®

multi EA 5000
Service Manual

Version 1.1
Table of Contents

1 Generals .................................................................................................................................... 7
2 Device configuration .................................................................................................................. 7
3 Power supply ............................................................................................................................. 8
3.1 Temperature controller power supply ................................................................................ 8
3.2 Firmware controller TERN power supply ........................................................................... 8
4 Main board................................................................................................................................. 9
4.1 Main board power supply .................................................................................................. 9
4.2 Service points and service LEDs ..................................................................................... 10
5 Firmware controller unit ........................................................................................................... 13
5.1 I/O allocation .................................................................................................................... 15
5.2 Testing the firmware controller ........................................................................................ 17
5.3 Configuration of the Terminal program ............................................................................ 18
6 Software and firmware............................................................................................................. 34
6.1 Software installation (PC) ................................................................................................ 34
6.2 Software update(PC) ....................................................................................................... 37
6.3 Firmware update (TERN controller) ................................................................................. 37
6.3.1 FW-update with UpdateCenter of multiWin ................................................................. 38
6.3.2 FW-update with terminal program ............................................................................... 45
6.4 Replacement of the firmware controller TERN ................................................................ 50
7 Combustion module and temperature control ......................................................................... 51
7.1 Temperature control for the valve heating and transfer line ............................................ 52
7.2 Temperature control for the furnace heating ................................................................... 52
7.3 Temperature controller update ........................................................................................ 57
7.3.1 Update with program SIOW.exe .................................................................................. 57
7.3.2 Update with UpdateCenter of multiWin........................................................................ 62
7.4 Setting of the temperature controller ............................................................................... 63
7.5 Replacing the temperature controller............................................................................... 67
7.5.1 Checking the furnace ................................................................................................... 67
7.5.2 Replacing the thermocouple in the furnace ................................................................. 67
7.5.3 Furnace replacement ................................................................................................... 68
7.5.3.1 Removing of furnace ............................................................................................ 68
7.5.3.2 Mounting of furnace ............................................................................................. 69
8 Gas supply module .................................................................................................................. 71
8.1 Checking the "high performance" gas box....................................................................... 73
8.1.1 Setting the main oxygen (A1) flow rate in the "high performance" gas box ................. 74
8.2 Calibrating the internal MFM............................................................................................ 77
8.3 Gas box replacement ...................................................................................................... 81
8.4 Check of MFM ................................................................................................................. 82
8.5 Replacing the MFM ......................................................................................................... 83
9 Measuring gas drying unit ....................................................................................................... 84
9.1 Membrane dryer unit ....................................................................................................... 84
9.1.1 Tightness check of the membrane dryer ..................................................................... 85
9.1.2 Replacement of the membrane dryer .......................................................................... 86
9.2 Auto-protection valve assembly ....................................................................................... 87
9.2.1 Valve coupling with filter unit/ checking the filter ......................................................... 87
9.2.2 Filter replacement ........................................................................................................ 88
9.2.3 Replacing the pneumatic seal...................................................................................... 89
9.2.4 Removing the complete valve coupling ....................................................................... 91
9.2.5 Check of the AP valve assembly ................................................................................. 91
10 Sample dosing module ............................................................................................................ 92
10.1 Auto-injector .................................................................................................................... 94
10.2 MMS 5000 ....................................................................................................................... 96

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 10.2.1Exchange of the main board .................................................................................... 96
10.2.2Updating the firmware of the MMS sampler ............................................................ 96
10.2.3Replacing the main board of the MMS sampler ....................................................... 96
10.2.4Replacement of mechanical components ................................................................ 97
10.2.5Rack and syringe detection ..................................................................................... 97
10.2.6Check of the auto-sampler with service program .................................................... 97
10.2.7Testing the interface sampler in simulation mode (MMS5000) with the service
program ................................................................................................................... 99
10.3 ABD ............................................................................................................................... 100
10.3.1 Block schema of ABD with multi EA® 5000 ............................................................ 101
10.3.2 Test of the ABD with service program ................................................................... 101
10.3.3 Testing the interface sampler in simulation mode (ABD) with the service program.....
............................................................................................................................... 103
10.4 GSS module .................................................................................................................. 105
10.4.1 Structure of GSS module ....................................................................................... 105
10.4.2 Testing the communication of GSS module with evaluation unit (multiWin®) ....... 106
10.4.3 Testing the GSS module with the service program ............................................... 106
10.4.4 Testing the interface sampler in simulation mode (GSS module) with the service
program ................................................................................................................. 108
10.5 LPG module (LPG/GSS module) ................................................................................... 109
10.5.1 Testing the LPG module (LPG/GSS module) with components test of multiWin® . 111
10.5.2 Testing the LPG module (LPG/GSS module) with the service program ................ 112
10.5.3 Testing the interface sampler in simulation mode (LPG-/GSS module) with the
service program ..................................................................................................... 115
10.5.4 Final test of LPG module (LPG/GSS module) ....................................................... 116
11 Detectors ............................................................................................................................... 117
11.1 UVFD APSA370 ............................................................................................................ 117
11.1.1 Check of technical parameter and requirements APSA370 on its display ............. 117
11.1.2 Testing the communication of APSA370 with evaluation unit(multiWin®) ............. 118
11.1.3 Testing the APSA370 with the service program .................................................... 118
11.1.4 Testing the interface for APSA370 with the service program (simulation mode) ... 119
11.2 UVFD5000 ..................................................................................................................... 120
11.2.1 Check of technical parameter inside the components test (multiWin) ................... 120
11.2.2 Testing the UVFD5000 with the service program .................................................. 121
11.2.3 Testing the interface for UVFD5000 with the service program (simulation mode). 123
11.3 CLD APNA370 ............................................................................................................... 125
11.3.1 Check of technical parameter and requirements APNA370 on its display............. 125
11.3.2 Testing the communication of APNA370 with evaluation unit (multiWin®) ............. 126
11.3.3 Testing the APNA370 with the service program .................................................... 126
11.3.4 Testing the interface for APNA370 with the service program (simulation mode)... 128
11.4 CLD5000 ....................................................................................................................... 129
11.4.1 Check of technical parameter inside the components test (multiWin) ................... 129
11.4.2 Testing the CLD5000 with the service program ..................................................... 130
11.4.3 Testing the interface for CLD5000 with the service program (simulation mode) ... 132
11.5 Cl module ...................................................................................................................... 133
11.5.1 Measuring principle and conditions ....................................................................... 133
11.5.2 Measuring cell "high sensitive" .............................................................................. 133
11.5.3 Measuring cell "sensitive" ...................................................................................... 135
11.5.4 Temperature stabilization of the measuring cell .................................................... 136
11.5.5 Mixer control .......................................................................................................... 138
11.5.6 Measuring cell detection ........................................................................................ 139
11.5.7 Testing the coulometer electronics ........................................................................ 141
11.5.7.1 Testing the "high sensitive" cells .................................................................... 142
11.5.8 Power supply ......................................................................................................... 144
11.5.9 Control electronics ................................................................................................. 145

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 11.5.10 Checking the Cl module >>> components test ...................................................... 148
11.5.10.1 Checking the Cl module >>> Service program (test mode) ........................... 149
11.5.10.2 Checking the Cl module >>> Service program (simulation mode)................. 149
11.6 TC module ..................................................................................................................... 150
11.6.1 Structure of the TC-module ................................................................................... 151
11.6.2 Checking the NDIR optics (hardware) ................................................................... 152
11.6.3 Checking the NDIR optics >>> components test ................................................... 153
11.6.4 Checking the NDIR optics >>> Service program (test mode) ................................ 153
11.6.5 Checking the NDIR optics >>> Service program (simulation mode) ..................... 154
11.6.6 Replacing the NDIR optics ..................................................................................... 154
12 Error evaluation ..................................................................................................................... 155
12.1 Error evaluation with Terminal program (display mode) ................................................ 155
12.2 Error evaluation with multiWin ..................................................................................... 161
12.2.1 Components test.................................................................................................... 161
12.2.2 System information ................................................................................................ 162
12.2.3 Record of LOG-files ............................................................................................... 163
12.2.3.1 MultiWin_info.txt............................................................................................. 165
12.2.3.2 multiWin_Error.LOG ....................................................................................... 165
12.2.3.3 <multiWin_Comm.log>................................................................................... 168
12.3 Error messages ............................................................................................................. 170
13 Consumables......................................................................................................................... 173
14 Spare parts ............................................................................................................................ 173
15 Recommended tools and measuring instruments ................................................................. 174
16 Contact .................................................................................................................................. 175

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1 Generals
The multi EA® 5000 is an analyzer with a modular design. It is used for determining the sulfur,
nitrogen, chlorine and carbon contents of solid, liquid, pasty, viscous and gaseous samples. The
determination is made by pyrolysis followed by thermal oxidation in accordance with national and
international standards.
Depending upon its intended functions, a basic module incorporates at least one detector module
and one sample introduction module. The multiWin® control and evaluation software controls the
basic module and the connected modules, and evaluates the measurement data.
You will find information about the structure and function of the individual detection and sample
introduction modules and about the multiWin® control and evaluation software in their respective
user manuals.

2 Device configuration

Figure 1: Functional diagram multi EA® 5000

The analysis system multi EA® 5000 consists of the basic module containing the sampler control,
detector analysis, combustion module with temperature controller and the gas supply. The center
of the control is the firmware controller unit TERN.

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3 Power supply
The power supply takes place via a 24VDC/3A power supply unit providing the main operating
voltage for the main board (X1) and the gas box (fixed or high performance). In addition the
furnace is controlled via a power supply unit 48VDC/1000W by the temperature controller module.
The remainder of the power supply takes place in the main board and temperature controller
modules (see corresponding sections).
The analyzer is protected by two 6.3AT fuses in the mains switch combination element.

3.1 Temperature controller power supply

The temperature controller obtains its power supply from the main board via X14
(+24VPROTECTED, VCC) and directly from the power supply unit via X5 (+24V). From the +24V
+5V, -5V and +5_REF are being generated and can be measured at the following measuring
points.

3.2 Firmware controller TERN power supply

Figure 2: power supply TERN-firmware controller

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4 Main board
The main board takes care of the remaining power supply and signal distribution for the internal
component assemblies (firmware controller unit, temperature controller, gas ox, AD/DA signal
conversion etc.) and external components (sampler, detectors)

4.1 Main board power supply

The power supply of the main board (24VDC) is protected with a 4.0AT fuse. From this the
following voltages are derived at on the main board:
 +24V....internal temperature, internal MFM
 +24VPROTECTED.... is available after analyzer initialization and required for valves,
temperature controller, gas box and pump controller
 +7.5V.... Power supply for firmware controller TERN
 VCC (+5V).... USB interface/driver
 VREF (+5V).... AD/DA driver circuits

Figure 3: power supply (main board)

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4.2 Service points and service LEDs

The key service measuring points of the main board are on the right side next to the firmware
controller unit. Here all supply voltages (X14) and the input voltages (X13) of the AD converters
can be measured (see also I/O allocation of the firmware controller).
For improved error detection the service LEDs at the top of the main board are used indicating the
switching states of the output ports of the firmware controller unit (see also I/O allocation of the
firmware controller).

Figure 4: service LED/valve-driver(main board)

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Figure 5: interfaces (main board)

Figure 6: flow / temperature evaluation (main board)

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Figure 7: USB-converter (main board)

Figure 8: main board rear side

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5 Firmware controller unit
In the multi EA® 5000 the microcontroller unit TERN is used to control the individual modules. It
receives its commands from the evaluation program multiWin of the external PC (Windows) and is
linked to the main board via the connections J1, J2; J4, H1, H2, H3. The 7.5VDC operating power
supply is implemented via connection Xxx (see figure). This voltage is adjusted down to a
stabilized voltage of 5VDC on the microcontroller unit.

figure 9: Firmware controller TERN

Figure 10: connectors Firmware controller(main board)

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figure 11: Firmware controller TERN with main board

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5.1 I/O allocation

The microcontroller unit has 16 interfaces whose allocations are as listed below.

PIO ValveNo multi EA® 5000 Display Firmware controller Plug-in connector /
port connection
(N7)

A0 V0 Dryer flushing LED V0 J2 / Pin 37 X7 / Pin 4(HPG)

X8 / Pin 3(fixed gas box)
A1 V1 Furnace ventilation LED V1 J2 / Pin 35 X7 / Pin 6(HPG)
X8 / Pin 6(fixed gas box)
A2 V2 LED V2 J2 / Pin 31

A3 V3
LED V3 J2 / Pin 30
A4 V4 NPOC (TOC) LED V4 J2 / Pin 29 X29 / Pin 4
A5 V5 Condensate pump (TOC)
LED V5 J2 / Pin 22 X29 / Pin 5
A6 V6 NS/Cl change-over
LED V6 J2 / Pin 38 X2 / Pin 13
(H=Cl L=N/S)
A7 V7 24 volt valves LED LOCKIN J2 / Pin 20 X2 / Pin 15
B0 V16
LED V16 J2 / Pin 18
B1 V17 Inlet change-over
LED V17 J2 / Pin 17 X7 / Pin 8(HPG)
(H=MVS L=pipe)
X8 / Pin 5(fixed gas box)
B2 V18 Dryer suction pump
LED V18 J2 / Pin 16 Anode D20(K3/A1)
B3 V19
LED V19 J2 / Pin 12
B4 V20
LED V20 J2 / Pin 11
B5 V21
LED V21 J2 / Pin 10
B6 V22
LED V22 J2 / Pin 4
B7 V23 COM change-over optics (TOC)

LED V23 J2 / Pin 3 X29 / Pin 23

C0 Pressure sensor (L=OK )
J2 / Pin 27 X7 / Pin 7
C1 Manual feeder (L=present)
J2 / Pin 25 X9 / 2
C2 Furnace J2 / Pin 24 X5 / Pin 1
(H=vertical ; L=horizontal)

C3 Status TOC J2 / Pin 15 X9 / 4

C4
C5 Flame sensor (L=present) J2 / Pin 13

C6
C7

Figure 12: I/O allocation table

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 PortNo multi EA
5000
(N7)
D A 0
converter
1
2
3
A D 0 Inside J4 / Pin 1 X13 / Pin 2
converter temperature
1 1 Control MFM J4 / Pin 2 X13 / Pin 3
2
3

2  0 Test 24V J4 / Pin 5 X13 / Pin 6

converter 1 Test 6.8V Tern J4 / Pin 6 X13 / Pin 7
1 2 Test 5V dig. J4 / Pin 7 X13 / Pin 8
3 Test 10V Flow J4 / Pin 8 X13 / Pin 9
COM 1 PC X10
2 Optics X23
3 CLD X24

4 Sampler Bus X22

5 TERN Display X15
6 Chlorine X25
7 Sulfur X26 / X27
8 Temperature
controller
9 Gas box X7 / X8
Figure 13: Table AD/DA converter + interface selection

Firmware installation/update is in accordance with the description in the section Software and
firmware.

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5.2 Testing the firmware controller

The microcontroller unit can be tested directly via a Terminal program.

For this purpose the Service PC must be connected to the analyzer over COM5 (see figure) via a
null modem cable.

Service Firmware controller

PC TERN (COM5)

1 4
2 3 used
3 2 used
4 1
5 5 used

7 8
8 7
9 9
Figure 14: Null modem cable allocation

Figure 15: Test mode configuration (up to ser. No. N7-356 )

Figure 16: Test mode configuration (ser.no. N7-357 and higher)

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5.3 Configuration of the Terminal program

The TERN microcontroller unit is updated or tested using a Terminal program, which will be
provided for download with the evaluation program multiWin via extranet (software download).
For the TEST-function (TERN-display) the Terminal program must be configured as follows:

 Start the program <Terminal.exe>

 Select <Configuration> and <Display>

Figure 17: Start of Terminal program (TERN display)

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 - Select the corresponding interface for RS232 communication

Figure 18: interface selection (TERN display)

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 After the Terminal program has been configured and started the following display window is
shown:

Figure 19: Terminal program window 1

 For a test of the main unit (FW-controller) without multiWin, press "A" to adjust the hardware.

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 In the next screen the correct device has to be selected ( "7").

Figure 20: Terminal program window 2

 To configure the temperature controller press "A".

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 The next step is to set the right type of the thermocouple (standard: 1:::Pt-Rh-10).

Figure 21: Terminal program window 3

 For setting of the Zero-Point select “4”.

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 Then you have to connect the short circuit bar (service tool) instead of the thermocouple.

Figure 22: Terminal program window 4

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 Start the “Zero-Point-Adjustment” with <Enter>.

Figure 23: Terminal program-adjust furnace 1

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 After an automatically internal stabilization time, you confirm the new value for the new offset
value (3128). Afterwards this value will be set (stored) inside the TERN microcontroller unit.

Figure 24: Terminal program-adjust furnace 2

For adjustment of the furnace temperature you have to correct the Offset value.
Example:
- current temperature 1060 (measured by an external thermosensor [thermometer]inside the
combustion tube[hottest position]) during the operation (multiWin) within 30 minutes
- nominal(displayed) temperature 1050°C
- correction of displayed temperature with new Offset value:
previous Offset value (14) + 10°= 24

>>> measured temperature 1050°C

>>> displayed temperature 1050°C

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Figure 25: Terminal program-adjust furnace 2

 Using the command <C> you can check the temperature of the furnace; Please reconnect the
thermocouple. Press <enter> to check.

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Figure 26: Terminal program-check temperature

 Exit from this function with <Enter>.

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 For checking the valves and I/O ports please press <D>. This valve check is very similar to the
components test inside the multiWin®-program, there are the same features available.

Figure 27: Terminal program-valve check

 Exit this function with <enter>.

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 The next screen displays the coefficients of the flow calibration and the count of sample
injections after selecting this function with <F>.

Figure 28: Terminal program-print flow calibration

 Using the command <G> you can select the test of the serial ports (COM test).

Figure 29: Terminal program-COM-Test 1

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 Now you have to follow the instructions on screen and connect the required COM ports.

Figure 30: Terminal program-COM test 2

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 With command <I> you can select the LPG/GSS-Test

Figure 31: Terminal program-LPG/GSS-Test

 This function can be used for testing the hardware inside the LPG- or LPG/GSS-module.

 The final test is the measurement of the voltages supplied to the main board.
 With command <J> the voltages supplied to the main board, will be measured and evaluated by
the FW-controller

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Figure 32: Terminal program-Test Voltage

 With the function <K> you can choose another type of analyzer (main board) for testing.

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Figure 33: Terminal program-End

 The command “Q” exit from this test mode.

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6 Software and firmware
The analyzer is controlled via a firmware controller (microcontroller unit "TERN") with responsibility
for the process control of the individual modules and components which it monitors and controls.
The multiWin® program serves as user interface in Windows and communicates with the firmware
controller via a USB port. This USB port is also used for firmware updates.

6.1 Software installation (PC)

The installation routine to install the analysis program starts automatically or is started manually.

Figure 34: Start of installation routine

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6.2 Software update(PC)

A software update will be performed analog to the installation using an update routine.

6.3 Firmware update (TERN controller)

The firmware controller unit operates using a control program (firmware) that communicates with
the external analysis program (PC: multiWin®) via the port COM0 (USB). To ensure a correct
communication between the two programs the protocol ID (version number) of the firmware
program is queried during the initialization of the analyzer and compared to the version of the
multiWin® program. It may therefore be necessary when updating the multiWin® program to also
update the firmware controller unit TERN.
An update of the firmware program is also necessary when replacing the firmware controller. This
is also carried out via the USB port of the analyzer by using multiWin or a terminal program.

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6.3.1 FW-update with UpdateCenter of multiWin

 Close multiWin® software

 Start multiWin
 Login: Operator: Admin
Password: Admin
 Open Menu >>>Extras >>>UpdateCenter Firmware

Figure 35: multiWin-UpdateCenter Firmware

 Select Analyzer

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Figure 36: multiWin-UpdateCenter Firmware analyzer

 Browse for file <TXXXXXXXX.HEX in folder Firmware on CD or download

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 Check that the outlet(heated transfer line) of the auto-protection valve
assembly(combustion tube) is removed from the drying vessel(Cl-module)!

 The UpdateCenter Firmware will guide you now through the whole process of FW-update and
confirm all performed activities with “next”

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 Set the Prog.-jumper (up to N7-356) or the Prog-switch (N7-357 and higher) into prog position

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 The complete Update process needs about 20-25 minutes.

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 Confirm the end of update “finish” with “enter” and switch off the analyzer!

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 Change programming switch from “Prog”(Update) into “RUN”(operation)position.
 Reconnect the outlet of AP valve assembly with the drying vessel(Cl module).
 After the TERN firmware controller has been successful programmed, leave the UpdateCenter
firmware with <ok>
 Close multiWin
 Restart Analyzer, sampling devices and detectors
 Restart multiWin
 Check/update the multiWin program version!
 Check/perform the sampler adjustment!

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6.3.2 FW-update with terminal program

 Close multiWin® software

 Connect the COM-0 interface to the PC

Figure 37: Terminal program FW-update

 (Service program >>> Serviceterminal)

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 Start the program <serviceterminal.exe>

 Open Configuration and select Update

 Select the interface of the used COM port

 Start update

 Select the file <L29F400.hex> for preparation of the update medium

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 Select firmware file <Txxxxxxxx.hex>

 Check that the outlet (heated transfer line) of the auto-protection valve assembly
(combustion tube) is removed from the drying vessel (Cl-module)!

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Figure 38: Switch FW-update

 Change programming jumper from “RUN” into “Update”

 The firmware update will be run automatically. Follow the instruction on screen.

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 Confirm the end of update “finish” with “enter” and switch off the analyzer!
 Change programming switch from “Update” into “RUN” position.
 Reconnect the outlet of AP valve assembly with the drying vessel(Cl module).
 After the TERN firmware controller has been successful programmed, check/update the
multiWin program version!
 Check/perform the sampler adjustment!

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6.4 Replacement of the firmware controller TERN

 Switch off the analyzer and disconnect the mains voltage

 Remove the side wall of the analyzer
 Main board cover by removing the attachment screws
 Disconnect the power supply from the firmware controller unit to the main board
 Remove the firmware controller unit TERN from the main board
 Reconnect the power supply from the firmware controller unit to the main board
 Attach new firmware controller unit to the main board
 Recommission the detector module
 Check/perform firmware update (see firmware update of the microcontroller unit TERN)
 Set gas flow for the "high performance" gas box(main O² h/v)
 Calibrate the gas flow of internal MFM
 Perform/check sampler settings

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7 Combustion module and temperature control
The central unit of the temperature controller is the temperature control module "T control" with its
connections to the furnace module, valve heating, the heated gas transfer and the fans.
The voltage supply to the temperature control module is via the main power supply unit (SP-150-
24) providing 24VDC (see figure).
The adjustment and analysis of the furnace temperature is implemented via the microcontroller unit
(TERN). For this purpose the temperature control module is connected via a plug-in connector to
the main board.

Figure 39: Temperature control module "T-Control" with circuitry

The temperature controller has 4 different heating channels controlled independently of each other
as shown below:

Heating Plug-in
circuit Type connector

Heating 1 Valve heating X11

Heating 2 Transfer line X9
Heating 3 not used X10
Heating 4 Power supply unit(furnace) X13

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7.1 Temperature control for the valve heating and transfer line

The temperature of the heating circuits 1 and 2 is analyzed by a temperature sensor LM35
outputting a voltage of 10mV/°C (X11-3/4 or X9-3/4).
The target temperature of both circuits is fixed to 100°C in the firmware and can be adjusted via
the function "TERN Display" or the Service mode of the multiWin program.

7.2 Temperature control for the furnace heating

The heating coil (3,0…3,6Ω) of the furnace is supplied with direct voltage (48VDC) from the
furnace power supply unit (110...230VAC/ 48VDC) .

The control input Heating 4 (X13-2) switches the power supply unit into the off-mode (12V) or
on-mode (0V).

The furnace of the multi EA® 5000 contains a thermocouple (Pt/Rh10) which is analyzed via
heating circuit 4. The output adjustment/furnace temperature control takes place via the control
input OUT 0 (X13-3) of the furnace power supply unit (110...230VAC/48VDC) by way of voltage
variation (0...5VDC). During the heating up process of the furnace the power supply (furnace)
provides 48VDC (100% = X13-3: 5V). 20° before reaching the set temperature, the power supply
provides only ~50% of voltage (performance) for keeping the temperature (X13-3: 2,5V)

Example:

Set temperature (method) 1050°C

Heating up process: 0...1030°C (100% = 48VDC)

Keeping temperature: 1030…1050°C (50% = 23VDC)

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Figure 40: Temperature controller front view (supply side)

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Figure 41: Temperature controller rear view

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Figure 42: Temperature controller electronics 1

Figure 43: Temperature controller electronics 2

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Figure 44 Temperature controller electronics 3

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7.3 Temperature controller update

7.3.1 Update with program SIOW.exe

 Remove the cover for the temperature controller/main board.

Figure 45: Temperature controller operating mode

 Remove/disconnect the connection cable between the temperature controller and the main
board (TC - main board)
 Move the jumper of the temperature controller from position "Operation" (JP2) to position "Prog"
(lowest position X4)
 Plug the programming cable onto the temperature controller (X3).

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Figure 46: Temperature controller

 Start the file (program) <Siow.exe> for the firmware update of the temperature controller.

Figure 47: Siow.exe file

 Select port >>> Config>>>COM port options

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 Switch on the analyzer >>> Message in the program <Siow> : Please select *.hex file

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 File >>> Download Software >>> hex.file

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 Download complete >>> Switch off device
 Move jumper back to "Operating Position"
 Connect ribbon cable main board - temperature controller >>> remove plug, insert bridge

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7.3.2 Update with UpdateCenter of multiWin

 Close multiWin® software

 Start multiWin
 Login: Operator: Admin
Password: Admin
 Open Menu >>>Extras >>>UpdateCenter Firmware

 Select “Temperature controller”

 Browse for temperature controller FW-file <XXXXXXXX.HEX>

 Don’t transfer a wrong file, it will bring the temperature controller out of function!!!
 Please ask [email protected] for the correct FW version for the temperature
controller and its firmware compatibility.
Another update after a wrong transfer isn’t possible!!!

 The UpdateCenter Firmware will guide you now through the whole process of FW-update and
confirm all performed activities with “next”
 After successful FW update, please close multiWin
 Restart analyzer + multiWin
 Check the temperature settings/adjustment of furnace

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7.4 Setting of the temperature controller

 Commission the service function of the firmware computer (COM5 port) via the HyperTerminal
program

Figure 48: Connection Display/TERN Controller (main board)

 Switch on the device

 >>> A Adjust device
 >>> Select 7

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 >>> A adjust furnace
 >>> Set Pt-Rh-10

Figure 49: Short circuit plug

 >>> Remove thermocouple from temperature controller

 >>> Plug shorting bar (service tool) into thermocouple connection (temperature controller)
 >>> Wait 1 minute to stabilize the temperature controller
 >>> Calculate the Zero-point value by pressing "ok"

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After an automatically internal stabilization time, you confirm the new value for the “Zero-Point” with
<enter>. The new offset value (2608) will be set (stored) inside the TERN microcontroller unit.

Figure 50: temperature sensor inside furnace

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For adjustment of the furnace temperature you have to correct the Offset value.
Example:
- current temperature 1040(measured by an external thermosensor [thermometer]inside the
combustion tube[end of evaporation tube]) during the operation(multiWin) within 30 minutes
- nominal temperature 1050°C
- correction with new Offset value: previous Offset value(14) + 10°= 24

Using the command <C> you can check the temperature of the furnace; to do so you have to
reconnect the thermocouple. Press <enter> to check.
 >>> Reconnect thermocouple to temperature controller
 >>> Exit the menu with: Q

Decommission the service function of the firmware computer (COM5 port) via the HyperTerminal
program

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7.5 Replacing the temperature controller

 Remove the cover for the temperature controller/main board

 Disconnect electrical connections
 Detach temperature controller from the back wall
 The new temperature controller is installed in reverse order
 Carry out a firmware update of the temperature controller
 Define the thermocouple in the service function of the firmware computer TERN
 Adjust the offset of the temperature controller in the service function of the firmware computer
TERN
 Temperature check using an external thermometer in the combustion tube

7.5.1 Checking the furnace

 Measure the resistance of the heating coil (approx. 3,0..3,6 Ohm)

 Measure the temperature in the combustion tube using an external temperature sensor
 Furnace replacement:

7.5.2 Replacing the thermocouple in the furnace

 Move the device into service position (remove front doors)

 Move furnace into the horizontal position
 Remove protective cover
 Disconnect the connection between the thermocouple and the main board
 Pull out the thermocouple
 Insert new thermocouple up to 2mm before the limit stop and secure with the screw
 Connect the thermocouple to the main board
 Adjust the furnace offset in the test mode of the firmware controller
 Measure the temperature in the combustion tube using an external temperature sensor

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7.5.3 Furnace replacement

7.5.3.1 Removing of furnace

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7.5.3.2 Mounting of furnace

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8 Gas supply module
The multi EA® 5000 can be operated in the vertical and the horizontal mode dependent on the
sample matrix to be measured.

Figure 51: flow schema-vertical mode

Figure 52: flow schema-horizontal mode

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The leak test that is carried out automatically (self check) by the multiWin® program is implemented
using the MFM integrated into the C/N/S branch.
The gas supply to the multi EA® 5000 is almost via the "high performance" gas box. The main
board of the first series of multi EA® 5000 (up to ser.no N7-357) was equipped with an option for
another gas box type, which was set by a jumper ("gas box select" >>> fix / HPG) on this main
board. On the new main boards, are only designed for the high performance-gasbox.
The gas box is controlled and communicates via the integrated microcontroller unit (TERN) by
RS232.

Figure 53: Main board (gas box selection[up to ser.-no.N7-357]

Figure 54: Gas box connections

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8.1 Checking the "high performance" gas box

Figure 55: "High performance" gas box flow diagram

The following gas flow rates and gas pressures values can be measured at the respective
connections dependent on the mode (horizontal/vertical).

Input/output Description Gas flow rate / pressure value

E1 Oxygen inlet 4....6bar
E2 Argon inlet 4....6bar

A1 Flushing gas flow for membrane dryer 500ml/min +/-10ml

A2 Main O² 300ml/min +/-5ml
A3 Inlet tube(vertical) 100ml/min +/-5ml
A4 Inlet MVS(horizontal) / NPOC 100ml/min +/-5ml
A5 Valve tube seal 3.0bar
A6 Purge flow Cl-bypass 20ml/min +/-5ml

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8.1.1 Setting the main oxygen (A1) flow rate in the "high performance" gas box

The gas flows Inlet Ar and Inlet O² (furnace/MVS) can be adjusted via the method parameters.
The gas flow Main O² is stored in firmware depending on the:
 initialized furnace position
 installed combustion tube (>> edit device)

This setting can only be performed by authorized service persons as described in the following
section (example: H/V combustion tube):

 For calibration of the main oxygen (Main O²) it is necessary to connect an external flow meter to
the outlet "3" of the "HPG" gas box.

Figure 56: Measuring arrangement for MFC calibration

 In addition, it is necessary to change to the service mode of the multiWin program. This
requires a change of user:

User: Service
Password: ajidc@03677

Figure 57: Service login

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Next the "Service" function must be selected under Extras.

Figure 58: "Service" function selection

 In the next window the component to be calibrated is selected (MFC/MFM).

Figure 59: Component selection

 After selecting the MFC the target gas flow rate for the main oxygen (300ml/min) can be entered
in the next window.

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Figure 60: Setting the target gas flow

 The actual gas flow is measured at output "3" of the gas box and can be modified by adjusting
the set tension.

Figure 61: Saving the gas flow

 After successful calibration of the MFC and saving the values in the firmware controller the main
oxygen (hose no.3) must be reconnected to the combustion tube.

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8.2 Calibrating the internal MFM

To check the tightness of the "HPG" gas box an MFM has been integrated into the gas line to the
N/S/C detector. Using the MFM the firmware controller monitors the tightness in the N/S/C mode.
After replacing the MFM it can be calibrated using a routine.
 For this purpose an external flow meter must be connected to the outlet "Sample N/S/C" of the
analyzer. Please connect a bypass from main O² (gasbox outlet 3) to MFM in to ensure a
correct calibration routine of MFM.

Figure 62: MFM calibration in vertical mode

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Figure 63: MFM calibration in horizontal mode

 Analog to the MFC calibration the service mode is then started:

and MFM selected in the "component selection" window.

Figure 64: Start of the MFM calibration

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 After executing the start function the following screen appears to query an output flow rate
("N/S/C" connection) of 600ml/min from the analyzer.
 If this flow value is incorrect the gas box must be checked for leaks and repaired/exchanged..

Figure 65: Start of the MFM calibration-check 600ml/min

 After confirming the flow rate the automatic calibration of the MFM starts, taking approx. 7
minutes.

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Figure 66: MFM calibration-automatic calibration routine

Figure 67: MFM calibration-Calibration routine with coefficients

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 After completion of the calibration routine the coefficients are calculated automatically. By
pressing the function "Initialize" the new coefficients are transferred to the firmware controller.
 With "Save" they can be saved on the PC in the multiWin directory.
 After completing the gas calibration it is necessary to change from the service mode to the
normal user mode
(user: User; password: User).

8.3 Gas box replacement

 Switch off the device and move the furnace into the horizontal position
 Remove pneumatic and electrical connections from the gas box
 Undo the 4 attachment screws (back wall)
 Remove the gas box towards the front
 Insert new gas box and attach to back wall
 Restore pneumatic and electrical connections
 Check the gas box (gas flow rates and pressure) in accordance with the tables in the section
bearing the same name

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8.4 Check of MFM

 Remove the base protecting shield from the main board

 Measure the voltages of MFM on connector X12 without/with operation (multiWin)

Figure 68: main board-MFM voltages

 Compare the measured monitor voltages(pin 1) with the determined values from flow
Calibration

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8.5 Replacing the MFM

 Remove MFM from the main board via plug-in connector X12
 Install the new MFM
 Perform the MFM calibration routine(see calibration of the internal MFM)

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9 Measuring gas drying unit
9.1 Membrane dryer unit

Because the analysis of the measuring gas in the detectors is sensitive to interference by moisture,
the measuring gas is dried in the analyzer. This is done using concentrated sulfuric acid in the Cl
branch (see user manual section Cl mode). In a C/N/S method a membrane dryer is used for this
purpose. Drying uses the counter-flow method, i.e. the measuring gas flow (red) and the purging
gas flow(green) are in different directions. To utilize the complete drying function of the membrane
dryer the purging gas flow is inducted by a pump.

Figure 69: Membrane dryer and pump

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9.1.1 Tightness check of the membrane dryer

 Loosen the inlet of membrane dryer from the auto-protection valve assembly
 Remove Peek connector from the membrane dryer
 Observe the membrane dryer, that the inert tube is 5mm out from the o-ring
 Cut careful a part of the outer hose and tighten the inert hose into the o-ring by to ensure a
correct drying function
 Reconnect the Peek connector to the membrane dryer and fix it with the ap-valve assembly
 Loosen hose no.5 from the outlet connector (sample out) of membrane dryer.
 Observe the position of inert tube(5mm from o-ring) according the inlet connector Inspection
 Reconnect hose no.5 to the sample out fitting of membrane dryer
 Final test:
o Observe the MFM flow inside the components test
o Interrupt the purge gas flow (hose no.14) to the pump and observe the flow on screen: If the
membrane dryer was tighten correct, there isn’t any change of sample flow value.
o Reconnect the purge flow (hose no.14) to its fitting.

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9.1.2 Replacement of the membrane dryer

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9.2 Auto-protection valve assembly

9.2.1 Valve coupling with filter unit/ checking the filter

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9.2.2 Filter replacement

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9.2.3 Replacing the pneumatic seal

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9.2.4 Removing the complete valve coupling

9.2.5 Check of the AP valve assembly

 Loosen the inlet of membrane dryer from the auto-protection valve assembly
 Remove Peek connector from the membrane dryer
 Observe the membrane dryer, that the inert tube is 5mm out from the o-ring
 Cut careful a part of the outer hose and tighten the inert hose into the o-ring by to ensure a
correct drying function
 Reconnect the Peek connector to the membrane dryer and fix it with the ap-valve assembly
 Loosen hose no.5 from the outlet connector (sample out) of membrane dryer.
 Observe the position of inert tube (5mm from o-ring) according the inlet connector inspection
 Reconnect hose no.5 to the sample out fitting of membrane dryer
 Final test

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10 Sample dosing module
The sample dosing is implemented via the corresponding module (MMS; MMS+ABD; Autoinjector;
LPG;GSS; LPG+GSS). The sample dosing valves communicate via COM4 and are connected to
each other with the following T-cables (sampler connection cables).

Figure 70: communication links

Figure 71: communication links with MMS

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Figure 72: communication links with MMS+ABD

Figure 73: T- cable for Sampler-Bus(basic module – MMS – ABD – LPG - GSS)

Figure 74: pinout of X22 for sampler

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10.1 Auto-injector

The auto-injector features a syringe detection (end position + volume). The end position detection
is via an integrated switch. The syringe volume detection is implemented via optical detection.

The auto-injector is controlled via COM 4, it uses a separately interface at the multi EA® 5000,
which provides also the power supply. A step motor guarantees the velocity-limited injection of the
sample. The power 24VDC for the auto-injector will be supplied by connector X28 (1/5).

Figure 75: pin out of X28 for auto-injector( main board multi EA5000)

The syringes of the auto-injector will be detected by a optical sensor in the aspirating position.

Figure 76: syringes for auto-injector

1…40µl syringe
2…20µl syringe
3…10µl syringe
4…100µl syringe

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Figure 77: auto-injector with syringe

Figure 78: pin-out of holder (auto-injector)

Figure 79: pin-out of connector(auto-injector holder))

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10.2 MMS 5000

The MMS sampler can be fitted with up to 112 samples. It features a syringe and rack size
detection implemented each via magnetic sensors. All additional information can be found in the
MMS 5000 manual

10.2.1 Exchange of the main board

After exchange of the main board (MMS):

 Check/update the correct firmware version
 Enter command “B1” for sampler with syringe
 Check the self-initialization of the MMS in all 4 directions (X,Y,Z + Z1[piston])

10.2.2 Updating the firmware of the MMS sampler

An update of the sampler firmware depends on the main board and the installed firmware:
 main board FW 6.x : update possible with programming device FL101 and program "PSDsoft
Express" (see service manual MMS5000)
 main board FW 11.x and higher: update with Update FirmwareCenter of multiWin program (see
FW update of main unit Chapter)

Please contact [email protected] concerning the compatible sampler firmware version.

10.2.3 Replacing the main board of the MMS sampler

 To replace the main board the rear wall must be removed by undoing the 8 attachment screws.
 The main board can then be disconnected from the rear wall and the connection cables.
 The new main board is installed in reverse order of removal.
 Next the MMS firmware update has to be executed.
 Using the command "B1" (configuration "with syringe"), transferred via the service program, the
sampler is ready for use.
 Check the self-initialization of the MMS in all 4 directions(X,Y,Z + Z1[piston])
 The sampler configuration must then still be carried out in the multiWin program.

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10.2.4 Replacement of mechanical components

 After replacing mechanical components (limit switches, drives, belts) the sampler is tested by a
continuous operation routine of the service program.
 The sampler configuration must then be checked/carried out in the multiWin program.

10.2.5 Rack and syringe detection

The sampler MMS has an automatically rack and syringe detection integrated, which will be
inquired by command <ST> after initialization of the sampler (<Q>)while the initialization routine.
The rack and the syringe will be detected with coded magnets (rack/syringe) and Hall-sensors at
the MMS. Followed sample racks and syringes are available:

syringe type syringe size syringe rack type rack size

magnets
0 no syringe 1 112(AOX)
1 500µl 2 60
2 100µl 3 35(solid)
3 250µl 4 112
4 50µl 7 no rack
5 Solid samples
6 AOX-columns
Figure 80: syringe and rack detection

10.2.6 Check of the auto-sampler with service program

 Please check the MMS with the service program

 Start the service program and select the sampler APG55/60/MMS

Figure 81: sampler check

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 Start the communication with “Start”
 Activate IDC-address

 Send command “Q” for initialisation of the MMS, the firmware version will be send from the
MMS.

 The command “ST” requires the information about the type of the mounted rack and the syringe
size (example 2/4: syringe 100µl / rack 112).
 MultiWin- program detects the MMS only, if rack and the syringe are mounted.

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10.2.7 Testing the interface sampler in simulation mode (MMS5000) with the service
program

 Start the service program and select simulation>>> Sampler>>>MMS

 Select the Rack

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 Start multiWin
 Initialize the analyzer
 Main window of multiWin displays now the MMS5000 with the specific rack

10.3 ABD

The automatic boot feeder unit is used for feeding samples in the horizontal operating mode. This
is controlled dependent on the light intensity of the flame. A photo-resistor is used measure/capture
the light intensity and is amplified by the flame sensor electronics and analyzed by the connected
MVS microcontroller unit. Prior to the calculation the operating point of the flame sensor is
determined. A specific quantity of light should hit the photo-resistor and only vary to a specific
degree. This query takes place within a period of 50 sec. If the flame sensor is outside its operating
range, the error message "Error 14" is issued. This indicates a faulty (fatigued) flame sensor that
has to be replaced.

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10.3.1 Block schema of ABD with multi EA® 5000

Figure 82: operation ABD + multi EA5000

10.3.2 Test of the ABD with service program

 Provide all connections for control of ABD with service program via the T-cable

Figure 83: service program >>> test ABD + multi EA5000

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 Start the service program and select the MVS

 Start the communication with “Start”

 Activate ABD
 Insert “I” for initialization
 Press “V” to display the firmware version
o Answer: “ABD_22-Sept-2010” (or higher version)

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 Press “F” for setting of the flame sensor value

o answer: OkF flame sensor setting correct

o answer: Okf flame sensor setting not successful within 50s

 All commands to control the ABD are described enclosed:

command description

V report version
I initialize
Bn set cooling time (n=1.....900 sec)
A open port
a close port
S.. start sample transfer
s start sample return
E Stop / cancel sample transfer
D display Status
O starting continues output of flame-sensor-value
o display one flame-sensor-value
J fast sample transfer (only ABD)
F start adjustment flame sensor
MVS returns "OKF" if adjustment OK and returns
"Okf", if adjustment not possible within 50 sec.

10.3.3 Testing the interface sampler in simulation mode (ABD) with the service program

 Start the service program and select simulation>>> MVS

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 Activate ABD

 Start multiWin
 Initialize the analyzer (basic initialisation)
 Main window of multiWin displays now the ABD

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10.4 GSS module

The GSS module is used to feed gaseous samples found unpressurized in a corresponding
container to the furnace module.

10.4.1 Structure of GSS module

Figure 84: flow diagram GSS-multi EA5000

Figure 85: GSS - multi EA5000 >>> power supply/communication

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10.4.2 Testing the communication of GSS module with evaluation unit (multiWin®)

 Make a direct connection between the evaluation unit (service program) and the GSS module
via specific T-cable
 Start multiWin
 Initialize the analyzer (basic initialization)
 Main window of multiWin displays now the GSS

10.4.3 Testing the GSS module with the service program

Checking the function and communication of the LPG module using the service program:

 Make a direct connection between the Service PC(service program) and the LPG module via
specific T-cable or a null-modem cable

Figure 86: GSS-service program

 Start the service program

 Device selection >>> GSS

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 "Start" the communication
 Version query with "2V"
 Following commands are available to control the GSS module:

Commands GSS: description

BF fill piston burette

BN reset ml display to zero
dose indicated quantity in
DO<x.x> ml
GDM<x.x> dosing rate in ml/min
MO2 set dosing function
RS report status
SC continue after stop
SH stop

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10.4.4 Testing the interface sampler in simulation mode (GSS module) with the service
program

 Make a direct connection between the Service PC (service program) and the sampler interface
sample via specific T-cable.

 Start the service program

 Simulation >>> GSS

 Start multiWin
 Initialize the analyzer (basic initialization)

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 Main window of multiWin displays now the GSS

10.5 LPG module (LPG/GSS module)

The LPG module (LPG/GSS module) is used to dose liquefied gas samples (+ gaseous samples)
to the furnace module of multi EA® 5000. The liquefied gas sample found in a gas bomb is fed to
the dosing valve. The sample inlet and the dosing valve are cooled by a peltier cooling unit in order
to dose the sample in its liquid state. This permits a high measuring accuracy (repeatability).
The dosing valve has its own internal pneumatic control unit. This in turn is controlled via the
RS232 connection by the internal microcontroller unit of the analyzer (main device). The power
supply is implemented by a power supply unit providing 24VDC.

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Figure 87: flow schema LPG/GSS with multi EA5000

Figure 88: LPG/GSS - multi EA5000 >>> power supply/communication

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10.5.1 Testing the LPG module (LPG/GSS module) with components test of multiWin®

Checking the function and communication of the LPG module using the components test of
multiWin® program:

 Initialize the analyzer unit with LPG module

 Activate a LPG method
 Open the components test >>> instruments >>> components test >>> LPG/GSS
 Make a direct connection between the Service PC(service program) and the LPG module via
specific T-cable or a null-modem cable

Figure 89: LPG/GSS – components test

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10.5.2 Testing the LPG module (LPG/GSS module) with the service program

Checking the function and communication of the LPG module using the service program:

 Make a direct connection between the Service PC (service program) and the LPG module via
specific T-cable or a null-modem cable

Figure 90: service program - LPG/GSS

 Start the service program

 Device selection >>> LPG

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 "Start" the communication
 Version query with "V"

o answer:

 V3OP3.1 CT15 HT80

 V1OP3.1 CT15 HT80

1=LPG or 3=LPG/GSS software version set temperature set temperature

cooling unit (valve) heater (expansion)

 The current temperature of the cooling unit (CT 20 = 20°C) and the heating (HT80 = 80°C) can
be read in the information received by the LPG.

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 Following commands are available for controlling the LPG module (LPG/GSS module)

command description

V show Version
* LPG Vx y.y CTaa HTbb
x=1 LPG, x=2 GSS, x=3 LPG/GSS
y.y = Version
aa = cooling temperature
bb = heating temperature

U xy - Valve on / off
x=1 Ar-Valve
x=2 dosing valve
x=3 switch valve GSS
x=4 activate / deactivate heating and cooling
y=0 off
y=1 on
y=2 switch (only for dosing valve)

G xxx Start dosing LPG xxx = dosing volume(µl)

g xxx Start dosing GSS xxx = dosing volume(µl)
E Stop dosing

K xxx - set sample-loop LPG (µl)

L xxx - set sample-loop GSS (µl)
M xxx - set dose-time (1/10 sek)
T xxx - set heat-temperature (°C)

k Show configuration
* K xxx yyy zzz
xxx = sample-loop LPG(µl)
yyy = sample loop GSS(µl)
zzz = dose time(1/10 sec)

S Show State
s Show state(Service)
*Sxyz
*sxyzab
x=0 ready, x=2 no Ar-pressure,
x=4 heattemp. Out of range, x=8 cooling out of range
x=16 Tempsensor heating out of work, x=32 Tempsensor cooling
out of work
y=0 Ar-valve off, y=1 Ar-valve on
z=0 switching valve GSS off, z=1 switching valve GSS on
a=actual cooling-temp.
b=actual heating-temp.

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10.5.3 Testing the interface sampler in simulation mode (LPG-/GSS module) with the
service program

 Make a direct connection between the Service PC (service program) and the sampler interface
sample via specific T-cable.

 Start the service program

 Simulation >>> LPG/GSS

 Start multiWin
 Initialize the analyzer (basic initialization)

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 Main window of multiWin displays now the LPG/GSS module

10.5.4 Final test of LPG module (LPG/GSS module)

 Reconnect the LPG module with the main unit (multi EA® 5000)
 Initialize Check the carrier gas flow of 55ml/min without sample connection
 Connect a sample bomb and check the tightness of dosing valve, expansion chamber and
hoses
 Analyze a known LPG sample or a standard and check the reproducibility.

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11 Detectors
11.1 UVFD APSA370

For detailed description of operation, service and maintenance, please use the specific manuals for
APSA370.

11.1.1 Check of technical parameter and requirements APSA370 on its display

Figure 91: APSA370-ANALOG INPUT

Display APSA370 analogue values

These technical parameter should be in expected range:

- LAMP [light intensity] : 200…1000mV (Alarm <200mV)

- PUMP [pressure]: 40…50KPa (Ambient-55KPa)
- SAMPLE [flow]: 0,2….1,0l/min

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11.1.2 Testing the communication of APSA370 with evaluation unit(multiWin®)

11.1.3 Testing the APSA370 with the service program

Checking the UVFD using the service program:

 Ensure a direct connection between the Service PC (service program) and the UVFD via null
modem cable (RS232)

 Start the service program (<geraetetest.exe>)

 Device selection >>> UVFD >>> APSA360/370

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 "Start" the communication between Service program and UVFD

command description

DA display measurement status/values

Z1 show firmware version

11.1.4 Testing the interface for APSA370 with the service program (simulation mode)

Checking the interface of firmware controller (multi EA® 5000) using the service program
 Ensure a direct connection between the Service PC (service program) and the analyzer (UVFD
interface) via null modem cable
 Start the service program
 Simulation >>> UVFD >>> APSA360/370
(Enable "log commands" for subsequent analysis)

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 Start multiWin
 Initialize the analyzer (basic initialization)

 Main window of multiWin displays APSA 370 as UVFD

11.2 UVFD5000

For detailed description of operation, service and maintenance, please use the specific manuals for
UVFD 5000.

11.2.1 Check of technical parameter inside the components test (multiWin)

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Figure 92: UVFD5000 – components test

These technical parameter should be in expected range:

- Temperature sensor : 14…16°C
- Temperature lamp: < 65°C

11.2.2 Testing the UVFD5000 with the service program

Checking the UVFD using the service program:

 Ensure a direct connection between the Service PC (service program) and the UVFD via null
modem cable (RS232)

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 Start the service program (<geraetetest.exe>)
 Device selection >>> UVFD >>> UVFD5000

 "Start" the communication between Service program and UVFD

command description status

V display firmware version V UVFD_110321_417

D display analyzer data Y 19.22 205.494 203.398 10.2747 28.0 01b 1.0

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11.2.3 Testing the interface for UVFD5000 with the service program (simulation mode)

Checking the interface of firmware controller (multi EA® 5000) using the service program
 Ensure a direct connection between the Service PC (service program) and the analyzer (UVFD
interface) via null modem cable
 Start the service program
 Simulation >>> UVFD >>> UVFD5000
(Enable "log commands" for subsequent analysis)

 Start multiWin
 Initialize the analyzer (basic initialization)

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 Main window of multiWin displays UVFD5000

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11.3 CLD APNA370

For detailed description of operation, service and maintenance, please use the specific manuals for
APSA370.

11.3.1 Check of technical parameter and requirements APNA370 on its display

Figure 93: APNA370-ANALOG INPUT

Display APNA370 analogue values

These technical parameters should be in expected range:

- DETECTOR [temperature]: 40…45°C

- DETECTOR [pressure]: 70…80KPa (Ambient-25KPa)
- SAMPLE [flow]: 0,9 1,3l/min

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11.3.2 Testing the communication of APNA370 with evaluation unit (multiWin®)

11.3.3 Testing the APNA370 with the service program

Checking the CLD using the service program:

 Ensure a direct connection between the Service PC (service program) and the CLD via null
modem cable (RS232)

 Start the service program (<geraetetest.exe>)

 Device selection >>> CLD >>> APNA360 (APNA370)

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 "Start" the communication between Service program and CLD

command description

DA display measurement status/values

Z1 show firmware version

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11.3.4 Testing the interface for APNA370 with the service program (simulation mode)

Checking the interface of firmware controller (multi EA® 5000) using the service program:
 Ensure a direct connection between the Service PC (service program) and the analyzer (CLD
interface) via null modem cable
 Start the service program
 Simulation >>> CLD >>> APNA360 (APNA370)
(Enable "log commands" for subsequent analysis)
 Start multiWin
 Initialize the analyzer (basic initialization)
 Main window of multiWin displays APNA 370 as CLD

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11.4 CLD5000

For detailed description of operation, service and maintenance, please use the specific manuals for
CLDD5000.

11.4.1 Check of technical parameter inside the components test (multiWin)

These technical parameter should be in expected range:

- Pressure differential: 300…600mbar
- Temperature exhaust : 390…410°C (set-temperature+/-10°C):

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11.4.2 Testing the CLD5000 with the service program

Checking the UVFD using the service program:

 Ensure a direct connection between the Service PC (service program) and the UVFD via null
modem cable (RS232)

 Start the service program (<geraetetest.exe>)

 Device selection >>> CLD >>> CLD5000

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 "Start" the communication between Service program and CLD

command description status

V display firmware version V EACLD_120223_605

D display analyzer data Y 0.09 2806.12 2804.99 2805.85 349.4 19 401.0 0 2805.02 -20.375

O O3-generator on

o O3-generator off

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11.4.3 Testing the interface for CLD5000 with the service program (simulation mode)

Checking the interface of firmware controller (multi EA® 5000) using the service program
 Ensure a direct connection between the Service PC (service program) and the analyzer (CLD
interface) via null modem cable
 Start the service program
 Simulation >>> CLD >>> CLD5000
(Enable "log commands" for subsequent analysis
 Start multiWin
 Initialize the analyzer (basic initialization)
 Main window of multiWin displays CLD5000

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11.5 Cl module

11.5.1 Measuring principle and conditions

The Cl-module is equipped with a coulometer electronics supporting the potentiometric (high
sensitive cell) and the amperometric (sensitive or high concentrated) principle.
For the multi EA® 5000 the measuring cells "high sensitive" and "sensitive" are recommended in
depends on the application or measuring range(see data sheet in the operation manual).

11.5.2 Measuring cell "high sensitive"

In the options "high sensitive cell" operates a sensor electrode for indication and platinum (Pt) +
silver electrode (Ag) for generation of silver ions. The sample gas will be introduced through a glas
capillary into the electrolyt of coulometric cell.

Figure 94: gas schema of Cl-module ("high sensitive cell")

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Figure 95: "high sensitive cell" - electrodes

Figure 96: Overview of the Cl-module ("high sensitive cell")

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11.5.3 Measuring cell "sensitive"

In the options "sensitive cell" operates a combination electrode for indication and generation. This
electrode combines indicator electrodes (Ag), generator cathode (Pt) and gas inlet. The
combination electrode is stored in the corresponding storage container in the front door after the
measurement was finished. This must be filled with electrolyte. The generator anode is as a silver
circle in the two base elements of the measuring cells.
The recommended filling level for the measuring cell is shown in the figure below. This filling level
must be checked before the measurement. During the measurement it must be ensured that the
filling level does not drop below the specified minimum. The measuring cell cover must be attached
during the measurement by its corresponding attachment screws.

Figure 97: Filling level of the "sensitive" measuring cell

Figure 98: Overview of the Cl module ("sensitive cell")

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11.5.4 Temperature stabilization of the measuring cell

A Peltier cooling installed under the holder of the measuring cell is used for the temperature
stabilization of the electrolyte. The target temperature is set in the method configurations of the
multiWin program. The device test program is required for checking the stability of the measuring
cell temperature. The PC with the device test program is connected to the chlorine module via a
null modem cable. The program must be started after switching on the device. In the menu bar
under “Device selection” the coulometer of type 2 is then selected.

A new window opens in the menu bar under Start. With the command <SE> the continuous
transmission of parameters starts.

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Figure 99: Cl-module ”high sensitive” - <SE>

In the field Received the penultimate value indicates the Peltier temperature. Because the program
continually receives data from the chlorine module, the temperature is changing continually. The
temperature may fluctuate by max. ± 3°C. Using a thermometer it must also be checked that the
output temperature matches the real temperature.

Figure 100: Circuit diagram of the temperature stabilization

Figure 98 shows the measuring points for the temperature stabilization. At the plug-in connector X4
under the pins 1 and 2 the operating voltage of 5 V for the fan of the Peltier element can be
measured. At pins 3 and 4 the operating voltage of 5 V of the Peltier element can be picked up.

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Pins 6 and 7 are measuring points of the temperature sensor for the Peltier temperature. Here a
voltage of 100 to 300 mV is present, corresponding to a temperature of 10 to 30°C. The fuse F1
(1AT) is connected upstream of the Peltier unit. At pin 5 the operating voltage (5VDC) of the
temperature sensor can be measured.

Figure 101: temperature-/mixer control board

11.5.5 Mixer control

The mixing of the electrolyte by a magnetic mixer in the measuring cell is carried out by an array of
electromagnets fitted below the measuring cell adapter. This can be tested using a filled measuring
cell. The chlorine module must be connected to a Service PC for this purpose. The mixing function
is active when the module is switched on.

The measuring points for the mixer control are in the circuit diagram annex 4. At the plug-in
connector X3 under pins 1 and 2 an operating voltage of 24 V can be measured. At the voltage
regulator IC2 a voltage of 5 V can be picked up. Because IC2 is very inaccessible, the 5 V is
measured at the measuring point and pin 2 of the plug-in connector X3 (figure 100). The fuse F2
protects with 2.5 AT the power supply for the mixer control.

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Figure 102: temperature-/mixer control board

11.5.6 Measuring cell detection

Figure 103: Measuring cell detection

1… Magnetic sensor for the measuring cell detection

2 ... Measuring cell adapter
3… Measuring cell guide

The multi EA® 5000 works with an automatic measuring cell detection.
The type of the measuring cell in the Cl-module is automatically detected by the analysis of
magnetic sensors during the initialization of the analyzer. At the rear of the measuring cells
corresponding magnets have been fitted.

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The device test program is used to test the measuring cell detection. With the SE command the
continuous transmission of parameters starts.
For an analysis of the measuring cell type the first value issued in the field Received is used. With
the output A01 a "sensitive" measuring cell and with the output A10 a "high concentration"
measuring cell is used.

Figure 104: connector X8 - cell detection

The measuring points for the cell detection are in the circuit diagram annex 4. At the plug-in
connector X8 under pins 1 and 10 an operating voltage of 10 V can be measured. At the pins 1
and 10 a voltage of 5 V is present.

TTL1 TTL2 TTL3 TTL4 Type of cell

Measuring cell [X8/Pin5] [X8/Pin6] [X8/Pin7] [X8/Pin8] [Service program]

high sensitive H H L H P100

sensitive H L H H A01

high concentrated L H H H A10

Figure 105: Measuring cell detection

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11.5.7 Testing the coulometer electronics

Figure 106: Plug-in connector X12 – coulometer pcb

The coulometer electronics can be tested by measuring the voltage at specified measuring points.
Pin 1 of the plug-in connector X12 represents the mass during the measurements. At pin 3 the
main operating voltage of 24V of the coulometer board can be measured. At pin 8 10 V are present
and at pin 10 5 V. These are the reference voltages of the coulometer electronics. At pin 7 +5 V
can be measured and at pin 9 -5 V.

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11.5.7.1 Testing the "high sensitive" cells

Figure 107: Test circuit for measuring the voltage(sensor electrode) of ”high sensitive cell”

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Figure 108: Test circuit for measuring the generator current of ”high sensitive cell”

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Figure 109 coulometer pcb (pinout of sensor electrode)

1….ground
2… voltage sensor electrode (behind preamplifier) 1,0….2,00V
3… +12V
4… -12V

11.5.8 Power supply

The power supply of the Cl module is implemented for the control electronics and the coulometer
via the power supply unit NT_24V (110...230VAC/24VDC). The Peltier power supply unit
(110...230VAC/5VDC) provides only the supply voltage for the Peltier element of the cooling unit.

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11.5.9 Control electronics

Figure 110: Control electronics Cl module- view from top

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Figure 111: Control electronics Cl module - rear face

Figure 112: Cl module Control electronics 1

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Figure 113: Cl module Control electronics 2

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11.5.10 Checking the Cl module >>> components test

 Open the left side wall

 Check the operating voltages of the coulometer
 Check the coulometer in the component test of the multiWin® program

Figure 114: Component test Cl-module "high sensitive"´

Figure 115: Component test Cl module "high sensitive"´ >>> start generator current 100µA

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11.5.10.1 Checking the Cl module >>> Service program (test mode)

Checking the Cl module using the service program:

 Make a direct connection between the Service PC (service program) and the Cl module via null
modem cable
 Start the service program
 Device selection >>> Coulometer
 "Start" the communication between Service program and the coulometer
(for commands see the help function of the service program)

11.5.10.2 Checking the Cl module >>> Service program (simulation mode)

Checking the port at the firmware controller using the service program
 Make a direct connection between the Service PC(service program) and the analyzer (Cl
interface) via null modem cable
 Start the service program
 Simulation >>> Coulometer
(Enable "log commands" for subsequent analysis)

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 Start multiWin
 Initialize the analyzer (basic initialization)
 Main window of multiWin displays Cl module

11.6 TC module

In the TC module the CO2 content of the sample after oxidation is determined using NDIR optics.
The NDIR optics are supplied with the necessary voltages by their own internal power supply. The
radiation source sends an infrared light via its internal optics that is analyzed by the internal NDIR
controller.

Figure116: principle of NDIR-detector

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11.6.1 Structure of the TC-module

Figure 117: sample flow schema TC-module

Figure 118: power supply/communication of TC-module

The input fuses 4,0A (time-lag) are located in the main power socket. The communication will be
performed by a null-modem cable to the firmware controller of multi EA® 5000.

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11.6.2 Checking the NDIR optics (hardware)

 Open the right side door of the TC module

 Check the operating voltages

Figure 119: NDIR-detector

1…+24V
2…-15V
3…GND (+/-15V)
4…+15V
5…GND (5V/24V)
6…+5 V
7… interface connector “slave” (not used)
8… jumper interface selection (“master” position)
9… interface connector “master” (to firmwarecontroller multi EA® 5000)

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11.6.3 Checking the NDIR optics >>> components test

Check the NDIR detector in the component test of the multiWin® program
 The analogue values must in the nominal range after warm-up time of 20 minutes:
 Minimal AD-value: 1000….30000
 Maximal AD-value: 34000…64000
 If the AD-values are out of the ranges, please exchange the whole NDIR-detector.

Figure 120:: component test - NDIR

11.6.4 Checking the NDIR optics >>> Service program (test mode)

Checking the C-module using the service program:

 Make a direct connection between the Service PC (service program) and the Cl-module via null
modem cable
 Start the service program
 Device selection >>> NDIR >>> C201
 "Start" the communication between Service program and NDIR (C201)
(for commands see the help function of the service program)

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11.6.5 Checking the NDIR optics >>> Service program (simulation mode)

Checking the port at the firmware controller using the service program
 Make a direct connection between the Service PC(service program) and the analyzer (C-
interface) via null modem cable
 Start the service program
 Simulation >>> NDIR >>> C201
(Enable "log commands" for subsequent analysis)

11.6.6 Replacing the NDIR optics

 Open the right/left side door of the TC module

 Disconnect the gas connections
 Disconnect the electrical connections and protective ground from the NDIR detector
 Remove the NDIR base plate
 Remove the NDIR detector from the base plate
 Installation of the NDIR detector is in reverse order of removal
 Check/set the jumper for the communication to “master”
 After recommissioning the analyzer a standard substance (TC) must be measured after a
stabilization period of 1h

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12 Error evaluation
12.1 Error evaluation with Terminal program (display mode)

Figure 121: Test mode configuration (up to ser. No. N7-356)

Figure 122: Test mode configuration (ser.no. N7-357 and higher)

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Figure 123: TERN display start screen (operating mode)

The test function of the firmware controller unit must be activated with "T". In addition, the data
output must be activated from minimum to maximum using the "I" key. To record this information
for subsequent analysis the following setting must be completed:
Transfer >>> Capture Text>>> browse to the right folder and insert a name for this file(N7-xxx_x)
- press “start” for start of record communication(firmwarecontroller)
- multiWin can be started now

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As followed you’ll find a captured communication of the firmware controller:

Auswahl: InitBoard durchlaufen T0813042315

GTyp=7
VorInit durchlaufen
an PC:1*15*ERRO*50*T0813042315*079

A = Adjust-Device
T = Testmode on/off <on>
D = Demomode on/off <off>
S = SampDemo on/off <off>
I = more Info on/off <off>

vom PC=16*DEMO*1*0*005
an PC:2*16*DEMO*0*006
Auswahl: vom PC=5*VERS*1*ee5b6ef1-8ddc-4b3d-bd93-e1c4e6367751*0*088
MAC=ee5b6ef1-8ddc-4b3d-bd93-e1c4e6367751
an PC:3*5*VERS*1*T0813042315*0*074
Auswahl: vom PC=0*INIT*0*7*15*7*0*2*028
Geraet.Typ=7
an PC:4*0*INIT*0*0*052
Auswahl: I
Rohrtyp=2
OfenTyp[0]=0
an PC:5*0*INIT*0*0*053
AntwOfen=V TC4 09 G4
OfenTyp[0]=0
an PC:6*0*INIT*0*0*054
an PC:7*0*INIT*0*0*055
Test Optik durchlaufen Typ=0
an PC:8*0*INIT*0*0*056
Test N-Sensor durchlaufen Typ=16
an PC:9*0*INIT*0*0*057
Fehler Horiba Antw=
zum S-Coul=#00/2f
Test S-Sensor durchlaufen Typ=32
an PC:10*0*INIT*0*0*001
zum Cl-Sensor: SG
zum Cl-Sensor: HY
zum Cl-Sensor: HY
zum Cl-Sensor: DI
Cl-In=11
zum Cl-Sensor: SW
CL-Modus= A0
zum Cl-Sensor: RW100
TestCl-Sensor durchlaufen Typ=1
an PC:11*0*INIT*0*0*000
zum Cl-Sensor: C32
an PC:12*0*INIT*0*0*003
an PC:13*0*INIT*0*0*002
an PC:14*0*INIT*0*0*005
an PC:15*0*INIT*0*0*004
an PC:16*0*INIT*0*0*007
an PC:17*0*INIT*0*0*006

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zum Cl-Sensor: HY
zum Cl-Sensor: C0
an PC:18*0*INIT*0*0*009
zum Samp=6
zum Samp=6Q
an PC:19*0*INIT*0*0*008
an PC:20*0*INIT*0*0*002
an PC:21*0*INIT*0*0*003
an PC:22*0*INIT*0*0*000
an PC:23*0*INIT*0*0*001
OK/OKU Sampler empf.
an PC:24*0*INIT*0*0*006
zum Samp=6ST
SampKonf=2 4
Init InitParam : Samp.Rack 4
XYZ Probe: 59 1451 543
XYZ Spl : 1098 113 1281
XYZ Ofen : 871 393 1485
zum Samp=6A
zum Samp=6ZL10
zum Samp=6S
an PC:25*0*INIT*0*0*007
an PC:26*0*INIT*0*0*004
zum LPG=2
zum LPG=2V
vom LPG=LPG V3NP 3.2 CT15 HT80
LPG.Typ=3
zum LPG=2k
vom LPG=K 1 250 15
V_LPG=1 V_GSS=250 D_Time=6
zum LPG=2U 41
an PC:27*0*INIT*0*0*005
zum MVS
zum MVS 1V
vom MVS ABD_17-Jan-14
an PC:28*0*INIT*0*0*010
an PC:29*0*INIT*0*0*011
an PC:30*0*INIT*0*1*0*16*32*1*0*144*64*52*100*0*000
vom PC=0*INIT*1*049
Geraet.Typ=7
an PC:31*0*INIT*1*0*003
Auswahl: I
Rohrtyp=2
OfenTyp[0]=0
an PC:32*0*INIT*1*0*000
AntwOfen=V TC4 09 G4
OfenTyp[0]=0
an PC:33*0*INIT*1*0*001
an PC:34*0*INIT*1*0*006
an PC:35*0*INIT*1*0*007
Test N-Sensor durchlaufen Typ=16
an PC:36*0*INIT*1*0*004
Fehler Horiba Antw=
zum S-Coul=#00/2f
Test S-Sensor durchlaufen Typ=32

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an PC:37*0*INIT*1*0*005
zum Cl-Sensor: SG
zum Cl-Sensor: HY
zum Cl-Sensor: DI
Cl-In=11
zum Cl-Sensor: SW
CL-Modus= A0
zum Cl-Sensor: RW100
TestCl-Sensor durchlaufen Typ=1
an PC:38*0*INIT*1*0*010
zum Cl-Sensor: C32
an PC:39*0*INIT*1*0*011
an PC:40*0*INIT*1*0*005
an PC:41*0*INIT*1*0*004
an PC:42*0*INIT*1*0*007
an PC:43*0*INIT*1*0*006
an PC:44*0*INIT*1*0*001
zum Cl-Sensor: HY
zum Cl-Sensor: C0
an PC:45*0*INIT*1*0*000
zum Samp=6
zum Samp=6Q
an PC:46*0*INIT*1*0*003
an PC:47*0*INIT*1*0*002
an PC:48*0*INIT*1*0*013
an PC:49*0*INIT*1*0*012
an PC:50*0*INIT*1*0*004
OK/OKU Sampler empf.
an PC:51*0*INIT*1*0*005
zum Samp=6ST
SampKonf=2 4
Init InitParam : Samp.Rack 4
XYZ Probe: 59 1451 543
XYZ Spl : 1098 113 1281
XYZ Ofen : 871 393 1485
zum Samp=6A
zum Samp=6ZL10
zum Samp=6S
an PC:52*0*INIT*1*0*006
zum LPG=2
zum LPG=2V
vom LPG=LPG V3NP 3.2 CT15 HT80
LPG.Typ=3
zum LPG=2k
vom LPG=K 1 250 15
V_LPG=1 V_GSS=250 D_Time=6
zum LPG=2U 41
an PC:53*0*INIT*1*0*007
zum MVS
zum MVS 1V
vom MVS ABD_17-Jan-14

an PC:11*1*STAT*1*#*0*0*0*0*157*0*0*0*0*0*0*0*024
an PC:12*1*STAT*1*#*0*0*0*0*157*0*0*0*0*0*0*0*027
vom Tempcont C 92 0 0 157 128

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an PC:13*1*STAT*1*#*0*0*0*0*157*0*0*0*0*0*0*0*026
an PC:14*1*STAT*1*#*0*0*0*0*157*0*0*0*0*0*0*0*029
vom Tempcont C 92 0 0 157 128
an PC:15*1*STAT*1*#*0*0*0*0*157*0*0*0*0*0*0*0*028
an PC:16*1*STAT*1*#*0*0*0*0*157*0*0*0*0*0*0*0*031
vom Tempcont C 92 0 0 157 128

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12.2 Error evaluation with multiWin

12.2.1 Components test

Figure 124: components test – control flow

Figure 125: components test - valves

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12.2.2 System information

Figure 126: System Information

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12.2.3 Record of LOG-files

Figure 127: multiWin – Error analysis 1

Figure 128: multiWin – Error analysis 2

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Any errors occurring during operation are constantly recorded in LOG files
(<multiWin_Error.LOG>) or when requested (<multiWin_Flow.txt> ; <multiWin_COMM.txt>) and
can be analyzed by the Service after transmission. They are found in the user files folder (see fig.
multiWin application data).

<multiWin_info.txt> : systemparameter after saving

<multiWin_Error.LOG> : all error messages

<multiWin_Flow.txt> : program flow of multiWin(command sequences)

<multiWin_COMM.txt> : communication between PC and firmwarecontroller

<multiWin_Exception.txt> : access violation, detailed error description of multiWin-errors-

The LOG-files can be carried out directly in the windows explorer under:

C:\documents and settings\all user\application data\ajidc\multiWin\N7-xxx

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12.2.3.1 MultiWin_info.txt
[System]
OSName = Windows XP; Microsoft Windows NT 5.1.2600 Service Pack 2
CPU = x86 Family 6 Model 15 Stepping 13; Intel(R) Pentium(R) Dual CPU E2200 @ 2.20GHz; 2194MHz
.NET runtime version: v2.0.50727

[Application]
multiWin = 5.3.5.0

[Device]
SerialNumber = N7-212/L
Firmware = T0813042315
ProtocolId = 8

[Detectors]
N = EACLD_130809_610
S = UVFD_110427 521
Cl = Vers.4_1 SW 110714

[Other]
Sampler = 11.3
TemperatureController = TC4 09 G4
GasSupply = TRIPLE MFC-Controller V3_4 SW 04-04-2011
ABD = ABD_17-Jan-14
LPG = LPG V3NP 3.2 CT15 HT80

12.2.3.2 multiWin_Error.LOG
[System]
OSName = Microsoft Windows XP Professional; 5.1.2600; Service Pack 2
CPU = x86 Family 6 Model 15 Stepping 13; Intel(R) Pentium(R) Dual CPU E2200 @ 2.20GHz;
2194MHz
.NET runtime version: v2.0.50727

[Application]
multiWin = 5.0.3619.0

[Device]
SerialNumber = N7-012/I
Firmware =
ProtocolId = 3

[Detail]

2012.04.27 07:54:48,265625 CommERRO_0011 NoSignalReceived VERS

2012.05.31 18:05:25,625000 CommERRO_0205 GasBoxCommunicationError4
2012.06.04 11:56:35,000000 CommERRO_0017 ProtocolIdError; PC: 7, firmware: 6
2012.06.15 09:33:44,359375 CommERRO_0011 NoSignalReceived VERS
2012.06.15 09:35:01,671875 CommERRO_0011 NoSignalReceived VERS
2012.07.02 12:30:22,015625 CommERRO_0110 NDetectorNoConnectionTo
2012.07.02 12:30:32,687500 CommERRO_0120 SDetectorNoConnectionTo
2012.12.17 11:24:39,437500 CommERRO_0250 LPGNoConnection
2013.01.14 08:42:42,093750 CommERRO_0110 NDetectorNoConnectionTo

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2013.01.14 08:42:59,781250 CommERRO_0120 SDetectorNoConnectionTo
2013.01.28 17:53:10,140625 CommERRO_0120 SDetectorNoConnectionTo
2013.01.30 09:26:37,781250 CommERRO_0270 AutoInjectorSyringeNoConection
2013.01.30 10:23:57,656250 CommERRO_0273 AutoInjectorSyringeFillingNotCorrect
2013.01.30 10:25:28,250000 CommERRO_0270 AutoInjectorSyringeNoConection
2013.12.06 09:26:41,250000 CommERRO_0250 LPGNoConnection
2013.12.16 18:25:58,859375 CommERRO_0052 FirmwareStandby

2014.01.16 15:09:21,046875 CommERRO_0232 FlamesensorError

2014.02.13 13:26:50,890625 CommERRO_0050 FirmwareReset T0813042315
2014.02.18 15:12:36,312500 CommERRO_0273 AutoInjectorSyringeFillingNotCorrect
2014.03.11 10:42:58,015625 CommERRO_0134 ClDetectorWrongStatus
2014.03.11 10:42:58,640625 CommERRO_0137 ClDetectorCheckMeasuringCell
2014.03.11 10:43:01,609375 CommERRO_0134 ClDetectorWrongStatus
2014.03.11 10:43:02,234375 CommERRO_0137 ClDetectorCheckMeasuringCell
2014.03.12 16:48:59,890625 CommERRO_0014 SignalDataFlowError
2014.03.12 16:51:59,656250 CommERRO_0011 NoSignalReceived DEMO
2014.03.13 09:17:55,328125 CommERRO_0014 SignalDataFlowError
2014.03.13 09:21:33,156250 CommERRO_0011 NoSignalReceived DEMO
2014.03.14 07:55:41,062500 CommERRO_0011 NoSignalReceived DEMO
2014.03.14 10:55:19,328125 CommERRO_0110 NDetectorNoConnectionTo
2014.03.14 11:16:20,171875 CommERRO_0018 ReturnError; METH; 50
2014.03.19 14:50:06,968750 SerialCommunication.Read.TimeoutException
5*3*MESS*j60*0*0*0*0*1
2014.03.19 14:50:11,484375 CommERRO_0014 SignalDataFlowError
2014.03.19 14:50:56,890625 CommERRO_0011 NoSignalReceived DEMO
2014.03.20 10:37:54,265625 CommERRO_0134 ClDetectorWrongStatus
2014.03.25 16:04:56,812500 CommERRO_0011 NoSignalReceived DEMO
2014.03.26 11:42:50,609375 SerialCommunication.Read.TimeoutException ?
2014.03.26 11:43:19,468750 CommERRO_0067 MTXTMissing
2014.03.26 11:44:23,578125 CommERRO_0014 SignalDataFlowError
2014.03.26 11:44:25,921875 SerialCommunication.Read.TimeoutException ?
2014.03.26 11:48:08,718750 CommERRO_0067 MTXTMissing
2014.04.01 10:23:12,125000 CommERRO_0011 NoSignalReceived DEMO
2014.04.01 10:30:31,156250 CommERRO_0050 FirmwareReset T0813042315
2014.04.07 08:33:46,578125 CommERRO_0250 LPGNoConnection
2014.04.11 08:19:06,015625 CommERRO_0011 NoSignalReceived DEMO
2014.04.14 11:14:34,703125 CommERRO_0232 FlamesensorError
2014.04.14 11:19:09,125000 CommERRO_0014 SignalDataFlowError
2014.04.14 11:21:34,109375 CommERRO_0232 FlamesensorError
2014.04.15 08:54:37,203125 CommERRO_0110 NDetectorNoConnectionTo
2014.04.15 11:24:50,703125 SerialCommunication.Read.TimeoutException 
2014.04.15 11:24:55,203125 CommERRO_0014 SignalDataFlowError
2014.04.15 11:31:47,531250 CommERRO_0011 NoSignalReceived DEMO
2014.04.16 08:46:30,125000 CommERRO_0014 SignalDataFlowError
2014.04.25 09:28:25,375000 CommERRO_0014 SignalDataFlowError
2014.04.25 10:08:37,375000 CommERRO_0050 FirmwareReset T0813042315
2014.04.28 16:49:35,296875 CommERRO_0014 SignalDataFlowError
2014.05.07 14:18:12,812500 CommERRO_0011 NoSignalReceived DEMO
2014.05.07 14:29:30,609375 CommERRO_0020 TimeoutInitEnd;
2014.05.15 11:05:36,406250 CommERRO_0050 FirmwareReset T0813042315
2014.05.28 17:14:09,437500 CommERRO_0014 SignalDataFlowError
2014.05.28 17:14:27,218750 CommERRO_0011 NoSignalReceived DEMO
2014.05.28 17:53:00,718750 CommERRO_0226 SamplerRuntimeExceeded
2014.06.02 11:37:27,859375 CommERRO_0222 BoatBroken

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2014.06.02 11:40:21,468750 CommERRO_0224 SamplerFalseClamshell
2014.06.02 17:20:34,546875 CommERRO_0107 CDetectorAnalogValuesOutOfRange
2014.06.03 08:55:29,125000 CommERRO_0050 FirmwareReset T0813042315
2014.06.03 14:33:05,984375 CommERRO_0011 NoSignalReceived ENDE
2014.06.04 12:46:38,937500 CommERRO_0021 TimeoutCheckStatusOK;
2014.06.05 11:40:30,375000 CommERRO_0220 SamplerNoConnection
2014.06.16 10:37:03,000000 CommERRO_0011 NoSignalReceived DEMO
2014.06.17 14:09:13,218750 CommERRO_0224 SamplerFalseClamshell
2014.06.30 11:00:50,421875 CommERRO_0134 ClDetectorWrongStatus
2014.06.30 12:01:29,937500 CommERRO_0014 SignalDataFlowError
2014.06.30 12:02:21,656250 CommERRO_0011 NoSignalReceived DEMO
2014.07.07 13:28:54,015625 CommERRO_0206 GasPreasureError
2014.07.07 14:15:39,000000 CommERRO_0206 GasPreasureError
2014.07.17 13:48:50,875000 CommERRO_0014 SignalDataFlowError
2014.07.21 10:28:00,906250 CommERRO_0011 NoSignalReceived DEMO
2014.07.21 10:28:06,234375 CommERRO_0050 FirmwareReset T0813042315
2014.07.29 21:17:18,156250 CommERRO_0052 FirmwareStandby
2014.07.31 17:14:30,781250 CommERRO_0120 SDetectorNoConnectionTo
2014.07.31 17:14:37,875000 CommERRO_0110 NDetectorNoConnectionTo
2014.07.31 17:14:39,578125 CommERRO_0120 SDetectorNoConnectionTo
2014.07.31 17:26:04,171875 CommERRO_0120 SDetectorNoConnectionTo
2014.08.04 10:57:00,625000 CommERRO_0014 SignalDataFlowError
2014.08.04 11:03:56,484375 CommERRO_0011 NoSignalReceived DEMO
2014.08.13 17:30:01,968750 CommERRO_0011 NoSignalReceived DEMO
2014.08.20 13:00:51,062500 CommERRO_0011 NoSignalReceived DEMO
2014.08.20 13:02:31,328125 CommERRO_0011 NoSignalReceived DEMO
2014.08.20 14:10:32,937500 CommERRO_0120 SDetectorNoConnectionTo
2014.08.20 14:10:34,562500 CommERRO_0110 NDetectorNoConnectionTo
2014.08.20 14:17:42,437500 CommERRO_0120 SDetectorNoConnectionTo
2014.08.21 12:24:58,046875 CommERRO_0050 FirmwareReset T0813042315
2014.08.21 12:38:25,343750 CommERRO_0275 AutoInjectorNoSyringe
2014.08.21 15:53:16,328125 CommERRO_0011 NoSignalReceived DEMO
2014.08.21 15:53:24,640625 SerialCommunication.Read.TimeoutException ?
2014.08.21 15:53:25,343750 CommERRO_0011 NoSignalReceived VERS
2014.08.22 08:15:40,046875 CommERRO_0105 CDetectorWrongType
2014.08.29 15:57:07,906250 SerialCommunication.Read.TimeoutException ?
2014.08.29 15:57:47,109375 CommERRO_0067 MTXTMissing
2014.09.01 15:20:07,250000 CommERRO_0014 SignalDataFlowError
2014.09.02 09:21:07,140625 CommERRO_0050 FirmwareReset T0813042315
2014.09.03 15:18:57,890625 CommERRO_0011 NoSignalReceived DEMO
2014.09.03 15:19:34,687500 CommERRO_0050 FirmwareReset T0813042315
2014.09.04 10:42:45,718750 CommERRO_0050 FirmwareReset T0813042315
2014.09.04 11:00:33,609375 CommERRO_0250 LPGNoConnection
2014.09.04 11:04:48,468750 CommERRO_0133 ClDetectorWrongCell

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12.2.3.3 <multiWin_Comm.log>
[System]
OSName = Windows XP; Microsoft Windows NT 5.1.2600 Service Pack 2
CPU = x86 Family 6 Model 15 Stepping 13; Intel(R) Pentium(R) Dual CPU E2200 @ 2.20GHz;
2194MHz
.NET runtime version: v2.0.50727

[Application]
multiWin = 5.3.5.0

[Device]
SerialNumber = N7-212/L
Firmware = T0813042315
ProtocolId = 8

[Detail]
2014.09.04 10:42:45,703125 > 1*15*ERRO*50*T0813042315*079
2014.09.04 10:42:45,718750 CommERRO_0050 FirmwareReset T0813042315
2014.09.04 10:42:58,203125 < 16*DEMO*1*0*005
2014.09.04 10:42:58,296875 > 2*16*DEMO*0*006
2014.09.04 10:42:58,296875 < 5*VERS*1*ee5b6ef1-8ddc-4b3d-bd93-
e1c4e6367751*0*088
2014.09.04 10:42:58,531250 > 3*5*VERS*1*T0813042315*0*074
2014.09.04 10:42:58,531250 < 0*INIT*0*7*15*7*0*2*028
2014.09.04 10:42:58,906250 > 4*0*INIT*0*0*052
2014.09.04 10:43:00,546875 > 5*0*INIT*0*0*053
2014.09.04 10:43:00,687500 > 6*0*INIT*0*0*054
2014.09.04 10:43:03,390625 > 7*0*INIT*0*0*055
2014.09.04 10:43:10,484375 > 8*0*INIT*0*0*056
2014.09.04 10:43:10,703125 > 9*0*INIT*0*0*057
2014.09.04 10:43:14,375000 > 10*0*INIT*0*0*001
2014.09.04 10:43:20,562500 > 11*0*INIT*0*0*000
2014.09.04 10:43:22,500000 > 12*0*INIT*0*0*003
2014.09.04 10:43:23,703125 > 13*0*INIT*0*0*002
2014.09.04 10:43:24,921875 > 14*0*INIT*0*0*005
2014.09.04 10:43:26,109375 > 15*0*INIT*0*0*004
2014.09.04 10:43:27,328125 > 16*0*INIT*0*0*007
2014.09.04 10:43:28,531250 > 17*0*INIT*0*0*006
2014.09.04 10:43:30,484375 > 18*0*INIT*0*0*009
2014.09.04 10:43:33,453125 > 19*0*INIT*0*0*008
2014.09.04 10:43:34,656250 > 20*0*INIT*0*0*002
2014.09.04 10:43:35,875000 > 21*0*INIT*0*0*003
2014.09.04 10:43:37,078125 > 22*0*INIT*0*0*000
2014.09.04 10:43:38,296875 > 23*0*INIT*0*0*001
2014.09.04 10:43:39,500000 > 24*0*INIT*0*0*006
2014.09.04 10:43:40,046875 > 25*0*INIT*0*0*007
2014.09.04 10:43:41,031250 > 26*0*INIT*0*0*004
2014.09.04 10:43:41,578125 > 27*0*INIT*0*0*005
2014.09.04 10:43:42,203125 > 28*0*INIT*0*0*010
2014.09.04 10:43:42,250000 > 29*0*INIT*0*0*011
2014.09.04 10:43:42,906250 > 30*0*INIT*0*1*0*16*32*1*0*144*64*52*100*0*000
2014.09.04 10:43:43,000000 < 0*INIT*1*049
2014.09.04 10:43:43,703125 > 31*0*INIT*1*0*003
2014.09.04 10:43:45,359375 > 32*0*INIT*1*0*000

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2014.09.04 10:43:45,468750 > 33*0*INIT*1*0*001
2014.09.04 10:43:46,609375 > 34*0*INIT*1*0*006
2014.09.04 10:43:46,656250 > 35*0*INIT*1*0*007
2014.09.04 10:43:46,921875 > 36*0*INIT*1*0*004
2014.09.04 10:43:50,578125 > 37*0*INIT*1*0*005
2014.09.04 10:43:54,500000 > 38*0*INIT*1*0*010
2014.09.04 10:43:56,437500 > 39*0*INIT*1*0*011
2014.09.04 10:43:57,625000 > 40*0*INIT*1*0*005
2014.09.04 10:43:58,843750 > 41*0*INIT*1*0*004
2014.09.04 10:44:00,046875 > 42*0*INIT*1*0*007
2014.09.04 10:44:01,265625 > 43*0*INIT*1*0*006
2014.09.04 10:44:02,468750 > 44*0*INIT*1*0*001
2014.09.04 10:44:04,406250 > 45*0*INIT*1*0*000
2014.09.04 10:44:07,375000 > 46*0*INIT*1*0*003
2014.09.04 10:44:08,593750 > 47*0*INIT*1*0*002
2014.09.04 10:44:09,781250 > 48*0*INIT*1*0*013
2014.09.04 10:44:11,000000 > 49*0*INIT*1*0*012
2014.09.04 10:44:12,203125 > 50*0*INIT*1*0*004
2014.09.04 10:44:13,437500 > 51*0*INIT*1*0*005
2014.09.04 10:44:13,984375 > 52*0*INIT*1*0*006
2014.09.04 10:44:14,421875 > 53*0*INIT*1*0*007
2014.09.04 10:44:14,890625 > 54*0*INIT*1*0*000
2014.09.04 10:44:14,937500 > 55*0*INIT*1*0*001
2014.09.04 10:44:15,046875 > 56*0*INIT*1*1*0*16*32*1*0*144*64*52*100*0*001

2014.09.04 10:44:24,562500 < 1*STAT*1*056

2014.09.04 10:44:24,640625 > 88*1*STAT*1*018
2014.09.04 10:44:24,734375 > 89*1*STAT*1*#*0*32*32*32*0*0*0*0*0*0*0*0*043
2014.09.04 10:44:25,140625 > 90*1*STAT*1*#*0*32*32*32*0*0*0*0*0*0*0*0*035
2014.09.04 10:44:25,640625 > 91*1*STAT*1*#*0*32*32*32*42*0*0*0*0*0*0*0*020
2014.09.04 10:44:25,640625 < 10*SETV*10*100*200*100*600*3*0*057
2014.09.04 10:44:25,843750 > 92*10*SETV*0*046
2014.09.04 10:44:26,140625 > 93*1*STAT*1*#*1280*32*32*32*42*0*0*0*0*0*0*0*045
2014.09.04 10:44:26,140625 < 10*SETV*8*0*1050*051
2014.09.04 10:44:26,281250 > 94*10*SETV*0*040
2014.09.04 10:44:26,281250 < 0*INIT*4*052
2014.09.04 10:44:26,734375 > 95*0*INIT*4*1*1*018
2014.09.04 10:44:26,765625 < 0*INIT*5*053
2014.09.04 10:44:27,218750 > 96*0*INIT*5*1*250*022
2014.09.04 10:44:27,250000 < 17*HINT*1*006
2014.09.04 10:44:27,718750 > 97*17*HINT*1*0*0*034
2014.09.04 10:44:28,140625 > 98*1*STAT*1*#*1280*32*32*32*42*0*0*0*0*0*0*0*038
2014.09.04 10:44:28,140625 < 10*SETV*9*1*10*054
2014.09.04 10:44:28,296875 > 99*10*SETV*0*037
2014.09.04 10:44:28,656250 > 1*1*STAT*1*#*1280*32*32*32*42*0*0*0*0*0*0*0*022
2014.09.04 10:44:29,140625 > 2*1*STAT*1*#*1280*32*32*32*42*0*0*0*0*0*0*0*021
2014.09.04 10:44:29,640625 > 3*1*STAT*1*#*1280*32*32*32*42*0*0*0*0*0*0*0*020
2014.09.04 10:44:30,140625 > 4*1*STAT*1*#*1280*32*32*32*42*0*0*0*0*0*0*0*019
2014.09.04 10:44:30,656250 > 5*1*STAT*1*#*1280*32*32*32*42*0*0*0*0*0*0*0*018
2014.09.04 10:44:31,140625 > 6*1*STAT*1*#*1280*32*32*32*42*0*0*0*0*0*0*0*017
2014.09.04 10:44:31,640625 > 7*1*STAT*1*#*1280*32*32*32*42*0*0*0*0*0*0*0*016
2014.09.04 10:44:32,140625 > 8*1*STAT*1*#*1280*32*32*32*42*0*0*0*0*0*0*0*031

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12.3 Error messages

Error message
Firmware sends error

Error message 1…. 50 sent by by multiWin

Error message 60…. 420 sent by by firmware controller

1 Communication error: no reply from firmware!

2 Communication error: Serial port not present!
3 Communication error: Serial port not reachable!
4 Communication error: Unknown connection type!
5 Communication error: Error when opening the port!
6 Communication error: Named Pipe Server not found!
7 Communication error: Operating system error: Unauthorized access!
8 Communication error: Error when reading from the port!
9 Communication error: Error when writing to the port!

11 no reply to signal
12 Signal echo received, check port selection
13 CRC error
14 Data transfer interrupted
15 unknown protocol structure
16 Firmware command missing
17 incorrect interface protocol ID

20 Timeout InitEnd
21 Timeout StatusBusy
22 Timeout End
23 Timeout StopEnd

50 Firmware reset

61 Command from the PC not complete

62 Command from the PC without STX
63 Command from the PC no * available
64 Command from the PC CRC error
65 Command from the PC invalid command
66 Command from the PC invalid MESS command

100 C sensor: no connection

101 C sensor: CRC error
102 C sensor: Status error
104 C sensor: Analog values out of range
105 C sensor: incorrect type
106 C sensor: incorrect command reply
107 C sensor: Analog values out of range (coarse)

110 N sensor: no connection

111 N sensor: Error ozone on/off

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 120 S sensor: no connection

130 Cl sensor: no connection

131 Cl sensor: incorrect command structure
132 Cl sensor: indication error
133 Cl sensor: incorrect cell
134 Cl sensor: incorrect status
135 Cl sensor: incorrect version

200 Gas box: no connection

201 Gas box: Error when setting target flow
202 Gas box: Conversion error 1
203 Gas box: Conversion error 2
204 Gas box: Conversion error 3
205 Gas box: Conversion error 4
206 Gas pressure error
207 Flow error
208 O2 pressure missing
209 Argon pressure missing

210 Rotary valve time error

211 Error lock furnace
212 Error lock TIC reactor

220 Sampler: no connection

221 Boat: Length measurement error
222 Boat: broken
223 Sampler: incorrect syringe size
224 Sampler: incorrect gripper
225 Sampler: Position not reached
226 Sampler: runtime exceeded

230 ABD: no connection

231 ABD: runtime exceeded
232 Flame sensor error

240 GSS: no connection

241 GSS: runtime exceeded
242 GSS: busy

250 LPG: no connection

251 LPG: runtime exceeded
252 LPG: Argon missing when dosing
253 LPG: incorrect sample volume

260 Sample Handling missing

270 Auto-injector - syringe: no connection

271 Auto-injector - syringe: runtime exceeded
272 Auto-injector - syringe: incorrect size
273 Auto-injector - syringe: not properly mounted

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 274 Auto-injector: no connection

300 Temperature controller: no connection

301 Thermocouple fracture / UV cover open
302 Housing temperature exceeded
303 Temperature controller: EEPROM error
304 Temperature controller: Communication error
305 Temperature controller: Version error
306 external furnace: not present
307 Temperature control faulty
308 Pre-furnace: no connection

400 Syringe pump: no connection

401 Syringe pump: Initialization
402 Syringe pump: invalid command
403 Syringe pump: invalid operand
404 Syringe pump: invalid command sequence
407 Syringe pump: device not initialized
409 Syringe pump: pump sluggish
410 Syringe pump: valve sluggish
411 Syringe pump: pump step prohibited
415 Syringe pump: command error
420 Syringe pump: incorrect type

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13 Consumables
Please download the current spare parts list from our service chapter in EXTRANET:

https://extranet.analytik-jena.com/

14 Spare parts
Please download the current spare parts list from our service chapter in EXTRANET:

https://extranet.analytik-jena.com/

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15 Recommended tools and measuring instruments
order no. description device/detector link / contact
800-001-00009 thermometer RS1313 main unit [email protected]

temperature sensor type K (diameter <

702-823.145 1.5mm;length >25cm) main unit [email protected]

Flowmeter Analyt GFM17 (calibrated for

800-001-00002 O² ; 0….1000ml/min) main unit [email protected]

Flowmeter Analyt GFM17 (calibrated for

800-001-00004 Ar ; 0….500ml/min) main unit [email protected]

800-003-00006 manometer 0...2.5bar main unit [email protected]

800-003-00008 manometer 0...6.0bar main unit [email protected]

121552-62 manometer GDH 200-13 main unit www.conrad.com/ce/en/

service program main unit [email protected]

702-823.146 short circuit connector main unit [email protected]

402-889.652 extended tool set (service) for leakage test main unit [email protected]

702-890.030 gas detector "sniffer" LPG-module [email protected]

702-889.445 tool set LPG/GSS complete LPG-module [email protected]

[spanner, three-square-wrench(inside),
tool for dosing valve]

800-003-00014 Tool-kit Cl-module Cl-module [email protected]

Communication cable for NDIR-Optic

702-011.059 (RS323-socket 10pin)>>test-NDIR main unit [email protected]

communication cable for NDIR-Optic

702-890.607 (RS323-plug10pin)>>simulation-NDIR TOC/TC-module [email protected]

702-808.359 Null-modem cable main unit [email protected]

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16 Contact

Analytik Jena AG
Konrad-Zuse-Straße 1
07745 Jena/ Germany

Application: Phone: +49 (0)36 41 – 77 72 24

Service: Phone: +49 (0)36 41 – 77 74 02

Fax: +49 (0)36 41 – 77 74 49
E-mail: [email protected]

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