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DSC Instrument

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0% found this document useful (0 votes)
143 views16 pages

DSC Instrument

Uploaded by

Fadhlan Arifin
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

TURN UP THE HEAT ON

THERMAL
ANALYSIS

Pyris™ TGA 9, DSC 9, and STA 9


Next Gen Thermal Analysis Instruments
All The Elements of Thermal Analysis  INTRODUCTION

in Perfect Balance
 WORKFLOW SOLUTIONS

 TGA 9 AND STA 9

 DSC 9
Research scientists and QA/QC analysts need high-resolution data to uncover the
subtle intricacies of material behavior, whether it be raw materials or composites.
They often face the challenge of complex instrumentation and unreliable  HYPHENATION
data. They must also navigate the pressures of rapid, accurate testing cycles
and stringent regulatory requirements, all while ensuring the thermal analysis  SOFTWARE
instruments deliver consistent and reliable results.​

PerkinElmer harnesses 60 years of expertise to transform thermal analysis,  INDUSTRIAL


unveiling the Pyris™ TGA 9, DSC 9, and STA 9 systems: a new generation
of compact, durable, high-resolution, and low-maintenance thermal analysis  PHARMACEUTICALS
systems. Our groundbreaking interchangeable furnace design enhances
versatility, enabling your lab to do more with less. The intuitive touchscreen
 MATERIALS
interface simplifies instrument operation, significantly enhancing productivity.​

With industry-leading temperature control and rapid heating, our instruments  CONSUMABLES
grant superior precision and control. Experience streamlined workflows and
deeper analytical insights with our comprehensive hyphenation solutions, all from
 CONTACT US
a single, trusted source.​

The modular design across the Pyris series ensures ease of troubleshooting and
maintenance, bolstered by a unified electronics module and a single gas system
for operational simplicity and increased reliability. New balance design for lower
gas consumption ensures low maintenance and improved ESG .
Turn Up the Heat on Innovation  INTRODUCTION

With TGA 9 and STA 9  WORKFLOW SOLUTIONS

 TGA 9 AND STA 9

The TGA 9 and STA 9 provide detailed thermogravimetric analysis across an extensive temperature range, ensuring precise quantification and characterization  DSC 9
of samples, raw materials, and composites. Their compact, robust design integrates a durable furnace and a responsive touchscreen, enhancing productivity and
offering outstanding value. The design features an alumina furnace, celebrated for 25 years of reliability, alongside a sensitive balance. The inclusion of a 48 position  HYPHENATION
autosampler revolutionizes your workflow, enabling automated analysis and freeing up valuable time. Enhanced with direct temperature control via a responsive
touchscreen, these systems significantly reduce sensor lag, delivering superior data quality and reliability.​The STA 9 offers differential thermal analysis, enabling
 SOFTWARE
measurement of melting points, glass transitions, alongside gravimetric data.

 INDUSTRIAL

Transition to Better Characterization  PHARMACEUTICALS

With DSC 9  MATERIALS

 CONSUMABLES

The new DSC 9 revolutionizes high-temperature Differential Scanning Calorimetry (DSC) analysis, and offers a dependable, user-friendly DSC system without  CONTACT US
compromising on performance. Engineered to fulfill stringent ASTM standards, including the Oxygen Induction Time (OIT) test, this instrument combines a high-capacity
stainless-steel furnace on a copper base, capable of reaching up to 750°C. This ensures comprehensive analysis and unparalleled insights into a variety of samples. The
DSC 9's compact and robust design integrates enhanced direct temperature control, elevating the quality of DSC analysis. The DSC 9 system delivers exceptional value,
characterized by its ease of maintenance, compliance with ASTM standards, and a durable build designed for prolonged and intensive use.
TGA 9/STA 9  INTRODUCTION

 WORKFLOW SOLUTIONS

Sharing a common design, the compact TGA 9 and STA 9 double thermal analysis capability and deliver all the performance you need.  TGA 9 AND STA 9
The innovative STA 9 provides real-time sample weight and heat flow measurements, ideal for both research and routine tasks. Its
advanced sensor technology and compact design make it perfect for characterizing inorganics, analyzing polymers, or testing oils.  DSC 9

 HYPHENATION

Robust Intuitive Interchangeable Unattended Sensitive  SOFTWARE


Furnace Touchscreen Furnace Operation Balance

Start and stop the


 INDUSTRIAL
Robust and compact Modular design with 48-position Highly sensitive
furnace that gives instrument along with interchangeable autosampler for single top-loading balance
you improved other basic control furnaces between sample autoloading or for unmatched  PHARMACEUTICALS
temperature functions, right TGA and STA for overnight multiple performance, easy
control, fast heating from the responsive instruments offers sample analysis. sample loading and  MATERIALS
and cool-down touchscreen on the great flexibility and unloading.
time, and precise instrument. versatility for budget-
 CONSUMABLES
measurements. constrained labs.

 CONTACT US
STA 9  INTRODUCTION

 WORKFLOW SOLUTIONS

With the power to acquire both TGA and DSC measurements simultaneously, the compact instrument delivers high performance thermal  TGA 9 AND STA 9
analysis across the widest range of applications. From compositional analysis to kinetic studies, the STA 9 is a real laboratory workhorse,
enabling high temperature thermal analysis for fuel cell, ceramics, catalysis applications and challenging academic research.  DSC 9
The STA 9 is equipped with our leading edge SaTurnA™ sensor technology, which measures both sample and reference temperatures to
ensure high precision and accuracy.  HYPHENATION

 SOFTWARE

From TGA From DSC  INDUSTRIAL


g Compositional analysis – quantitative content analysis g Melting/crystallization behavior
 PHARMACEUTICALS
g Decomposition temperatures g Glass transition temperatures
g Engine oil volatility measurements (TGA Noack test) g Transition and reaction enthalpies
 MATERIALS
g Filler content
g Flammability studies  CONSUMABLES
g Lifetime predictions (via TGA kinetics software)
g Measurement of volatiles (e.g. water, oil)  CONTACT US
g Oxidative stabilities
g Thermal stabilities
g Catalyst and coking studies
g Hyphenation to identify products
TGA 9/STA 9 Furnace Assembly  INTRODUCTION

 WORKFLOW SOLUTIONS

 TGA 9 AND STA 9

 DSC 9
TGA/STA Cell

 HYPHENATION

 SOFTWARE

Housing
 INDUSTRIAL

 PHARMACEUTICALS

Electronics
 MATERIALS

 CONSUMABLES

 CONTACT US

Improved Air Tightness


Improved sealing between subassemblies Balance
TGA 9 Assembly STA 9 Assembly  INTRODUCTION

 WORKFLOW SOLUTIONS

 TGA 9 AND STA 9

Alumina furnace, 25 years of Alumina furnace, 25 years of STA SaturnA™ metal sensor,  DSC 9
proven reliability proven reliability both sample and reference
TGA sensor position in one  HYPHENATION
Extended temperature range Extended temperature range
15 °C to 1100 °C 20 °C to 1100 °C  SOFTWARE

 INDUSTRIAL

 PHARMACEUTICALS

 MATERIALS

 CONSUMABLES

 CONTACT US
DSC 9  INTRODUCTION

 WORKFLOW SOLUTIONS

The new DSC 9 is a robust and compact workhorse that performs like a champion. It’s the single-furnace solution you can depend on for a wide  TGA 9 AND STA 9
range of routine and traditional materials characterization research applications in the academic, polymer and pharmaceutical markets.
 DSC 9

 HYPHENATION

New Furnace Meet ASTM Increased Unattended Direct Temperature  SOFTWARE


Design Standards Temperature Range Operation Control
 INDUSTRIAL
Robust and compact Precise measurement Best-in-class heating 48-position More accurate control
furnace that gives of parameters like and ramping up to autosampler for single and measurement
you improved melting points, 750 °C for analysis of sample autoloading or of both furnace and  PHARMACEUTICALS
temperature thermal stability, and diverse samples. for overnight multiple sample temperature,
control and precise purity essential for sample analysis. giving you greater  MATERIALS
measurements. meeting rigorous confidence in results.
quality and safety
 CONSUMABLES
criteria.

 CONTACT US
DSC 9 Furnace Assembly  INTRODUCTION

 WORKFLOW SOLUTIONS

 TGA 9 AND STA 9

DSC 9 cell Cell electronics Stainless steel on New temperature sensor  DSC 9
Extended temperature range Calibrations and corrections a copper base Direct temperature control
-180 °C to 750 °C stored on measuring cell PCB  HYPHENATION
For easier cell replacement

 SOFTWARE

 INDUSTRIAL

 PHARMACEUTICALS

 MATERIALS

 CONSUMABLES

 CONTACT US
Go Further With the Power of Hyphenation  INTRODUCTION

 WORKFLOW SOLUTIONS

Accelerate your research with the PerkinElmer Hyphenation System, a modular, multimodal TGA, IR, and GC/MS solution managed by an electronic  TGA 9 AND STA 9
control panel, enabling complete sample characterization with minimal sample prep. With its automation features and functionality, your research
can benefit from greater efficiencies and lower maintenance costs. And it delivers sample information and insights that can provide a real  DSC 9
competitive advantage that is simply not available with single-system analyses. And you can rely on a single partner, every step of the way – from
installation to application support. Learn about our rich history in hyphenation below.
 HYPHENATION

1980 1990 2000 2010 2020  SOFTWARE

Thermal
 INDUSTRIAL
TGA 7 PYRIS 1 TGA 4000/STA 6000 TGA 8000 TL Series EGA 4000
Introduced the first The first TGA with TGA 4000: Temperature control Designed for New controller First single-supplier,
hyphenation-ready anticonvention for accurate results, fast sample hyphenation with and transfer lines fully integrated TG-IR
 PHARMACEUTICALS
thermal system – tubing and long- purge and cooldown autosampler for hyphenation – winner of the R&D
built-in multitasking lasting glassware STA 6000: Simultaneous thermal World 100 Award
computer
 MATERIALS
performance, reliability, and productivity

Infrared  CONSUMABLES
1700 FTIR Spectrum GX Spectrum™ One Spectrum 100 Spectrum 400 Spectrum Two Frontier Spectrum 3
Spectrometer FTIR FTIR FTIR FTIR FTIR FTIR FTIR  CONTACT US
First With first-ever With patented DynaScan Incorporated smart First with First portable, low- High-performance Tri-range
microprocessor- validated FTIR interferometer, the first accessories for automated phase maintenance FTIR FTIR/FT-NIR system with
controlled FTIR, software, FTIR with smart accessory efficient analysis switching for everyday use for high-demand top fast-scan
with rotating Spectrum for recognition and validated of a wide range of – with application environments performance
mirror-pair design Windows® FTIR software (Spectrum samples packs and
for Windows®) powerful software

Gas Chromatography

AutoSystem™ XL GC with Clarus GC/MS GCMS 2400™ Platform


TurboMass™ Software Perfect combination of high-performance Innovative platform combined with
GC with precise induction interfaced GC and mass spec software detachable touchscreen and smart
with quadrupole benchtop MS sampling capabilities
Powerful and Intuitive Software  INTRODUCTION

 WORKFLOW SOLUTIONS

Your PerkinElmer thermal analysis instruments and data come to life on the Pyris™ software platform – the benchmark application for thermal analysis.  TGA 9 AND STA 9
Pyris is the preferred choice in thermal analysis because it is intuitive and user-friendly and provides a wide-range of standard features and capabilities for
maximum flexibility. PerkinElmer’s family of highly sensitive thermal analysis instruments have been standardized on this powerful software platform.  DSC 9
Pyris software is easy to use without losing capabilities. The software has been designed to allow you to conduct data acquisition and analysis in one window
and run multiple analyzers simultaneously.  HYPHENATION

A wide range of analysis options, data import/export flexibility and customizable features are provided to meet a wide range of needs.
 SOFTWARE

The new Pyris Touch software powered by an Android touchscreen  INDUSTRIAL


enables basic contorls of the instrument such as:

g Start & Stop the instrument  PHARMACEUTICALS

g Extend temperature
 MATERIALS
g Control autosampler

 CONSUMABLES

 CONTACT US
Industrial  INTRODUCTION

 WORKFLOW SOLUTIONS

 TGA 9 AND STA 9

UV Curving of Polymers Analysis of Recycled Polymers Oxidative Induction Testing


 DSC 9
The DSC 9, paired with a UV light source, The PerkinElmer TGA 9 efficiently OIT measures the oxidative stability of
enables precise measurement of curing measures properties like degradation polymers, indicating how well they resist  HYPHENATION
temperatures and calorimetric data for temperature, moisture, and ash content aging due to environmental factors like
resins under controlled temperature in polymers. For parameters like melting heat and oxygen. Antioxidants are added
 SOFTWARE
and light conditions. This aids in point, the STA 9 delivers simultaneous to plastics to slow this aging process.
optimizing photo-initiator concentration weight loss and heat flow data. For The exothermic reaction between
and processing parameters for product precise calorimetric values and thermal polymers and oxygen makes DSC an  INDUSTRIAL
development and scale-up. transitions, such as glass transition ideal method for such studies.
temperature and curing temperature,  PHARMACEUTICALS
the DSC 9 offers a high-performance
workflow.
 MATERIALS

 CONSUMABLES

 CONTACT US
Pharmaceuticals  INTRODUCTION

 WORKFLOW SOLUTIONS

 TGA 9 AND STA 9

Free and Bound Solvent/Water Weight Loss on Drying Thermal Degradation


 DSC 9
Thermogravimetric analysis with Weight loss on drying is a key parameter A key aspect of the characterization
the PerkinElmer TGA 9 is crucial for of pharmaceutical formulations. of pharmaceutical ingredients is the  HYPHENATION
determining free and bound solvents Thermogravimetric analysis allows for degradation temperature which can be
or water in pharmaceuticals, offering optimization of pharmaceutical drying determined under different conditions
 SOFTWARE
insights into formulations through its by allowing users to employ a variety of using the PerkinElmer TGA 9.
high sensitivity. heating rates and isothermal holds while
measuring the weight of the sample  INDUSTRIAL
under a different purge atmospheric
conditions.  PHARMACEUTICALS

 MATERIALS

 CONSUMABLES

 CONTACT US
Materials  INTRODUCTION

 WORKFLOW SOLUTIONS

 TGA 9 AND STA 9

Ceramic Geological Construction


 DSC 9
Porcelain clay, used for products like TGA and STA analyses are used Inorganic cement's strength varies with
sinks and ceramics, contains kaolin, to characterize geologic materials its mix and setting conditions. The STA 9  HYPHENATION
feldspar, and silica. The STA 9 measures by simultaneously measuring heat effectively characterizes the hydrate and
moisture and kaolin content via weight and weight changes, preventing carbonate mix from setting. Past failures,
 SOFTWARE
changes, and heat flow data to misinterpretation. These methods like the 1960s high alumina cement
determine the structure of the final identify water loss from hydrates collapse, show the importance of proper
product by analyzing reaction or and CO2 from carbonates, and testing. STA technology offers quick,  INDUSTRIAL
crystallization products. characterize chemical reactions in reliable analysis of cement's safety by
various atmospheres through emitted or measuring both weight loss and  PHARMACEUTICALS
absorbed heat and weight changes. heat flow.

 MATERIALS

 CONSUMABLES

 CONTACT US
Precision Engineered Consumables  INTRODUCTION

 WORKFLOW SOLUTIONS

The consumables for our latest range of thermal analysis instruments are designed with you in mind, with each fit to perform and  TGA 9 AND STA 9
manufactured with the highest quality materials available.

Whether you’re looking for sample introduction components or standards, we have the consumables you need to keep your instrument up
 DSC 9
and running smoothly and efficiently.
 HYPHENATION

 SOFTWARE

 INDUSTRIAL

 PHARMACEUTICALS

 MATERIALS

 CONSUMABLES

 CONTACT US

Click here to explore our Thermal Analysis Consumables


For more information visit www.perkinelmer.com

PerkinElmer U.S. LLC


710 Bridgeport Ave.
Shelton, CT 06484-4794 USA
(+1) 855-726-9377
www.perkinelmer.com

For a complete listing of our global offices, visit www.perkinelmer.com/ContactUs

Copyright ©2024, PerkinElmer U.S. LLC. All rights reserved. PerkinElmer® is a registered trademark of PerkinElmer U.S. LLC. All other trademarks are the property of their respective owners.

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