL/min solution, (L/mol.min (mol/L.min (mL)
) Vo ) )
(mL/min
)
1 300 295 595 0.672 9.3 6.3 93.8 225.04 0.00805 12.5
2 250 249 499 0.802 8.8 5.7 94.1 197.2 0.00597 13.1
3 200 199 399 1.003 8.8 5.6 94.4 168.2 0.00527 13.8
4 150 146 296 1.351 8.7 5.4 94.5 127.1 0.00384 14.0
5 100 96 196 2.041 8.2 4.7 95.7 107.7 0.00204 16.3
Volume
6 50 48 98 4.082 7.3 4.1 96.9 76.58 0.00074 18.8
of
0.25M
HCl =10ml
Volume of sample taken =50ml
Time taken to collect sample =6min
Volume of sample, Vs = 400 ml
Concentration of NaOH in the feed vessel, CNaOH,f = 0.1 mol/L
Volume of HCl for quenching, VHCl,s = 10 ml
Concentration of HCl in standart solution, CHCl,s = 0.25 mol/L
Concentration of NaOH used for titration, CNaOH,s = 0.1 mol/L
Reactor volume, VTFR = 0.4 L/400ml
Concentration of NaOH in feed tank, CAO = 0.1 M
Concentration of Et(Ac) in feed tank = 0.1 M
Graph residence time, T against conversion, X
4.5
4
3.5
3
residence time, T

2.5
2
1.5
1
0.5
0
0 1 2 3 4 5 6 7 8
Conversion, X

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