GAS CHROMATOGRAPH

GC47A Ver.2
SERVICE MANUAL
 221-30108

GC-17A Ver. 2
SERVICE MANUAL

SHIMADZU CORPORATION
ANALYTICAL INSTRUMENTS DIVISION
KYOTO, JAPAN
Copyright 0 Shimadzu Corporation 1995. All rights are reserved, including those to
reproduce this publication or parts there of in any form without permission in writing from
Shimadzu Corporation.
Information in this publication is subject to change without notice and does not represent
a commitment on the part of the vendor.
Any errors or omissions which may have occurred in this publication despite the utmost
care taken in its production will be corrected as soon as possible, but not necessarily im-
mediately upon detection.
Shimadzu Corporation will continue to supply original Shimadzu maintenance parts associat-
ed with a given product for a period up to 10 years from the cessation of production of that
product. Please be informed that after this period of time, Shimadzu Corporation cannot guar-
antee supply of such original maintenance parts. However, following discontinuation of a
product, the period of availability of maintenance parts which have been produced on a sub-
contract basis is up to the discretion of the concerned sub-contracting company.
Chapter 1 GG17A Ver. 2 Series .................................................................... I-1
1.1 Configuration of GC-17A Ver.2 Series .............................................................. l-2
1.2 Accessories of GC-17A Ver.2 ............................................................................ l-3

Chapter 2 GC-17AA Ver.2.. .............................................................................. 2-l

2.1 Configuration of GC- 17AA Ver.2 ...................................................................... 2-2
2.2 Configuration of GC-17AA Ver.2.. .................................................................... 2-4
2.2.1 Configuration of GC-17AA Ver.2.. .......................................................... 2-4
2.2.2 Configuration of oven cooling unit.. ........................................................ 2-7
2.3 Electric Circuit of GC-17A Ver.2.. ..................................................................... 2-8
2.3.1 GC base unit.. ........................................................................................... 2-8
2.3.2 Power unit.. .............................................................................................. 2-15
2.3.3 Key unit.. .................................................................................................. 2-17
2.3.4 Aux temperature control unit.. ................................................................. 2-19

Chapter 3 Gas Flow Controller ...................................................................... 3-l

3.1 AFC (Advanced Flow Controller) Ver.2 ........................................................... 3-2
3.1.1 Configuration of AFC Ver.2.. ................................................................... 3-2
3.1.2 Flow line AFC Ver.2 ................................................................................ 3-3
3.1.3 Electric circuit of AFC Ver.2 ................................................................... 3-5
3.2 Flow controller make-up 17A Ver.2 .................................................................. 3-6
3.3 Additional manual flow controller Ver.2 ........................................................... 3-7
3.4 APC (Advanced Presser Controller) Ver.2 ........................................................ 3-9

Chapter 4 injection Unit .................................................................................. 4-l

4.1 SPL-17 Ver. 3...................................................................................................... 4-2
4.1.1 SPL- 17 Ver.2 configuration ..................................................................... 4-2
4.1.2 SPL- 17 Vet2 configuration ..................................................................... 4-3
4.2 WBI-17 Ver. 2 .................................................................................................... 4-5
4.2. I WBI- 17 Ver.2 configuration .................................................................... 4-5
4.2.2 WBI-17 Ver.2 configuration .................................................................... 4-5
4.2.3 WBI-17 Ver.2 flow line ............................................................................ 4-6
4.3 OCI-17 Ver.2 ...................................................................................................... 4-7
4.3.1 OCI- 17 Ver.2 configuration ..................................................................... 4-7
4.3.2 OCI- 17 Ver.2 configuration ..................................................................... 4-8
4.4 SPWWBI flow line select unit 17A Ver.2 .......................................................... 4-9
4.4.1 Configuration of SPWWBI select unit 17A Ver.2 ................................... 4-9
4.4.2 Flow line of SPWWBI select unit 17A Ver.2.. ......................................... 4-9
Chapter 5 Detector Unit.. ................................................................................. 5-1
5.1 WFID-17 Ver.2/FID-17 Ver.2 unit ..................................................................... 5-2
5.1.1 WFID-17 Ver.2 configuration.. ................................................................ 5-2
5.1.2 WFID-17 Ver.2/FID-17 Ver.2 configuration.. .......................................... 5-4
5.1.3 WFID-17 Ver.2/FID-17 Ver.2 Hz, Air flow line.. ..................................... 5-6
5.1.4 Electric circuit of WFID-17 Ver.2 controller.. ......................................... 5-7
5.1.5 Electric circuit of WFID- 17 Ver.2 controller ........................................... 5-10
5.2 TCD-17 Ver.2 unit .............................................................................................. 5-13
5.2.1 TCD- 17 Ver.2 configuration .................................................................... 5-13
5.2.2 TCD- 17 Ver.2 configuration .................................................................... 5-14
5.2.3 Electric circuit of TCD-I 7 Ver.2 controller control.. ............................... 5- 17
5.3 FPD-17 Ver.2 unit ............................................................................................... 5-20
5.3.1 FPD-17 Ver.2 configuration ..................................................................... 5-20
5.3.2 PD-17 Ver.2 configuration ....................................................................... 5-21
5.3.3 Hz, air flow line of FFD-17 Ver.2 ............................................................ 5-22
5.3.4 Electrical system of FPD- 17 .................................................................... 5-23
5.4 ECD-17 Ver.2 unit .............................................................................................. 5-28
5.4.1 ECD- 17 Ver.2 configuration .................................................................... 5-28
5.4.2 ECD- 17 Ver.2 configuration .................................................................... 5-29
5.4.3 Electric circuit of ECD-17 Vet2 controller control.. ............................... 5-30
5.5 FTD-17 Ver.2 unit ............................................................................................. 5-34
5.5.1 FTD-17 Ver.2 configuration.. ................................................................... 5-34
5.5.2 FTD-17 Ver.2 configuration ..................................................................... 5-35
5.5.3 Flow line of FTD-17 Ver. 2 resister tube unit.. ........................................ 5-36
5.5.4 Electric circuit of FTD-17 Vet2 power controller.. ................................. 5-37

Chapter 6 Appendix .......................................................................................... 6-l

6.1 Maintenance parts list ........................................................................................ 6-2
6.2 Special key operations ........................................................................................ 6-4
6.3 GC generai ......................................................................................................... 6-7
6.3.1 Maintenance precautions ......................................................................... 6-7
6.3.2 Replacing restrictor and septum .............................................................. 6-8
6.3.3 Inspection of molecular sieve filter ......................................................... 6-9
6.3.4 Inspection of compressor and silica gal ................................................... 6-10
6.3.5 Injection port septum ............................................................................... 6-l 1
6.4 Temperature sensor ............................................................................................ 6-14
6.5 CA Thermocouple.. ............................................................................................ 6-15
6.6 Linear velocity and flow rate ............................................................................. 6-16
This manual describes the functions, configuration, inspection methods and
maintenance parts of the Gas Chromatograph GC-17A Ver.2 series model. Users
are recommended to refer to this manual for the troubleshooting, repair, daily
maintenance and inspection procedures of the Gas Chromatograph GC- 17A Ver.2
series equipment.
This manual does not contain operating instructions. Therafore, it is
recommended to refer to the operation manuals of the GC-17A Ver.2 and
information processor together with this manual. Due to changes in specifications
and upgrading of the equipment, the contents and diagrams of this manual is
slightly inconsistent with the equipment that is actually delivered to users. The
contents of this manual are also subject to change without notice.
 Chapter 1 GG17A Ver. 2 Series

j CONTENTS 1 1.1 Configuration of GC-17A Ver.2 Series.. ........................................ l-2

1.2 Accessories of GC-17A Ver.2.. ...................................................... l-3

l-l
GC-17A Ver.2 SERVICE MANUAL m
1 GC-17A Ver. 2 1
GC-17AA Ver.2 without _ GC- 17AA V2 common part GC- 17AAT V2 GC- 17AA V2 common part
DET 221-44087-91 221-43799-91 221-44087-91
221-43825-91 -92 -92 -92
-92 -93 -93 -93
-93 -94 -94 -94
-94 -96 -96 -96
-96
GC- 17A V2 accessory TCD-17 V2
221-43312-91 22 l-42474-9 1
-92
GC- 17A V2 assembly parts -93
221-43693-91
GC- 17A V2 accessory
Flow controller make-up 221-43312-91
221-43329-91
GC-17A V2 assembly parts
22 l-43693-9 1
Flow controller make-uu
221-43329-91 L

GC-17AAF V2 GC- 17AA V2 common uart GC-17AA TF V2 - - GC- 17AA V2 common part
221-43305-91 221-44087-91 221-43810-91 221-44087-91
-92 I -92 -92 -92
-93 -93 -93 -93
-94 -94 -94 -94
-96 -96 -96 -96
FID-17 V2 linear - TCD-17 V2
221-43310-91 22 l-42474-9 1
-92 -92
-93 -93
-94
- Fid- 17 V2 linear
GC-17A V2 acessory ASSY 221-43310-91
221-43312-91 -92
GC-17A V2 assembly parts -93
221-43693-91 -94

Flow controller make-up - GC- 17A V2 accessory parts

221-43329-9 1 221-43312-91
- GC-17A V2 assembly parts
221-43693-91
- Flow controller make-up
221-43329-91
- Additional piping, TCD- 17
221-42713-91

GC-17AA FW V2 GC- 17AA V2 common part GC-1’7AATFWV2 - - GC- 17AA V2 common part
221-43304-91 221-44087-91 221-43809-91 T 221-44087-91
-92 -92 -92 -92
-93 -93 -93 -93
-94 -94 -94 -94
-96 -96 -96 -96
GC-17A V2 wide-range controller - TCD-17V2
221-43311-91 221-42474-91
-92 -92
-93 -93
-94 - FID-17 V2 wide-range controller
GC-17A V2 accessory Assy 221-43311-91
221-43312-91 -92
-93
GC-17A V2 assembly psrts -94
221-43693-91
> - GC- 17A V2 accessory Assy
Flow controller make-up 221-43312-91
221-43329-91
-91 1OOV type - GC-17A V2 assembly parts
221-43693-91
-92 115V 0
- Flow controller make-up
-93 220v *
221-43329-91
-94240v ” - Additional piping, TCD-17
-96230V * 221-42713-91
Accessories of GC-17A Ver.2 (P/N 221-43312-91)
221-09688-91 Pipe. AIR IN

070-92025-52 Cable, HFBR-3600-2-02

221-l 5563-91 Graphite ferrule packed with 4 pcs. 221-43947-91 Holder capillary column, V2

221-35566-91 Stop joint with ring

221-35566-92 Stop joint with ring
201-35183 Column packing, aluminum
rr ’ \F Cap nut, M5rq.5 ~it~~plit
221-41532-91 Graphite posltlontng 119, SPL
201-35584 Septum INJ with 20 PCS.
221-41451-91 Capillary adaptor, DET
221-41532-92 Graphite positioning jig, FID
\

221-41444 SPL-17 glass Insert 7

221-41544 Glass insert spiit!ess 1 221-43947-91 Holder capillary column, V2
--
221-32126-08 Graphite fenule 0.8 086-03011 Wrench, round type 10x12
086-03003 Wrench, round type 6x8
221-32126-05 Graphite ferrule 0.5

Fig. 1.2 Accessories of GC-17A Ver.2 (P/N 221-43312-91)

GC-17A Ver.2 SERVICE MANUAL m

 Chapter 2 GC47AA Ver.2

1CONTENTS j 2.1 Configuration of GC-17AA Ver.2.. ................................................ 2-2

2.2 Configuration of GC-17AA Ver.2 .................................................. 2-4
2.2.1 Configuration of GC-17AA Ver.2.. ...................................... 2-4
2.2.2 Configuration of oven cooling unit ...................................... 2-7
2.3 Electric Circuit of GC- 17A Ver.2 .................................................. 2-8
2.3.1 GC base unit .........................................................................2-8
2-15
2.3.2 Power unit .............................................................................
2-17
2.3.3 Key unit ................................................................................
2.3.4 Aux temperature control unit ...............................................2- 19

2-1
GC-17A Ver.2 SERVICE MANUAL -
 .
,:j’&-’
‘2 :>C+ Configuration of GC-17AA Ver.2
-.,-__ ..,

GC-17AA V2 common part

CC-17AA V2 GC-17A V2 over Column oven Assy Grounding cable Assy oven
221-43050-91 22 l-4305 1-9 1 221-41623-91
221-44087-91 -92 -92
-93 -93 Bottom plate Assy Power switch Assy
-94 -94 221-43052-91 221-43053-91
-96
Oven inner tank Assy Oven welding plate Assy
221-43054-91 221-43055-91

PT sensor 17A V2 Assy Oven heat insulator frame Assy

221-43695-91 221-43056-g 1

Thermocoupler 17A V2 AssyI Oven heat insulator Assy

22 I-43696-91 22 I -43070-g I

PCBFLOWCOh’T17AV2 Oven cooling unit Assy Flap ASSY

221-43096-91 221-43057-91 221-43058-9 I

Column oven heater unit Assy Flap motor Assy

221-43652-91 (1OOV) 221-43059-91
-92 (115V)
-93 (22OV)
-94 (23OV)
-95 (24OV)

Fan motor Assy Motor unit Assy

221-43061-91 221-43324-91
-92 -92
-93 -93

Oven door Assy - Door heat insulator Assy

221-43062-91 221-43063-91

Oven case Assy

221-43064-91

GC base unit 17A V2 - -r PCB 17A V2 base unit

221-43295-91 221-43ooo-91

DOmmy ignitor Assy

221-41486-91

ROM, GC-17A ‘~2

221-43302-91

Lithium battery CR2032

074-73307-01

Power unit 17A V2 Assy- GC- 17A V2 power supply

22 l-43296-9 1 22 l-43299.,9 1
-92 -93 -91 IOOV type
-93
-94 J 18 dummy transformer -92 115V ”
-96 221-43317-91
-93 220v “
AC cable 17A V2 -94 240v “
221-43318-91
-93 -96 230V 0

PCB, POWER, CONT 17A V2

221-43122-91

% To be continued
 2.1 Configuration of GC-17AA Ver.2

% Key unit r Assy Key display Assy LCD Assy

221-41047-91 22 I-39544-9 1 221-41018-91

CC-17A V2 heater wiring Ass)

221-43297-91

GC-17A V2 Power controller cable

221-43298-91

Control-ralated parts V2 Assy- Dummy connector, temperature control block

221-43314-91 221-41604-91

- Nameplate set 17A V2

221-43313-91
-92
-93
-94
-96

SPL-17 v2
I- 221-42939-91

L
-93

AFC-SPL. piping Assy

221-43233-92 -91 IOOV type

-92 115V fi

-93 220v f/

-94240v *

-96 230V ”

2-3
GC-17A Ver.2 SERVICE MANUAL I
 2.2.1 Configuration of GC47AA Ver.2

221-43602 Upper rear cover

221-43599 INJ/DET cover

\

43601 Controller upper cover

221-43604 Right panel

221-43598 Right cover

221-43062-91 Oven door ASSY 221-41149 Vent cover door

( Mounting direction of cover

Fig.2.2.1-1 Configuration of GC-17AA Ver.2 (1)

2-4
- GC-17A Ver.2 SERVICE MANUAL
 2.2 Configuration of GC-17AA Ver.2

221-43329-91 Flow controller makeup 17A V2

221-42861 Inner oven lid

221-41047-91 Key unit ASSY

i 221-43228-91
, 221-4322%92
TFC ASSY GC-17A
TFC ASSY GC-17A
V2 1 OOV
V2 200V

221-43227-91 Front ASSY 1OOV

221-43227-92 Front ASSY 115V
221-43227-93 Front ASSY 220V
221-43227-94 Front ASSY 240V

Fig. 2.2.1-2 ConfigwaPion of GC-$7AA Wer.2 (2)

2-5
GC-17A Ver.2 SERVICE MANUAL -
 2.2 Configuration of GC-17AA Ver.2

21 l-43604 Right panel 21 I-43603 DET, flow controller cover

21 l-43061 -91 Fan motor ASSY 1 OOV

21 l-43061 -92 Fan motor ASSY 115V
21 l-43061 -93 Fan motor ASSY 220/24OV

21 l-43296-91 Power unit 100/l 15V

21 l-43296-93 Power Iunit 220/24OV

2214332591 PCB ASSY AUX TEMP

074-80662-01 SW power supply 5V, fl5V 1 OOV

074-80654-31 SW power supply 24V 1 OOV

21 l-42903-01 Rear c

042-60936-14 Guard, fan, FG-12UL

- i

Fig. 2.2.1-3 Configuration of GC-I7AA Ver.2 (3)

2-6
m GC-17A Ver.2 SERVICE MANUAL
 2.2 Configuration of GC-17AA Ver.2

2.2.2 Configuration of oven cooling unit

 2.3.1 GC base unit

I”, -
- LL Aid.--.I1 I 7 I

Fig. 2.3.1-I Assembly diagram of PCB, GC-17A Ver.2 base unit

2-8
m GC-17A Ver.2 SERVICE MANUAL
 2.3 Electric Circuit of GC-17A Ver.2

2.3.2 Power unit

(
(

i (

<
(

c
(

(
t

/;

<
(

C
.

c
C

I
.

FLOW FLOW AUX

SW REGULATOR
HEATER IHEATERZ TEMP CONT
J2

J
- J3 - 320 - 34
I

2-15
GC-17A Ver.2 SERVICE MANUAL m
 GC-17AA Ver.2

R4
---VA
IOKSI
BASE 2w
UNIT TLP633 332K

AC TAB 1 35 SW REGULATOR
ACC TAB 2 J6
INJ C J7
J&l

GND TAB 3

VALVE SPLl

VALVE SPL2

VALVE AIR

512
4 I

FG2 z A”X I thw ““..

00
582
OCI FAN “’

Fig. 2.3.2-2 Circuit diagram of power unit 17A Ver.2

 2.3 Electric Circuit of GC-17A Ver.2

2.3.3 Key unit

!h--?j 0 0 0
wz,i-fER FLOW I l=LOU L

Ii
i+biALyS~ S

R-V’ 0

Fig. 2.3.3-l Assembly diagram of key unit

2-17
GC-17A Ver.2 SERVICE MANUAL -
 2.3 Electric Circuit of GC-17A Ver.2

2 ___. -.-... - .-.--

41
1

/-
[
’ i

ii -
j /

1 !I

2-18
m GC-I-IA Ver.2 SERVICE MANUAL
 2.3 Electric Circuit of G&l-/A Ver.2

2.3.4 AUX temperature control unit

Configuration of AUX temperature control unit

AUX temperature control unit Installation manual for AUX temperature control unit
22 I-43345-91

PCB Assy AUX TEMP CONT

AUX heater wiring 17 V2

221-43848-91

Dummy connector, temperature control block

221-41604-91

GC- 17A V2 Jumper AUX temperature control

22 l-43344-9 1

GC- 17A V2 cable AUX power

221-43343-91

Tapping screw SUS 2.6 x 10

021-60018-01

PCB ASSY 22143325 BOARD 221-43327A

Fig. 2.3.4-l Assembling diagram of PCB, AUX temperature control

2-19
GC-17A Ver.2 SERVICE MANUAL m
 CNS (AUX4.5 LAMP)
R5 /

CNl (BASE UNIT)

AUXPC 6
AUX3C 7
AUX4C 8 OVER IiEAT
.*ToA
AUX5C 9

AUXPS 11
AUXBS 12
I
AUX4S 13
AUX5S 14
AGND 15

I III *“-$‘fl+a”l O.lpF

-l I I I I
= cc
FG FG
CHECK 111 .
Pi

‘CA

-IHl Hl CN2 (POWER CONT)

H2
,,/ 11, ,,,
I ! I ! I-!-- I
CN3 (AUX2) CN4 (AUXJ) CN5 (AUX4) CN6 (AUX5)

+4oooPPwc
R3 .
38.2 ’

Fig. 2.3.4-2 Circuit diagram of AUX temperature control

3.1 AFC (Advanced Flow Controller) Ver.2 ....................................... 3-2
3.1.1 Configuration of AFC Ver.2 ................................................. 3-2
3.1.2 Flow line AFC Ver.2 .............................................................3-3
3.1.3 Electric circuit of AFC Ver.2.. .............................................. 3-5
3.2 Flow controller make-up 17A Ver.2 .................................................. 3-6
3.3 Additional manual flow controller Ver.2 ...................................... 3-7
3.4 AK (Advanced Presser Controller) Ver.2 ................................... 3-9

3-,l
GC-17A Ver.2 SERVICE MANUAL m
 3.1 .I Configuration of AFC Ver.2
AFC 17A V2 Assy

AFC 17A V2 Assy Front Assy Solenoid valve Assy Coil Assy
221-43234-91 221-43227-91------I 221-43221-92 221-43216-91
-92 -92
-93 -93 Needle valve
-94 -94 22 l-26995
-95 -95
Small solenoid valve ASS)- Relay Assy
AFC-SPL pipe Assy 22 I -43690-g 1 221-43996-91 (115V)
221-43233-91 -92 -92 (24OV)
-93 -93 (230V)
= PCB FLOW CONT 17A Assy -94 Not necessary for
g 22 1-43096-g 1 -95 1OOV and 220V.
s
0 TFC Assy Solenoil valve Assy
g 221-43228-91 221-43221-91 Coil Assy
G - Capillary Assy
i4 221-43220-91
(3
- Pressure gauge sensor Assy
221-43642-91

- Differential pressure sensor Assy

221-41575-94

_ Pressure regulatora 6OOkpa

221-18150-92

-91 1OOV type

-92 115v n
-93 220v 1’
-94 240v ‘f
-9s 230V ‘,

3-2
m GC-17AVer.2 SERVICE MANUAL
 3.1 AFC (Advanced Flow Controller) Ver.2

3.1.2 Flow line of AFC Ver.2

 3.1 AFC (Advanced Flow Controller) Ver.2

Vt
TFC + PURGE VENT

Flow rate control + SPLIT VENT

vt=vc+vp+vs

Split mode, splitless mode (Not ready, after elapsing sampling time)

TFC

Flow rate control

Pressure
control

vt=vc+vp+vs

Splitless mode (Ready, during sampling time)

vt=vc+vp

Split OFF F mode

Flow rate control

Completely closed

vt=vc+vp

Split OFF P mode

Fig. 3.1.2-2 Flow line control diagram of AFC Ver.2

3-4
I GC-17A Ver.2 SERVICE MANUAL
 3.1 AFC (Advanced Flow Controller) Ver.2

3.1.3 Electric circuit of AFC Ver.2

Fig. 3.1.3-l PCB FLOW CONT 17A V2

C&l @
fU.2 -0
Ml I---- ----.-,
0.91 7c

Fig. 3.1.3-2 Circuit diagram of FLOW CONT 17A V2

3-5
GC-17A Ver.2 SERVICE MANUAL I,
 670-l 8558-i 1 Pressure gauge 2OOkPa

221-41408-91 Pipe PG-MF-MF Assy

018-21330 Teflon tape 221-l 9502-08 Resistor tube. HZ GCdA

221-l 8150-93 Bellows valve 2K

221-09884-l 8 Pipe MF-MM17 180

AUX IN

Fig. 3.2-l Flow line diagram of flow controller make-up 17A V2

Configuration of flow controller make-up 17A V2

670-18558-l 1 Pressure gauge 200kPa

037-02402-01 Knob B-20V

221-43701 NameDlate. AUX DET flow contrnllnr \ d

-
221-43073 Make-up fixture 221-14775-25 Sticking nameplate AUX

Fig. 3.2-2 Flow controller make-up 17A V2

3-6
- GC-17A Ver.2 SERVICE MANUAL
Configuration of manual flow controller Ver.2 (CFC-17A Ver.2)
CFC- 17 Ver. 2 Instruction manual, Manual flow controller,
221-43833-91 supplement J
-92 221-40159
-93 --I-
-94
-96
( Instruction manual, Manual flow controller,

I supplement E
22140160
1
I
- Manual flow controller main body V2 - - Small solenoid valve Assy
22 1-43999-9 1 22 I-43690-9 1
-92 -92
-93 -93
-94 -94
-96 -95

- Dividing pipe MM-MF-MF - Piping Assy MN flow controller main body

201-48386 22 1-44000-9 1

- Pipe MF-MM - Bellows valve, for capillary

201-48557-26 221-41463-91

- Pipe MF-MM 17 400 - Needle valve Assy

22 l-09864-40 221-17482

- Needle valve S 1
221-26995

- Pressure gauge 300kPa

670-18558-12

-91 IOOV type

-92 115v II
-93 220v ”
-94240v ‘,
-96 230V ‘,

3-7
GC-17A Ver.2 SERVICE MANUAL m
 3.3 Additional manual flow controller Ver.2

221-09864-20 Pipe MF-MM17 200

221-41463-91 Bellows valve, for capillary

221-41408-93 Pipe PG-MF-MF 160 260

670-18558-12 Pressure gauge 3OOkPa

221-31745 Housing

CARRIER IN CARRIER OUT

221-31745 Housing 221-31298-92 Pipe Assy GL-MF 140

221-41410-93 Pipe M5-MF 80 221-l 7482 Needle valve Assy

SPLIT lq ~~-+-j$+--~ SPLIT VENT

035-l 0202 O-ring 1 AP4 020-37065 S truss, M5x6

221-43690-91 Small solenoid valve Assy

22i -43690-92 Small solenoid valve Assy
221-43690-93 Small solenoid vaive Assy -9 1 1OOV type
221-43690-94 Small solenoid valve Assy
-92 115V b
221-43690-95 Small solenoid valve ASSY
-93 220v ”

-94 24Ov ”

-95 230v ”
PURGE >

221-09864-32 Pipe MF-MM17 320

Fig. 3.3 Flow line diagram of manual flow controller main body 17A V2

3-8
- GC-I-IA Ver.2 SERVICE MANUAL
 Configuration of APC-17 V2

APC-17 v2 Instruction manual APC-I 7 J

221-43838-91 22140161
Instruction manual APC- 17 E
c22140166
- Installation manual APC-17 J
221-40183
Installation manual APC- 17 E
c221-40184
- APC Assy
221-44022-91

- Resistor tube for APC Air

221-44020-91

- Resistor tube for APC HZ

22 l-44020-92

konfiguration (quantity) of APC mounting parts Assy (for 2ch, 4ch, and 6ch)
221-44015 -91, -92, -93

2ch 4ch 6ch

-91 -92 -93
APC mounting parts Assy PCB FLOW CONT 17A V2 1 2 3
221-44015-91 22 l-43096
-92
-93 IC M66 24opiFP 1 1 1
075-30820-01

Screw, SIJS Sems BK M4 X 8 1 2 3

02046547

Screw, SUS Sems BK M3 X 6 1 2 3

020-46534

3-9
GC-17A Ver.2 SERVICE MANUAL -
 Chapter 4 Injection Unit

/CONTENTS1
4.1 SPL-17 Ver. 2.. ...............................................................................4-2
4.1.1 SPL- 17 Ver.2 configuration ................................................. 4-2
4.1.2 SPL-17 Ver.2 configuration ................................................. 4-3
4.2 WBI-17 Ver. 2.. ..............................................................................4-5
4.2.1 WBI-17 Ver.2 configuration.. ............................................... 4-5
4.2.2 WBI-17 Ver.2 configuration ................................................. 4-5
4.2.3 WBI-17 Ver.2 flow line.. ...................................................... 4-6
4.3 OCI-17 Ver.2 ..................................................................................4-7
4.3.1 OCI- 17 Ver.2 configuration .................................................. 4-7
4.3.2 OCI-17 Ver.2 configuration .................................................. 4-8
4.4 SPWWBI flow line selection unit 17A Ver.2.. ............................... 4-9
4.4.1 Configuration of SPL/WBI selection unit 17A Ver.2.. ......... 4-9
4.4.2 Flow line of SPL/WBI selection unit 17A Ver.2.. ................ 4-9

4-l
GC-17A Ver.2 SERVICE MANUAL -
 4.1 .I SPL-17 Ver.2 configuration
SPL-17 v2 SPL Injection port Assy 17A V2
221-42939-g 1 221-41270-92

L
-93
-L Heater block i7A V2
221-43011

Heater, PI’, CA INJ 17A V2 Heater, INJ 17A V2

22 I-43025-9 1 221-43026-g 1
-93 -93
-T
Temperature sensor INJ 17A V2
221-43027-91
t Thermocouple INJ 17A V2
221-43028-91
-91 1001115V type
-93 220124Ov ‘r

4-2
- GC-17A Ver.2 SERVICE MANUAL
 4.1 SPL-17 Ver. 2

4.1.2 SPL-17 Ver.2 configuration

020-l 2104 Flat screw M3x6

Side of heat insulator, 17A V2

/ Heater y \ :I-411 :,:“‘k, l7A V2

221-43025-91 Heater PT, CA injection, 120V

221-43025-93 Heater - PT, CA injection, 240V 221-43021 Securing plate heater block, 17A V2

221-34579 Needle guide for fin

221-41286 Septum nut

221-41272-95 Glass insert fixing nut, 17A V2

221-43886
___- Heat insulator inj

221-42938 Top cover, SPL-17A V2

020-46539 SUS S

221-43011 Heater block, 17A V2

221-42998 Nipple for gasket

Fig. 4.1.2-1 Configuration 1 of SPL-17 Ver.2

4-3
GC-17A Ver.2 SERVICE MANUAL I
4.1 SPL-17 Ver. 2

221-42938 Top cover, SPL-17A V2

020-12104 SUS flat screw M3x6

221-43025-91 Heater PT, CA INJ, 17A V2, 120V

221-43025-93 Heater Pi, CA INJ, 17A V2,24OV
I

221-4301 i Heater block, 17A V2

221-41270-92 SPL injection port ASSY, 17A V2

221-43021 Securing plate heater block, 17A V2

Aluminum foil

.221-43027-91 Temperature sensor INJ, 17A V2

224-43026-91 Heater INJ, 17A V2 120V

221-43026-93 Heater INJ, 17A V2 240V
\

\221-43028-91 Thermocouple INJ, 17A V2-

Fig. 4.1.2-2 Configuration 2 of SPL-17 Ver.2

4.2.1 WBI-17 Ver.2 configuration

WBI unit, Ver.2

221-43861-91
-93

User’s manual, WBI-17 Ver.2 (Japanese version)

221-40137

User’s manual, WBI-17 Ver.2 (English version)

22140138

AFC-WI31 piping Assy

221-43868-91

Glass insert, wide bore

221-41599

4.2.2 WBI-17 Ver.2 configuration

WBI- 17 unit Ver.2 configuration is com-
mon with SPL-17 Ver.2 excluding the fol-
lowing two points.

Table Different points between WBI-17 Ver.2

and SPb-17 Ver.2

From INJ b!ock lower

From INJ block side to inside of col-
Fig. 4.2.2 WB1-17 Ver. 2

For other configuration, refer to configuration of SPL- I7 Ver.2.

4-5
GC-17A Ver.2 SERVICE MANUAL -
 221-43869-91 Dividing pipe Assy

221-34121-93 Molecular sieve filter

I-- 221-43870-91 Resistor tube Assv

201-48560-20 Pipe MF-GF 200

I
201-48560-20 Pipe MF-GF 200

221-43861-91 WBI unit V2 (100/l 15V)

221-43861-93 WBI unit V2 (220/24OV) 221-43708-91 Filter Assy PURGE

-L
----- ---- ----l
I M 1

w ’ SPLIT VENT
L----------I

Inside of L.:
Y -’ indicates the flow line of AFC V2.

Fig. 4.2.3 Flow line diagram of VW-17 Ver.2

4.3.1 OCI-17 Ver.2 configuration

User’s manual (Japanese version)

Instruction manual for OCI- 17 V2, English version

Injection, OCI- 17 Ver.2 Injection unit, OCI-17 Ver.2 without heater OCI injection port Assy,17 Ver.2
221-42218-92

Capillary adapter, PTV- 17

221-42221-91

Adapter for the on-column

221-42222-81
Accessory, OCI-17 Vet2
22 l-43778-9 1 Spacer, OCI
Step-downtransformer,OCI-17 221-42359
221-43265-91
Heater IT, CA Assy, ITV Micro heater, PTV
221-42405-91 221-42406
*-
Temperature Senser Assy E
221-41568-91

L
Themocouple Assy
221-41569-91

4-7
GC-17A Ver.2 SERVICE MANUAL M
 4.3 OCI-17 Ver. 2

4.3.2 OCI-17 Ver.2 configuration

221-42359 Spacer, OCI

// 221-42222-91 Insert OCI

221-39276 Sleeve

_;--------I--
-- 221 -43777

221-42221-91
Cover, lower OCI-17

Capillary adaptor
V2

OCI-17

Fig. 4.3.2 Configuration of WI-17 Ver.2

4-8
m GC-17A Ver.2 SERVICE MANUAL
4.4.1 Configuration of SPL/WBI selection unit 17A Ver.2
SPUWBI selection unit 17A V2 Instruction manual, SPUWBI selection unit, Japanese version
221-43829-91 22140141
-92 Instruction manual, SPUWBI selection unit, English version
221-40142
(
INJ U2 selection unit
221-43866-91

Piping Assy for selection unit

221-43871-91

Installation manual, SPLWBI, Japanese version

22140164
Installation manual, SPL.WBI, English version
22140165

4.4.2 Flow line of SPLlWBl selection unit 17A Ver.2

221-25500-91 10-wav valve Assv

Bellows vah /e
Carrier gas TFC
‘N a---
L.jJ SPL
S
P 0
T’l
201-48563-l 0 Pipe MF-GM 100

On’ ““‘“3-70 Pipe MF-GF 700

-4-l- I I c2?Is5% --
Needle valve / 1 r GX-SLN

Flow line selection

\\ - : SPL side

Fig. 4.4.2 Flow line diagram of SPL/VVBl selection unit 17A Ver.2
Chapter 5 Detector Unit

5.1 WFID-17 Ver.2/l?ID-17 Ver.2 unit ................................................. 5-2

5.1.1 WFID- 17 Ver.2 configuration ............................................... 5-2
5.1.2 WFID-17 Ver.2FID-17 Ver.2 configuration.. ...................... 5-4
5.1.3 WFID-1’7 Ver.2/FID-17 Ver.2 H2, Air flow line.. ................. 5-6
5.1.4 Electric circuit of WFID-17 Ver.2 controller.. ...................... 5-7
5.1.5 Electric circuit of W!?ID-17 Ver.2 controller ........................ 5-10
5.2 TCD- 17 Ver.2 unit ..........................................................................
5-13
5.2.1 TCD- 17 Ver.2 configuration .................................................S-13
5.2.2 TCD-17 Ver.2 codiguration .................................................5-14
5.2.3 Electric circuit of TCD- 17 Ver.2 controller control ............. 5- 17
5.3 FFD-17 Ver.2 unit ..........................................................................
5-20
5,3.1 FPD-17 Ver.2 configuration ................................................. 5-20
5.3.2 PD-17 Ver.2 configuration ....................................................5-21
5.3.3 FPD-17 Ver.2 Air flow line .............................................5-22
Hz

5.3.4 Electrical system of FPD-17 .................................................5-23

5.4 ECD-17 Ver.2 unit ..........................................................................
5-28
5.4.1 ECD- 17 Ver.2 configuration .................................................5-28
5.4.2 ECD-17 Ver.2 configuration .................................................5-29
5.4.3 Electric circuit of ECD-17 Ver.2 controller control ............. 5-30
5.5 FTD-17 Ver.2 unit .........................................................................5-34
5.5.1 FTD- 17 Ver.2 configuration 5-34
.................................................
5.5.2 FTD-17 Ver.2 configuration .................................................5-35
5.5.3 FTD-17 Ved resistor tube flow line .....................................5-36
5.5.4 Electric circuit of FTD-17 Ver.2 power controller ............... 5-37

5-l
GC-17A Ver.2 SERVICE MANUAL m
 5.1 .I WFID-17 Ver.2 configuration
/ FID-47 wide-range controllerVer.2 (

17 wide-range. - FID-17 unit -

-mDc
FID- Nozzle base Assy, FID- 17
Ver.2 v2 V2 Assy 221-39692-92
221-43311-91 221-42951-91 221-39631-92
-92 -93 Nozzle Assy Nozzle with cap 0.3mm dia
-93 221-37304-03 22 l-33265-02
-94
High-voltage unit Assy, FID-17 Ver.2
221-42940-91

Collector Assy, FID- 17 - Input cord Assy 17A

221-39695-93 221-21912-95

Ignitor Assy - Filament Assy ~ StemAssywith

221-41327-91 221-41847-91 filament
221-41980-91

- Heater PT, CA Assy, DET 7 Heater Assy, DET

221-43346-91 221-43347-91
-93 -93

Temperature sensor, DET 17A

221-43348-91

Thermocouple, DET 17A - ‘hmocouple, CA-l@.

221-43349-91 2 I l-32977-90

- FID wide-range controller - PCB, FID wide-range controller V2

control, 17A V2 221-43271-91
22 1-43290-g 1
- Cable, ITG WIDE
221-41124-91
t Signal cord DET Assy
221-41085-92 _

- Flow controller, Hz-Air FID - - - Small solenoid valve.

22 I-43076-9 I 22 1-43309-g 1
-92 -92
-93 -93
-94 -94

- FID DET piping Assy - Bellows valve 2K (HZ)

221-41089-91 221-18i50-9i

- Bellows valve 2K, including resistor (Air)

221-41511-91

- Pressure gauge, 2COkPa

670-18558-11
-91 1OOV type
-92 115v *
-93 22QV ‘<
-94 24Ov f/

5-2
- GC-17A Ver.2 SERVICE MANUAL
 5.1 WFID-17 VeCYFID-17 Ver.2 unit

FID-17 Ver.2 configuration

FID-17 linear controller Ver.2
FID-17linearcontroller FID- 17 unit Same as FID- 17 wide-range controller Ver.2
221-43310-91 221-42951-91
-92 -93
-93
-94 FID linearcontrollercontrol,17A V2 PCB, FID linear controller V2

221-43289-91 T 221-43268-91

Cable, ITG, LINEAR

221-41123-91

Signal cord DET Assy

221-41085-92

Flow controller, Hz-air FID - Same as WFID- 17 V2

221-43076-91
-92
-93
-94

FID-DET piping Assy

221-41089-91

-91 1OOV type

-92 115V 0
-93220v ”

-9424ov ”
 5.1 WFID-17 Ver.2/FID-17 Ver.2 unit

5.1.2 WFID-17 VerZFID-17 Ver.2 configuration

221-41327-91 lgnitor ASSY

221-39695-91 Collector ASSY, FID-17

221-42940-91 High-voltage unit ASSY. FID-17 V2

221-43683 Heat insulator top section, DET-17A V2

221-43346-91 Heater, PT. CA, DET V2 120V

221-43346-93 Heater, PT. CA, DET V2 240V

221-37304-03 Nozzle ASSY

[“q ,,I !l,,, \ 221-42948 Top cover, FID-17 V2

\.., 221-42947_______
BotIom-plate heater block, 17 V2-

‘\;;\I 221-42949 Sleeve for FID

023-66181-01 Flat washer, SUS 10

\y 221-33463 Nut, Hx12 L=6

221-39692-92 Nozzle base, FID-I 7 V2

Fig. 5.1.2-l Configuration 1 of WFID-17 Ver.2/FID-17 Ver.2

5-4
m GC-17A Ver.2 SERVICE MANUAL
 5.1 WFID-17 Ver.2/FID-17 Ver.2 unit

M3x6 221-41327-91 lgnitor ASSY

1 -1
020-46534 SUS SEMUS screw, M3x6

221-42948 Top cover, FID-17 V2

221-39695-91 Collector ASSY, FID-17

/
221-43683 Top heat insulator, DET-17 V2

221-42940-91 High-voltage unit ASSY, FID-17 V2

221-37304-03 Nozzle ASSY

221-39692-92 Nozzle base, FI D-l 7 V2

020-46541 SUS SEMUS screw, M

_ 023-66181-01 Flat washer, SUS 10

221-33463 Nut, Hx12 L=6

I
26mm
6 >

Fig. 5.1.2-2 Configuration 2 of WFID-17 Ver.2/FID-17 Ver.2

GC-17A hr.2 SERVICE MANUAL

 5.1 WFID-17 Ver.2/FID-17 Ver.2 unit

51.3 WFID-17 VerX/FID-17 Ver.2 HZ, Air flow line

221-41408-91 Pipe PG-MF-MF Assy

670-I 8556-l 1 Pressure gauge 200kPa

221-31745 Housing

221-09864-20 Pipe MF-MM17 2x180 201-3021 l-02 Washer, Ml0

221-l 8150-91 N Bellows valve 2K

Hz IN

201-47435 Septum, injection port, silicon

-~221-19503-08 Resistor tube, Hz GC-8A

040-21338-01 Needle, JNC4-M5

221-43309-91 Small solenoid valve 17V2 100

221-09864-18 Pipe MF-MM17 2x180

221-31745 Housing

Fig. 5.1.3 HZ, Air flow line of WFID-17 Ver.2/FID-17 Ver.2

5-6
- GC-17A Ver.2 SERVICE MANUAL
 5.1 WFID-17 Ver.2/FID-17 Ver.2 unit

51.4 Electric circuit of WFID-17 Ver.2 controller

5-7
GC-17A Ver.2 SERVICE MANUAL m
 Detector Unit

ab

A0 (UlEl-
ovy
Al
A’ YI
43 vt

CZZ
22OP I ,,
4 Fig. 5.1.4-2 Circuit diagram of WFID-17 V2 (112)
5.1 WFID-17 Ver.2/FID-17 Ver.2 unit

Q’ v

.F
IA

5-9
GC-17A Ver.2 SERVICE MANUAL m
 5.1 WFID-17 Ver.2/FID-17 Ver.2 unit

5.1.5 Electric circuit of FID-I7 Ver.2 controller

.
?
-4
30
i P 0

t
-
-6

Fig. 5.1.5-l Assembly diagram of PCB, FID-17 V2

5-10
- GC-17A Ver.2 SERVICE MANUAL
5.1 V\iFID-17 Ver.2/FID-17 Ver.2 unit

5-11
GC-17A Ver.2 SERVICE MANUAL -
 5.1 WFID-17 Ver.2/FID-17 Ver.2 unit

--
t

I/ ----I I

5-12
m GC-17A Ver.2 SERVICE MANUAL
 ,:,,’ :g-. : 2, ‘.
TCD-17 Ver.2 unit
xI

52.1 TCD-17 Ver.2 configuration

( TCD-17 V2 Assy /

Replacement work of major components such as TCD cell at the

local side cannot be done since the performance may not guar-

TCD-17 Assy - - TCD unit Assy - Heater, F’T, CA Assy, TCD Heater Assy, 1OOV/ I SOW
22 l-42474-91 221-41900-91 221-41902-91 221-41903-91
-92 -93 -93 -93
-93
- Sample inlet section Assy Temperature sensor Assy
221-41897-92 221-41568-91

Thermocouple Assy
221-41569-91

- TCD cell IM4 Assy Block M4 Assy

221-42503-91 221-42501-91

- Capillary adapter, DET Filament Assy

221-41451-91 221-41945-91

- TCD- 17 controller Assy - - PCB, TCD-17 Assy

221-42600-91 221-42594-91

- Connector Assy, TR TCD

22 I-42604-9 1

- Connector Assy, 12V TCD

221-42602-g 1

- Signal cord DET Assy

221-41085-91

- Cable, ITG, LINEAR

22!-4!!23-91

- Accessory TCD-17 Assy Vent piping Assy

221-42693-9 1 221-41908-91

- Resistance tube TCD Assy

221-42511-91

Graphite fitting jig, TCD

221-41532-95
-9 1 1OOV type
-92 115v f/
-93 220v ”

5-13
GC-17A Ver.2 SERVICE MANUAL -
 5.2 TCD-17 Ver.2 unit

5.2.2 TCD-17 Ver.2 configuration

221-41955-02 Bottom sheet, high-temperature side 221-41960 Heat insulator, bottom, inner tank
r-
I- 221-41934 Cell fixing block 22141961 Heat insulator, side, inner tank

020-05157 SUS SEMUS pan head screw, M4x45 221-41963 Heat insulator, lid, inner tank

023-77040 SW spring washer 2-M4 221-41931-02 Heat insulator, center, inner tank

22142470 Block cover 221-41938 Heat insulator, inside, outer tank

221-41936-02 Bottom sheet 221-41964 Heat insulator, inside bottom, outer tank

221-41965 Heat insulator, inside lid, outer tank

221-41917-01 Heater ring

221-42745 Heat insulator, front, center

\ / J--T
\ 221-42746 Heat insulator, upper, center

221-41966 Heat insulator, bottom of front,

TT” ‘,f /__ outertank

SEMUS BK screw, M4x25

erature fuse holder

978 Heat insuiator upper, inlet, -I_17 V2

2 Spacer, SBE-306

02-91 Heater, PT, CA ASSY, TCD

02-93 Heater PT CAASSY TCD

020-46654 SUS SEMUS screw, M4x20

023-04040 SUS nut, 1 M4

221-43023 Base plate, high-temperature side

221-41958 Bottom, inner tank

!l-4195602 Heater block, high-temperature side

-41959 Lid, inner tank Fig. 5.2.2-l Configuration 1 of TCD-17 Ver.2

5-14
m GC-17A Ver.2 SERVICE MANUAL
 5.2 TCD-17 Ver.2 unit

221-41940 Outer tank cover

221-41965 Heat insulator, inner part cover, outer tank

421-42746 Heat insulator, top of front

t insulator, cover, inner tank

22141931-02 Heat insulator, center, inner tank

221-41963 Heat insulator, cover, inner tank

5-15
GC-17A Ver.2 SERVICE MANUAL m
 5.2 TCD-17 Ver.2 unit

1903-91 Heater ASSY 1 OOV

7-38855-29 SBA-320

Fig. 5.2.2-2 Configuration 2 of TCD-17 Ver.2

5-16
- GC-17A Ver.2 SERVICE MANUAL
 5.2 TCD-17 Ver.2 unit

52.3 lectric circuit of TCD-17 Ver.2 controller control

VEBSZPLZZ OtlVO9 3 hssvLt-a3L83d L-L-J

NVdW NI 3OVW l-lzavi’#is@

-

5-17
GC-l-/A Ver.2 SERVICE MANUAL B
 R39 hDo 7l.m

+lq2+
Fig. 5.2.3-2 Circuit diagram of TCB-17 V2 (112)
 5.2 TCD-17 Ver.2 unit

5-19
GC-17A Ver.2 SERVICE MANUAL m
 II ,,:

.~ I. :,

/.’ _.:s*.:,
.. 3 FPD-17 Ver.2 unit

53.1 FPD-17 Ver.2 configuration

/ FPD-17 V2 1
FPD-I7V2- User’s manual, FPD-17 Ver.2 (Japanese version)
22 l-43756-9 1 22140124
-92
-93 User’s manual, FPD- 17 Ver.2 (English version)
-94 22140125

Installation manual, FPD- 17 Ver. 2 Japanese version

221-40179

f Installation manual. FPD- 17 Ver. 2 English version

( 22140180
FPD- 17 Ver.2 unit - - Nozzle base Assy, FPD- 17 -7 Qg~tt&z, nozzle base FPD
221-42968-91 221-41772-91
-93 Nozzle base welding Assy, FPD- 17
- Body
221-41777 22 1-42052-g 1
- Quartz plate Assy Nozzle S
221-00887-01 221-41852
- Radiation section ASSY, 17A Ver.2 Nozzle L
221-43759-91 22 l-42023
t Shield
221-41354
- ;;&s;syjPD17 7 ;;Y-@;$~FPD-~~

- Heater block, FPD-17 Ver.2 L Filament Assy

221-41787 221-41847-91
- Base section
Heater, PT, CA, Assy 22 l-43397-9 1
221-43346-91
-93 Tempera ture senser, 17A V2

t- Thermocouple, 17A V2
221-43349-91
- Photo-multiplier Assy, FPD- 17 Photo-multiplier R268
221-41823-91 670-14404
- Head section
Heater, PT, CA, Assy FPD
221-42168-91
-93 Temperature sensor Assy
221-41568-91
/-- Thermocouple Assy
FPD linear controller control Assy Cable, ITG, LINEAR 221-41569-91
221-41834-91 221-41123-91
-r
Accessory, FPD-17 Ver.2 Signal cord DET Assy
221-43758-91 221-41085-91
t PCB, linear amp. FPD Assy
22 1-399.59-9 1

Additional temperaturecontroller,17A Ver.2 - PCB AssY AUX TEMP

221-43345-91 221-43325-91

Flow controller, Hz-Air FPD ____ Small solenoid valve, 17A Ver.2
221-43757-91 221-43309-91
-92 -92
-93 -93
-94 -94 -91 1OOV type

Prassure regulator, 2K -92 11%’ fi

FPD-DET Piping Assy
221-41089-92 221-18150-91 -93 220v N
t Pressure gauge, 200kPa -94240v r/
670- 18558- 11
 5.3 FPD-17 Ver.2 unit

5.3.2 PD-I 7 Ver.2 configuration

221-41783-91 Cap Assy FPD17

22142964 Connection plate cover FPDl7V2

221-43760 Heater block FPDl7V2

221-41772-91 Nozzle base Assy FPD17

-II
----.._ “L _ 221-42965 Cover, lower FPD17V2

kl%l< 023-66181-01 Washer, Flat, SUSlO

201-30211-01 Washer, Ml0

221-33463 Nut, HXlPL -= 6

221-42168-91 Heater PT CA Assy FPDIOO

22 l-42 168-93 Heater PT CA Assy FPD220

-221-42057 Wiring holder

221-41777 EIod
____
221-41772-91 Nozzle base Assy FPDlP

2214334691 Heater PT CA DET V2 120V

-93 Heater PT CA DET V2 220V

22143760 Heater block FPDI 7V2

Fig. 5.3.2 Configuration of the FPD-17 Ver. 2

 5.3 FPD-17 Ver.2 unit

5.3.3 H2 and Air flow lines of the FPD-17 Ver. 2

221-09864-18 Pipe MF-MM17 180

221-l 8150-91 Bellows valve 2K

221-41408-91 Pipe PG-MF-MF Assy

018-21330 Teflon tape

670-l 8558-l 1 Pressure gauge 200 kPa

221-43309-91 Small type solenoid valve 17 V2 IOOV

221-09864-l 8 Pipe MFMM17 180
-53
-92
no
-94
n
,,
I,
il5V
220v
240V

l- IN OUT

OUT

221-41527-91 Pipe PG-MF-MF-MMASS

221-19503-08 Resistance tube, AIR GG8AF

201-47435 Rubber plug, injection hole, silicon

201-47435 Rubber plug, injection hole, silicon

221-42080-92 Branch pipe AIR FPD17 V2

201-47435 Rubber plug, injection hole, silicon

221-19503-08 Resistance pipe AIR GC-8AF

221-31745 Housing

Fig.5.3.3 HZand Air flow lines of the FPD-17 Ver. 2

5-22
m GC-17A Ver.2 SERVICE MANUAL
 5.3 FPD-17 Ver.2 unit

5.3.4 Electric circuit of FPD-17 Ver.2 controller

0
E-f/.?

Fig. 5.3.4-l Assembly diagram for PCB, FPD-17 V2

5-23
GC-17A Ver.2 SERVICE MANUAL I
 +R< Ml0
+12v
OV(12)
+15v
-15v
AD7248
A GND
+5v
D GND

Ii:
EE
-
Ei
Ii;

A0
2:
A3

1
t15v 2
4 AG 5
-15v 3.4
DC1 7
i DC24 8
DC4L B’3 +24V
+I--+
OUT#
I 1 I
m H4
--I LSi5 RN1 01 I X2

Fig. 5.3.4-2 Circuit diagram for FPD-17’ V2 (113)

 R14 10K

,R4,,q ’ -4iSl588 1
3>,4
c40.022p 2, ,l 7 132qr$ RN2227Xr
5""S I
K2 I nr

1OOK
Q I
I
I- T-
ITJIA12EZX41 I I I

Fig. 5.3.4-3 Circuit diagram for FPD-17 V2 (213)

Detector Unit
DC24V T101
(CN1.613)
181832 X4
4 D102 IK 150K TPI-\

ov (12) <- 1 1
(CNI .B6)
H.V.

10K
---O(GND)/

HV.OFF - II
t
Clot
0.11
i-l

AGND
(CNl.A2) <

Fig. 5.3.4-4 Circuit diagram for FPD-17 V2 (313)

 5.3 FPD-17 Ver.2 unit

The electrometer section of the FPD consists of Ml and peripheral

components. This electrometer reduces the Ml output to a l/10 and
sends this output from CN2 to a recording device (data processing
device).
M3 is a hybrid IC incorporating a circuit that prevents signal satu-
ration in Ml. Excess signal is sent from M2’S output pin 7 to M3’s
pin 3. The signal activates relay K4, which then sends Ml’s input
current to M2’s pin 1.
The high-voltage power supply unit for the photomultiplier consists
of M101, QlOl, Q102, and peripheral components.
This power supply unit uses the +24V direct-current power supply ,, .;; y;:~4
.““~;~.~
+,
that the GC base unit generates for relays. .?‘-:5i”
The +24V is converted to a stable +15V power by the Ml01 3-ter- I, *“,:““‘~,y:
? __‘;.“)_
T
minal regulator (TA780 15).
The +15V power is sent to a multivibrator transformer consisting ‘$
of 4104, Q103, and TlOl, by which the electric power is converted 5
to an alternate current of 700V and about 22 kHz. This AC power 5
source is rectified by components DlOl through D104 to about G
P
-700V and sent to the output terminal.
R107 (10K) is inserted in the return side to prevent excess current
from flowing into the photomultiplier. RlO7 switches off QlOl
when a current of over 225@ fiows and turn off the converter
input. The resistance value of R107 on the return side is IOK. The
M102’s input voltage of 225mV. When the voltage at the ends of
R107 exceeds 225mV, QlO5 is switched on and the base of QlO2 is
switched to L. This in turn switches off the DC/DC converter input
voltage and the high-voltage power supply. VRl (5K) inserted in
the base of Q102 is for the tine adjustment of the high-voltage
power supply.

5-27
GC-17A Ver.2 SERVICE MANUAL I
 5.4.1 ECD-17 Ver.2 configuration
1ECD-17 V2 1
ECD cell unit with ECD-17 Ver.2 without cell Base heater block, ECD Ver.2
indication, IOOV 22 I-42960-9 1 221-42954
221-4375 l-50
-----L- ECD cell with [email protected]) Heater, PT. CA DET Ver.2 Heater, DET Ver.2
221-25055-50 221-43346-91 221-43347-91
T
Temperaturesensor,DET Ver.2
221-43348-91
t Termbcouple, DET Ver.2
22 1-43349-P 1

ECD cell unit ECD- 17 Ver.2 without cell Base heater block, ECD Ver.2
221-43751-91 22 l-42960-9 1 221-42954
-93 -93
Heater, Pt. CA DET V2 Heater, DET Ver.2
---I ECD cell (ECD-9) 221-43346-91 22 1-43347-9 1
221-25055-91 -93 -93
Temperaturesensor,DET Ver.2
221-4334X-91
Termocoupl.e, DET Ver.2
221-43349-91

ECD- 17 Ver.2 User’s manual, ECD- 17 Vet2 (Japznese version)

controliercontrolwithout cell. 22140126
221-43747-91 User’s manual, ECD-17 Ver.2 (JEnglish version)
-92 ----r 221-40127
-93
Installation manual ECD- 17 Ver. 2,

Installation manual ECD- 17 Ver. 2, 1

ECD controller control Assy Cable, ITG, LINEAR

221-41123-91

Acessory, ECD- 17 Ver.2 Signal cord DET Assy

221-41085-91

L PCB, ECD Assy, 17

20 l-42870 221-39614-91
RI plate (English version)
22 l-07755

5-28
m GC-17A Ver.2 SERVICE MANUAL
 5.4 ECD-17 Ver.2 unit

5.4.2 ECD-17 Ver.2 configuration

02346081 Washer, fiat and small-sized round

l-25055-50 ECD-No.6 (with indication)

-___-- -91 ECD-9 cell ~-

Fig 5.4.2 Configuration of ECP-17 Ver. 2

5-29
GC-17A Ver.2 SERVICE MANUAL 7
 5.4 ECD-17 Ver.2 unit

5.4.3 Electric circuit of ECD-17 Ver.2 controller control

The ECD control for GC-17A V2 is a linear ECD type. Figs. 5.4.3-
2 and 5.4.3-3 show a circuit diagram of ECD-17.
The carrier gas (N2) Inside the ECD cell is ionized by radiation
from the radiation source (Nz) sealed inside the cell. When pulse
voltage is applied to the electrode inside the cell, electrons are
taken in to create a flow of electric current. The electrode is con-
nected with the input terminal (CN-2) of the ECD controller.
When the carrier gas includes no sample, a prescribed current flows
so that the input of the amplifier Ml of ECD-17 remains at OV. Ml,
as illustrated in Fig. 5.4.3-2, is designed as an integrating amplifier.
When there is no sample, its output remains at OV. Two operational
amplifiers of M2 are connected to the output side of Ml. The M2
amplifier at the output terminal 1 is a phaseinverting amplifier for
picking up signals. The M2 amplifier is designed so that the signal
output turns to + when Ml output changes to -. The amplification
degree of this amplifier is 1, which means that Ml output inverts.
On the other hand, the operational amplifier M2 at the output ter-
minal 7 functions as a buffer amplifier of M3. However, since the
A3 input requires a voltage input on the + side, this amplifier is
also used as a phase-inverting amplifier. The degree of amplifica-
tion is set at 1.

CNl SC -I
- IMADZU MADE IN JAPAN

Fig. 5.4.3-l Assembly diagram for PCB, ECD-17 Ver. 2

5-30
m GC-17A Ver.2 SERVICE MANUAL
 CN2
0
R32 475K
_- vvx
I’ l-

R21
10K

+15

10K
R18 1K

Li+---- +15

cm
(SH : 1)

Fig. 5.4.3-2 Circuit diagram for ECD-17 Ver. 2 (l/2)

Detector Unit
 CNl w1a tiw

C
+15v

-15v C

A GND C

M7
( Ml3 AD7248
+5v -15v +15v

D GND (

DO (

Dl (

D2 (

D3 (

(
D4
(
D5
(
D6
(
D7

Ml5
A4
A0 , ‘A

Al

A2

A3

G2B __

4#
(SH.2)

OUT#
- B9 IN#
IN#

Fig. 5.4.3-3 Circuit diagram for ECD-17 V2 (212)

 5.4 ECD-17 Ver.2 unit

M3 is a V/F converter, that generates pulse voltage in proportion to

input voltage. Since the duty cycle of this pulse voltage is very
small, the pulse width required for the cell must be provided. A
mono-stable multivibrator (M4 l/2) is used to expand the pulse
width, irrespective of the frequency of the pulse voltage. This pulse
width is determined by C IO and R 17.
M5 is a buffer for the mono-stable multivibrator and drives Ql.
The range of the ECD controller is changed by altering the frequen-
cy of the pulse voltage. Therefore, a l/10 counter (M4) is provided
between the V/F converter and the monostable multivibrator is
changed to either l/l0 or l/l. --’
In order to feed pulse voltage to the cell, the output of M5 is ampli- 2: *
I----
I 4::.
fied by Q 1, and deprived of the D. C. component by a pulse trans- :
L-i-
former ; therefore, only the A.C. component will be applied. The ”
current flow switching circuitry consists of R30, R31, R21, VRl, *g
and M9. s
Set a suitable current value for the required sensitivity or size of the 5
background for the analysis. tii
B

5-33
GC-17A Ver.2 SERVICE MANUAL -
 5.5.1 FTD-17 Ver.2 configuration
1 FTD-17V2 ]

FrD-17v2 - - User’s manual, FID- 17 Vet2 (Japanese version)

221-43762-g 1 22140128
-92 User’s manual, Ftd- 17 Ver.2 (English version)
( 221-40129 1
Installation manual FTD- 17 Ver. 2, Japanese version
221-40171
Installation manual FTD-17 Ver. 2, English version
22140172 >
Power controller, FTD- 17 PCB, power controller, FTD- 17
221-41871-91 221-41849-91

221-41871-93
Power controller FTD- 17 23 >

Electrode section FTD- 17 Electrode section, FTD-17 without collector

221-41722-91 ------I zI-z2-:*,,

221-18704-91

k;stt;~;p9iy,FrD-17 / ;;;gggysy
Branch pipe Assy
221-25288-92
! FTD resistance tube Assy, Hz
221-18713-95

FI’D resistance tube Assy, Air

221-18’713-96

i- Stop valve
201-35039-00

Cable, FTD power controller

221-41881-91

Accessory, FTD- 17 Ver.2

5-34
- GC-17A Ver.2 SERVICE MANUAL
 5.5 FTD-17 Ver.2 unit

55.2 Ftd-17 Ver.2 configuration

221-l 8697 Shield cap

I
023-04040 Nut, SUSl Ml4

ndentation, M3 x 6

036-l 1015 O-ring, Silicon PI 4

FiD nozzle
, High-pressure cable

22i-42940-91 High-pressure portion Assy FlU17 V2

AIR - J!i “1
~7304-03

221-39692-92
Nozzle
Nozzle
Assy-
base portion FID17 V2

H2+ -
Make-up gas

Capillary adapter

Fig. 5.52 Configuration of FID-17 Ver. 2

 5.5 FTD-17 Ver.2 unit

5.5.3 Flow lines of FTD-17 Ver.2 resistance tube unit

221-l 8713-95 FTD-9 resistance tube Assy H2

201-35039-00 Stop valve

H2 IN

221-25288-91 Branch pipe Assy 221-25288-91 Branch pipe Assy

201-35039-00 Stop valve

LI-------

AIR IN AIR OUT

\

221-25288-91 Branch pipe Assy 221-25288-91 Branch pipe Assy

221-18713-96 FTD-9 resistance tube Assy AIR

Fig. 5.53 Flow lines af FTD-17 Ver.2 resistance tube unit

5-36
0 GC-17A Ver.2 SERVICE MANUAL
 5.5 FTD-17 Ver.2 unit

Electric circuit of FTD-17 Ver.2 power controller

5-37
GC-17A Ver.2 SERVICE MANUAL -
 04
Dl
D2 24V
13
D3 c21 24V
D4 RSl 0
D5
D6
D7
A4
Al
A2
A3 READ
6# LOW 2sc
2661
OUl

IN

CN2

R3
5.11K

OUT
Y4t
(64)

--lIp,,l’” “-“‘P

Fig. 5.5.4-2 Circuit diagram for power controller, FTD-17 v2

 5.5 FTD-17 Ver.2 unit

The circuit consisting of M20, M21, R4, and R5 generates a pulse

signal of about 100 kHz. This signal is amplified by Tl, Q6, 47,
QS, and Q9. (The amplification rate depends on the setting.) This
high-frequency signal is then supplied to the primary side of the
toroidal coil inside the FID eke&ode.
Ml0 receives a current of set value from the key unit. The output
signal generated in the FTD (FID) control unit enters CN4 and it is
amplified to about 20 times at Ml ‘S pin 3.
The setting signs1 from the key unit and the feedback signal from
the FTD (FID) control unit are compared by M2. M2’s pin 1 or
pin7 generates an output that correspons to the difference in the
input signals.
For example, when the feedback signal from the FTD (FID) control
unit is large, M2’s pin1 turns H. The signal then enters the DOWN
side of the UP/DOWN counter (M6) and the counter output is
reduced. On the other hand, when it is the setting signal that is
large, the signal enters the UP side of the UP/DOWN counter and
the counter output is incresed.
When both signals are about the same (i.e., feedback signal within
a range of 90 to 100% of the setting signal)., M2’s pins1 and 7 turn
L, and the UP/DOWN counter maintains the same value. At the
same time, the READY lamp on the power controller lights up. M7
is a D/A converter. It converts the UP/DOWN counter output to an
output within a range of 0 to 2.4V.
CN5’s pins 9 and 10 are normally short-circuited, so that M7’s out-
put is supplied to M3. M3’s pin1 generates an output ranging
between --2.5 to -4SV. The second-stage M3 switches the polari-
ties of the output to a range of +2.5 to +4.5V.
A one fifth of the pulse height (voltage) generated at components
Q6 through Q9 and the output voltage from M3’s pin 7 are com-
pared by M4. As a result, the pulse height of the output from CN3
is between 12.5 and 22.5V. The oscillating circuit consists of Ml4
and peripheral components, and it feeds signal to the UP/DOWN
counter.
The oscillating frequency can be varied by SW02 (DIP SW)
When SW02 (1) and (2) are both OFF :
6-set cycle
When SW02 (1) ON:
3-set cycle
When SW02 (2) ON :
300-msec cycle

5-39
GC-17A Ver.2 SERVICE MANUAL -
 5.5 FTD-17 Ver.2 unit

Ml5 and peripheral circuits serve as the feedback ON/OFF circuit.

When the adjustment mode is “O,“(D) turns L and M17’s pin6 turns
L. Then the output of the UP/DOWN counterremains the same.
When the detector unit (Fid power controller) turns OFF, M15’s
pin5 turns H, switching Q4 ON and Ql OFF. This cuts off the out-
put voltage.

5-40
- GC-17A Ver.2 SERVICE MANUAL
Chapter 6 Appendix

6.1 Maintenance parts list .............................................................................. 6-2

6.2 Special key operations.. ........................................................................... 6-4
6.3 GC general.. ............................................................................................. 6-8
6.3.1 Maintenance precautions .............................................................. 6-8
6.3 2 Replasing restrictor and septum.. .................................................. 6-9
6.3.3 Inspection of molecular sieve filter.. ............................................. 6-10
6.3.4 Inspection of compressor and silica gel ........................................ 6-11
6.3.5 Injection port septum .................................................................... 6-12
6.4 Temperature sensor.. ................................................................................ 6-15
6.5 CA Thermocouple.. ................................................................................. 6-16
6.6 Linear velocity and flow rate .. ... .. .. .. ... ... . ... ... . .. .. .. .. ... .. .. ... .. .. . .. ... .. .. .. .. ... .. 6-17

6-1
GC-17A Ver.2 SERVICE MANUAL -
 Maintenance parts list
“~.,:.....j, ,,__ I

Table 6.1 Maintenance parts list

GG17AA Ver.2 ASSY GCi7AA Ver.2 ASSY
221-43295-91 GC base unit 17AV2 221-43234-91 AFC 17A V2 Assy 1oov
075-29344-18 CPU, N80 C 188XL- 12 -92 AFC 17A V2 Assy 115v
221-43302-9 1 ROM, GC- 17AV2 -93 AFC 17A V2 Assy 220v
075-30320-5 1 RAM, M5M5256BP-1OOL -94 AFC 17A V2 Assy 240v
07.5-30820-O 1 IC, M6624OP -95 AFC 17A V2 Assy 230V
075-23786-O) IC, AD677JN 221-43228-91 TFCAssy 17AV2
074-73307-01 Lithium battery CR2032 L 22 1- 4322 l-9 1 Solenoid valve Assy TFC

22 l-43 122-9 1 PCB, POWER CONT 17AV2 I- 22 l-43227-9 1 Front panel Assy ICOV
-92 Front panel Assy 115v
is--- 065-68207-03 SSR, S26MDOl
-93 Front panel Assy 220v
072-01665-36 Fuse, 326 015, ISA 1OOV system -94 Front panel Assy 240v
072-01665-34 Fuse, 326 010, 10A 1OOV system -95 Front panel Assy 230V
072-01664-33 Fuse, 313 005, 5A lOOV, 2COV system 22 l-4322 l-92 Solenoid valve Assy ESC
072-01665-33 Fuse, 326 008, 8A 200V system t 22 l-43690-9 1 Small solenoid valve Assy 1OOV
072-01664-30 Fuse 3A 200V system
-92 Small solenoid valve Assy 115V
074-80662-o 1 SW power supply 5V, ?c 15 1OOV system -93 Small solenoid valve Assy 220V
074-80667-01 SW power supply 5V. t 15 200V system -94 Small solenoid valve Assy 240V
-95 Small solenoid valve Assy 230V
074-80654-3 1 SW power supply 24V 1OOV system
374-80666-01 SW power supply 24V 250V system 221-43096-91 PCB, FLOW CONT 17A V2

221-39544-91 KEY DISPLAY Assy 221-43707-g 1 Filter Assy SPL

L- 221-41018-91 LCD Assy 22 l-43708-9 1 Filter Assy PURGE

-
22 l-43838-9 1 APC- 17 V2 (Japanese version)
22 l-4306 l-9 1 Fan motor kssy 1oov
-92 Fan motor Assy 115v -92 ‘, (English version)
I -93 Fan motor Assy 220124Ov L- 22 l-44020-92 APC Assy
L 221-43342-91 Motor main unit Assy 1oov 221-43597 Radiation fin cover
-92 Motor main unit Assy 115v
221-43599 DET. INJ upper cover
-93 Motor main unit Assy 220v --_I_____
22 l-43652-9 1 Column oven heater Assy 1oov
22 l-43059-9 1 Flap motor Assy -92 Column oven heater Assy 115v
-93 Column oven heater Assy 220v
22 l-43053-9 1 Power switch Assy
-94 Column oven heater Assy 240v
-95 Column oven heater Assy 230V
22 i-43345-9 1 AUX temperature control unit
L- 221-43325-91 PCB Assy AUX TEMP CONT 221-43695-g 1 Temperature censor (for column)

22 l-43696-9 1 Thermocouple (for column)

670- 18558- 11 Pressure gauge 200 kPa

221-18150-93 Bellows valve 200 kPa

670-18558-12 Pressuregauge300kPa

221-41463-91 Bellows valve for capillary

6-2
- GC-l-/A Ver.2 SERVICE MANUAL
 6.1 Maintenance parts list

INJ unit TCD-17 V2

22 I-32126-05 Graphite ferrule 0.5 221-41900-91 TCD unit Assy 100/115v
22 l-32 126-08 Graphite ferrule 0.8 -93 TCD unit Assy 220/24Ov
201-35584 Septum INJ, 20 pieces contained
22 l-42594-9 1 PCB, TCD- 17 Assy
201-35507-01 Septum heat insulation
22 I- 15563-g 1 Graphite ferrule, 4 pieces contained FPD-17 V2
201-47616 Silica wool, 2g contained 22 1-00892-O 1 Filter (S)
221-42939-91 SPL-17 V2 100/115V 221-00897-01 Filter(P)

L -93 SPL- 17 v2 22oi24Ov

22 I-43025-9 1 Heater, PT, CA INJ 17A V2 lOO/ 115V
221-27398-91 Filter (Sn)

22 l-42968-9 1 FPD- 17 V2 unit 1001115v

-93 Heater, PT, CA INJ 17A V2 220/24OV
-93 FPD- 17 V2 unit 220124Ov
221-41444 SPL- 17 Glass insert split
221-41544 SPL- 17 Glass insert splitless 221-41772-91 Nozzle base Assy FPD-17
L 221-41785 Quartz tube, nozzle base
221-43861-91 WBI-17V2 LOO/l 15v

L -93 WBI-17V2 22Ol24OV

- 221-43026-91 Heater,PT,CAINJ 17AV2 1001115V
-93 Heater, PT, CA INJ 17A V2 220/24OV
221-00887-01 Quartz plate Assy
670- 14404 Photo-multiplier, R268
221-43346-91 Base unit heater,PT, CA Assy 100/l 15V
221-41599 WBI- 17 Glass insert -93 Base unit heater,PT, CA Assy 220124OV
221-41484 Glass insert, packed column ~. 22 I-42 168-9 1 Head unit heater,PI, CA Assy 100/l 15V
221-42976-91 INJ, OCI-17 V2 -93 Head unit heater,PT, CA Assy220124OV
221-42222-91 Adapter for on-column
221-02467 Quartz pipe
t 22 l-42359 Spacer, OCI
--
221-39959-91 PCB, linear amplifier FPD Assy
22 l-43779-9 1 Cooling fan v2, IOOV
-92 Cooling fan 115v 22 l-43325-9 1 PCB Assy AUX TEIvIP
-93 Cooling fan 22ot24Ov
221-43309-91 Small solenoid valve IOOV
221-44073-91 Step-downtransformer
AssyOCI-17V2 200Vsystem
only -92 Small solenoid valve 115V
22 l-42223 Glass insert for PTV -93 Small solenoid valve 220V
WFID-17/FIDl7 V2 -94 Small solenoid valve 240V
--
221-42951-91 FID-17 unit V2 100/l 15v 221-!8150-91 Bellows valve 2k
-93 FID- I7 unit V2 22Ol24OV
670-i 8558- 11 Pressure gauge 200 kPa
22 l-39692-92 Nozzle base unit Assy FID- 17
22 I-37304-03 Nozzle Assy ECD-17 V2
k
221-42940-91 IIigh-pressure unit Assy FID-17 V2 221-42960-91 ECD-17 V2 without cell 1001115V
22 I-39695-9 1 Collector Assy FID- 17
221-41327-91
E 22 I-43346-9 1
Igniter Assy
Heater,PT, CA Assy DET loo/l 15v
L -93 ECD- 17 V2 without cell 220/2&W
22 l-43346-9 1 Heater, PT, CA DETV2
-93 Heater, PI’, CA DETV2
100/l 15v
220/2&W
-93 Heater,PT, CA Assy DET 220124OV
22 l-4327 l-9 1 PCB, FID wide control portion 17AV2 221-39614-91 PCB, ECD Assyl7

22 l-43268-91 PCB, FID linear control portion FTD-17 V2

221-43309-91 Small solenoid valve 1OOV
221-41849-91 PCB, power controller FTD-17
-92 Small solenoid valve 115V
-93 Small solenoid valve 220V 221-41722-91 Electrode unit FI’D-17
-94 Small solenoid valve 240V L 221-1870491 FID collector Assy

221-18150-91 Bellows valve 2k, Hz

22 l-415 1l-9 1 Bellows valve 2k, with resistancecontained, Air
670-l 8558- 11 Pressure gauge 200 kPa
 6.2.1 Complete initialization of the parameter (RAM)
A normal parameter is initialized as follows.

[FTq [--q [-F-J [E] [ENTE]

In this operation, the following parameters concerning basic envi-

ronmental setting of the GC are not initialized.
Setting of the installed unit (FUNCTION 14)
Setting the transmission (FUNCTION 15)
Changing the name on the screen (FUNCTION 17)
Customize (FUNCTION 18)
However, when the ROM (or the GC base unit) is replaced com-
plete initialization should be performed with the following opera-
tion.

In this operation, other than the above parameter,

c FUNC 14 (INSTALL setting)
c FUN@ 15 (OPT LINK setting)
C Column open temperature offset
C Zero point compensation value of AFC and APC, related
parameter
are also initialized. Especially, do not fail to perform resetting or
zero point compensation on the unit with the built-in AFC and
APC. Also, be sure to reset the ADJUST values of the AFC and the
APC.
Replace the values for resetting before key operation. For how to
confiu-m the values, refer to the article that follows.

6.2.2 Mode selection By pressing the (Eg key ten times, a different mode from the
normal one is selected. Pressing the [SC] key returns the mode
to normal.
1. Monitor function
The following functions are available with the (m] , and
m or @ key.
0 The monitor value for each temperature block is displayed to
the first decimal place. [In this case, the decimal point itself
is not displayed.)
@ The monitor displays the pressure values for FLOW 1, 2,
and 3 and the flow rate value to the first decimal place.
@ AFC and the room temperature are displayed.

6-4
- GC-17A Ver.2 SERVICE MANUAL
 6.2 Special key operations

In this case also, the decimal point itself is omitted.

The AFC indicates “-50” as temperature censor is not
mounted in practice. (-5.O”C = means that the temperature
censor is disconnected.)
The room temperature (ROOM) is the temperature of the GC
base unit and it is 5 “C = higher than the actual room temper-
ature.
0 DEMAND display
The heater power to each temperature zone and supply
power to the AFC and APC are displayed in percentage with
their maximum values being 100%.

2. Confirmation and setting of the AFC and APC related parameters.

0 CONTROL
CONTROL values of the AFC and the APC can be checked
with the LjL) and @ keys.
The initial value and its meaning of each parameter are as x
follows. 5
s
Be sure to initialize the CONTROL value. n
2

6-5
GC-17A Ver.2 SERVICE MANUAL B
 6.2 Special key operations

Table 6.2.2-i CONTROL initial values

CONTROL No. Initial values Contents CONTROL No. Initial values Contents
1 10 FLOW 1 (BP) Time constant 26 IO FLOW 4 (F) Proportionalconstan
2 10 FLOW I (BP) Proportionalconstant 27 20 FLOW 4 (F) Integral constan
3 8 FLOW 1 (BP) Integral constant 28 0 FLOW 4 (F) Differentialconstan
4 0 FLOW 1 (BP) Differentialconstant 29 10 FLOW 4 (P) Time constant
5 1 FLOW 2 (F) Time constant 30 200 FLOW 4 (P) Proportionalconstanl
6 10 FLOW 2 (F) Proportionalconstant 31 5 FLOW 4 (P) Integral constant
7 20 FLOW 2 (F) Integral constant 32 0 FLOW 4 (P) Differentialconstant
8 0 FLOW 2 (F) Differentialconstant
9 10 FLOW 2 (P) Time constant 37 I FLOW 3 (P) Time constant
IO 200 FLOW 2 (P Proportionalconstant 38 20 FLOW 3 (P) Proportionalconstant
11 5 FLOW 2 (F Integral constant 39 5 FLOW 3 (P) Integral constant
12 0 FLOW 2 (P Differentialconstant 40 0 FLOW 3 (P) Differentialconstant

17 1 FLOW 1 (I’) Time constant 45 1 FLOW 5 (P) Time constant

18 20 FLOW 1 (P) Propo~ionalconstant 46 20 FLOW 5 (P) Proportionalconstaix
19 5 FLOW 1 (P) Integral constant 47 5 FLOW 5 (P) Integral constant
20 0 FLOW 1 (P) Differentialconstant 48 0 FLOW 5 (P) Differentialconstant
21 10 FLOW 3 (BP) Time constant
22 10 FLOW 3 (BP) Proportionalconstant 53 1 FLOW 6 (P) Time constant
23 8 FLOW 3 (BP) Integral constant 54 20 FLOW 6 (p) Proportionalconstant
24 0 FLOW 3 (BP) Differentialconstant 55 5 FLOW 6 (P) Integral constant
25 I FLOW 4 (F) Time constant 56 0 FLOW 6 (P) Differentialconstant

@ ADJUST value
The ADJUST values of the AFC and APC can be checked
with the [E], B , and @ keys.
The meaning of each parameter is as follows.

6-6
m GC-17A Ver.2 SERVICE MANUAL
 6.2 Special key operations

Table 6.2.2-2 ADJUST values

DJUST No. 1 Contents

sm (AUX~A) Offset
SPLI (ALJXIB) Offset
SPLl P gain
SPLl F gain
SPLI F input value
FLQWl F mode F gain
FLOW1 Fmode F input value
PLOW2 Pmode P gain
SPL2 (AUX2A) Offset

SPL2 (AUX2B) Offset

SPL2 P gain
SPL2 P gain
SPL2 P input value
FLOW3 F mode F gain
FLOW3 Fmode F input value
FLOW4 Pmode P gain
FLOWS Offset
FLOW6 Offset
FLOW.5 Fmode F gain
FLOW5 Fmode F input value
FLOW5 Pmode P gain
FLOW6 Fmode F gain
PLOW6 Fmode F input value

FLOW6 P mode P gain

6-7
GC-17A Ver.2 SERVICE MANUAL m
 6.3.1 Maintenance precautions
1. Make sure to turn off both the power switch of the GC-l7A
and main power supply to the equipment. (The same applies
to peripheral devices.)
2. Always make sure to close the hydrogen gas valve on the sup-
ply side before working on any equipment which use the gas.
3. Make sure to turn off the main valve on the supply side
before inspecting any flow system and never remove any
joint until the gas pressure completely decreases.
h!L
II\ If the gas flows in the reverse direction due to loosening the
joint before completely lowering the gas pressure, it may
result in a pressure control malfunction caused by dust and
external particles.
(A filter is installed in the primary side of the pressure con-
troller but not in the secondary side.)
4. When connecting a pipe, always hold the pipe in one hand
and manually tighten the joint with your other hand, making
sure it is correctly aligned. Following this, grip two wrench-
es with one hand, squeezing them together until the joint is
fully tightened. (Refer to Fig. 6.3.1- 1)
-\!!L
‘1, While only one wrench can be used to connect a pipe to a
firmly secured joint, it is recommended to use two wrenches
at all times.

Fig. 6.3.1-1 Method of using wrenches

5. Loosening of a joint or screw while they are hot may cause

scorching; therefore, make sure that the temperature is suffi-
ciently low before loosening them.

6-8
- GC-17A Ver.2 SERVICE MANUAL
 6.3 GC general

6. For safety, do not put removed parts or screws on top of or

inside the equipment.
7. Insulators removed for the purpose of parts replacement
must be properly re-installed in their original position. When
the insulator for the column thermostatic oven has been
removed and re-installed, make sure that heat does not
escape from inside the thermostatic oven after the insulator
is re-installed.
8. When working on the temperature sensor or the heater unit
for the purpose of parts replacement, make sure that they are
properly in contact with the heat conductor block by taking
such measures as wrapping aluminum foil (cooking foil)
around them. Always check the resistance and insulation.
9. In the case of fuse replacement, always use parts with the .- ,_.’
specified capacity. j’~;.;&
\I,
7ir Use of improper parts may lead to an accident. ‘.“*r--z
/
10. Always make sure that the connector is adequately inserted. ’ ;x ”
Never loosen or tighten any joint of any section while it is still hot. z
The screw threads may become damaged and unusable due to EL
expansion of the joint section caused by heating. a”
Use a wet towel to quickly cool a desired section.
Squeeze together two wrenches as far as single-hand grip will allow.

6.3.2 Rephcing restrictor and septum

1) Cut off the tip of the septum placed at the injection port.

Cut here

2) Put a relatively thick syringe needle through the plug and

insert the tip of the restrictor (narrow tube) into the syringe
needle.

6-9
GC-17A Ver.2 SERVICE MANUAL I
 6.3 GC general

3) Without removing the tip of restrictor from the syringe needle,

move the septum so as to let the restrictor pass through it.
(This is necessary since small pieces of the septum may other-
wise clog the restrictor.)

4) Put the entire component inside the housing.

N:h%ote2
Fig 6.3.2 Procedure for restrictor replacement

<<Note2+> 1. Be careful not to bend the restrictor when inserting it into the
joint.
2, Make sure to secure the designated length of the joint so that
it does not touch the end of the restrictor.

6.3.3 Inspection of rnoiecular sieve filter

The GC-I 7A V2 Series Gas Chromatograph equipped with an elec-
tronic flow controller is provided with a molecular sieve filter in its
carrier gas flow line.
This filter requires periodic aging.
The molecular sieve filter contains molecular sieve 5A. When the
filter is used for a long period of time in the flow line of the Gas
Chromatograph, the absorption capacity of the sieve gradually
decreases as it accumulates various impurities from the gas being
used. If the filter is continually used in the flow line without cor-
recting its reduced absorption capability, it may lead to a base line
fluctuation.
Therefore, it is necessary to perform heat aging once every 3 to 6
months by following the procedure described below.
0 Remove the molecular sieve filter installed in the carrier gas
flow line of the Gas Chromatograph using two 12-mm
wrenched. (Make sure to cool each thermostatic oven and

6-10
m GC-17A Ver.2 SERVICE MANUAL
 6.3 GC general

stop the gas flow before removing the molecular sieve filter.)
@ Short-circuit the joints where the molecular sieve filter was
installed.
@ Remove the column from the column oven.
@ Install the molecular sieve filter to the INJ outlet using a
wrench, and firmly tighten it to prevent leakage.
@ Allow the carrier gas to flow at 40-50 ml/min. (N2 or He gas
can also be used.)
@ Heat the column oven to 34OC and maintain the tempera-
ture for more than 5 hours. (This procedure is called aging.)

<<Note>> Make sure that the carrier gas is flowing through the molecular fil-
ter during heat aging.

@ After completing the aging, cool the column oven to approx-

imately room temperature and stop the carrier gas flow
before removing the molecular sieve filter and re-installing it
into the original flow line. .-x
z
<<Note>> Never install or remove the joints to or from a heated section such b
as the molecular sieve filter and column until they have sufficiently 2

cooled. If joints are connected or disconnected while they are hot,

threads may become damaged due to the expansion of the joints. In
case work has to be performed as soon as possible, apply a wet
cloth to cool the joints sufficiently.,

6.3.4 Inspection of compressor and silica gel

The air compressor tank, which supplies air to the FID, tends to
accumulate dew condensation inside. Since the results of an FID
analysis are likely to be affected if this dew condensation is acci-
dentally supplied to the FID, make sure that the air fed to the
equipment is completely dry by placing a silica gel container
between the FID and the compressor for moisture removal. Silica
gel is blue when dry but turns red as it absorbs moisture. Red silica
gel should be replaced with fresh, blue silica gel. (Red silica gel
can be dried and reused by heating it in an oven.) Also be sure to
open the drain plug of the air compressor to remove water that has
accumulated in the tank at the end of the day.

6-11
GC-17A Ver.2 SERVICE MANUAL m
 6.3 GC general

6.3.5 Injection port septum

Since leakage may occur if the injection port septum is used over 20
or 30 times, be sure to replace it whenever necessary. Also note that
leakage may occur much sooner (i.e., after only several times of use)
when a syringe needle thither than a regular micro-syringe is used.
Please note that any damaged or bent syringe needle tip can severe-
ly damage the septum.
It is recommended to use a proper septum in accordance with the
temperature of the injection port.
Low-bleed septum (green) * * * * injection port temperature
of above 300 “C(heat-resist-
ing septum)
Silicon septum (cream) * * * * * injection port temperature
of below 300 “C

Change the septum by following the procedure described below.

(1) Press the [S] and [E] keys if the equipment is

in operating mode. The temperature control operation stops
after the indicated STOP TIME passes, and the carrier gas
stops when the indicated FLOW OFF TIME elapses from the
moment the temperature control stopped.

<<Note>> If the carrier gas is stopped while the column oven is still hot, it can
damage the column. Pay special attention when setting the FLOW
OFF TIME.
When the FLOW OFF TIME is set at 9999 (initial setting), press
the [%mJ (E] and [w] keys to stop the carri-
er gas after the temperature of the column oven lowers below 50 “C

(2) Make sure that the temperature of the injection port has suf-
ficiently lowered (below 100 “C ) before removing the sep-
tum securing nut by fingers as shown in Fig, 6.3.5-l.
After removing the nut, take out the needle guide and sep-
tum. (Do not turn the septum securing nut while it is hot, as
this can cause scorching.)
(3) Insert a new septum.
(4) Attach the needle guide and secure it with the nut. Turn the
nut all the way with fingers.

6-12
m GC-17A Ver.2 SERVICE MANUAL
 6.3 GC general

Septum securing nut

Needle guide

Septum

Fig. 6.3.6-l

The septum is made of silicon rubber. When it is heated above --

12OoC???, melted plasticizer eludes from the septum and can cause j’
ghost peaks in the analysis. The GC-17A V2 is therefore provided _ ,;,g
,* .; !
:”
with a septum purge gas flow passage to apply carrier gas purge _
constantly to the septum surface inside the injection port. (In case x
5
of the AK, the standard setting is 3 ml/min at 100 kPa.) 5
However, if the flow rate of the septum purge gas is too low, peak E
Q
tailing and ghost peaks increase. If the septum purge gas flow rate
must be maintained at a low level, the septum should be aged at.
high temperature prior to use in order to minimize ghost peaks
resulting from the injection port septum.
The method of aging the injection port septum is as follows.
Method of aging the injection port septum
@ Wrap the septum with aluminum foil (cooking foil) as shown
in Fig. 6.3.5-2.
Injectian port septum
/ (P/N 201-35584: package of 40 pieces)

Aluminum foil

Fig. 6.3.5-2 Method of aging the injection

port rubber plug

@ Place the plugs wrapped in aluminum foil inside the thermo-

static oven of the Gas Chromatograph.
@ Adjust the Gas Chromatograph to the following setting.

6-13
GC-17A Ver.2 SERVICE MANUAL II
 6.3 GC general

INJ, DET 300“C

COL INIT TEMP 50 “C
COL INIT TIME 5 min
COL PROG RATE 10 “C/min
COL FINAL TEMP 250°C
COL FINAL TIME 30 min

---I 30min I+-

250°C

START

Turn the heater ON. When the READY lamp lights up, the
column oven starts increasing its inside temperature.
After the temperature has reached the specified setting, turn
OFF the power of the Gas Chromatograph. Then, when the
column oven has cooled down to room temperature, remove
the septums wrapped in the aluminum foil. (It will take about
1 hour for the oven to sufficiently cool down.)
Place the aged injection port septums in a clean bottle and
seal it tight for storage.

<<Note>> Be sure to lower the column inlet pressure before removing the
septum. if the septum is removed when the column inlet pressure is
still high, a sudden drop in pressure may cause silica wool to squirt
or oxygen to enter the column and cause oxidation.

6-14
m GC-l-/A Ver.2 SERVICE MANUAL
Relationship between temperature and temperature sensor resistance

i-----l
'C 1 Ohm 1 Ohm/‘; “C Ohm Ohm /“C ‘C Ohm Ohm /“C
120 51.32 80 131.42 280 206.66
0.415 0.388 0.364
110 55.47 90 135.30 290 210.30
0.412 0.386 0.363
-100 59.59 + 100 139.16 + 300 213.93
0.411 0.385 0.361
90 63.70 110 143.01 310 217.54
0.409 0.384 0.361
80 67.79 120 146.85 320 221.15
0.408 0.382 0.359
70 71.87 130 150.67 330 224.74
0.406 0.382 0.358
60 75.93 140 154.49 340 228.32
0.404 0.380 0.357
50 79.97 150 158.29 350 231.89
0.403 0.379 0.356
40 84.00 160 162.08 360 235.45
0.402 0.378 0.354
30 88.02 170 165.86 370 238.99
0.401 0.377 0.354
20 92.03 180 169.63 380 242.53
0.399 0.375 0.352
10 96.02 190 173.38 390 246.05
0.398 0.375 0.35 1
i0 100.00 + 200 177.13 +400 249.56
0.397 0.373 0.350
10 103.97 210 180.86 410 253.06
0.396 0.372 0.349
20 107.93 220 184.58 420
0.395 0.371
30 111.88 230 188.29 430
0.393 0.370
40 115.81 240 191.99 440
0.392 0.368
50 119.73 250 195.67 450
0.391 0.368
60 123.64 260 199.35 460
0.390 0.366
70 127.54 270 203.03
0.388 0.365
___--

6-15
GC-17A Ver.2 SERVICE MANUAL m
 .I I CA Thermocouple

CA Thermocouple electromotive force

“C 0 1 2 3 4 5 6 7 8 9 10 “C
1
t millivolts
- - 1
(+)o 0.00 0.04 0.08 0.12 0.16 0.20 0.24 0.28 0.32 0.36 0.40 (-t)C
10 0.40 0.44 0.48 0.52 0.56 0.60 0.64 0.68 0.72 0.76 0.80 10
20 0.80 0.84 0.88 0.92 0.96 1.oo I .04 1.08 1.12 1.16 I .20 20
30 1.20 1.24 1.28 1.32 1.36 1.40 1.44 1.49 1.53 1.57 1.61 30

40 1.61 1.65 1.69 1.73 1.77 1.81 1.85 1 .vo 1 .v4 1.98 2.02 40
50 2.02 2.06 2.10 2.14 2.17 2.23 2.27 2.3 1 2.35 2.39 2.43 50
60 2.43 2.47 2.5 1 2.56 2.60 2.64 2.68 2.72 2.76 2.80 2.85 60

70 2.85 2.89 2.93 2.97 3.01 3.05 3.10 3.14 3.18 3.22 3.26 70
80 3.26 3.30 2.35 3.39 3.43 3.47 3.5 1 3.56 3.60 3.64 3.68 80
90 3.68 3.72 3.76 3.81 3.85 3.89 3.93 3.97 4.01 4.06 4.10 90
--
100 4.10 4.14 4.18 4.22 4.26 4.3 1 4.39 4.43 4.47 4.5 1 100

110 4.5 1 4.55 4.60 4.64 4.68 4.72 4.76 4.80 4.84 4.88 4.92 110
120 4.92 4.96 5.01 5.05 5.09 5.13 5.17 5.21 5.25 5.29 5.33 120
130 5.33 5.37 5.41 5.45 5.49 5.53 5.57 5.61 5.65 5.69 5.73 130

140 5.73 5.77 5.81 5.85 5.89 5.93 5.97 6.01 6.05 6.09 6.13 140
1.50 6.13 6.17 6.2 1 6.25 6.29 6.33 6.37 6.41 6.45 6.49 6.53 150
160 6.53 6.57 6.61 6.65 6.69 6.73 6.77 6.81 6.85 6.89 6.93 160
.-x
170 6.93 6.97 7.01 7.05 7.09 7.13 7.17 7.21 7.25 7.29 7.33 170
z 180 7.33 7.37 7.41 7.45 7.49 7.53 7.57 7.61 7.65 7.69 7.73 180
x 190 7.73 7.77 7.81 7.85 7.89 7.93 7.97 8.01 8.05 8.09 8.13 190
--
a” 8.50 8.54
200 8.13 8.17 8.21 8.25 8.29 8.33 8.37 8.41 8.46 200
--
210 8.54 8.58 8.62 8.66 8.70 8.74 8.78 8.82 8.86 8.90 8.94 210
220 8.94 8.98 9.02 9.06 9.10 9.14 9.18 9.22 9.26 9.30 9.34 220
230 9.34 9.38 9.42 9.46 9.50 9.54 9.59 9.63 9.67 9.7 1 9.75 230

240 9.75 9.79 9.83 9.87 9.9 i 9.95 9.99 10.03 10.07 10.11 10.16 240
250 10.16 10.20 10.24 10.28 i0.32 10.36 10.40 10.44 10.48 10.52 10.57 250
260 10.57 10.61 10.65 10.69 10.73 10.77 10.81 10.85 10.89 10.93 10.98 260

270 10.98 11.02 11.06 11.10 11.14 11.18 11.22 il.26 11.30 11.34 Il.39 270
280 11.39 11.43 11.47 11.51 11.55 li.59 11.63 11.67 11.72 11.76 11.80 280
290 11.80 11.84 11.88 il.92 11.96 12.01 12.05 12.09 12.13 12.17 i2.21 290
-- --
300 12.21 12.25 12.29 12.34 12.38 12.42 12.46 12.50 12.54 12.58 12.63 3oa

310 12.63 12.67 12.71 12.75 12.79 12.83 12.88 12.92 12.96 13.00 13.04 310
320 13.04 13.08 13.12 13.17 13.21 13.25 13.29 13.33 13.37 13.42 13.46 320
330 13.46 13.50 13.54 13.58 13.62 13.67 13.71 13.75 13.79 13.83 13.88 330

340 13.88 13.92 13.96 14.00 14.04 14.09 14.13 14.17 14.21 14.25 14.29 340
350 14.29 14.34 14.38 14.42 14.46 14.50 14.55 14.59 14.63 14.67 14.71 350
360 14.71 14.76 14.80 14.84 14.88 14.92 14.97 15.01 15.05 15.09 15.13 360

370 15.13 15.18 15.22 15.26 15.30 15.34 15.39 15.43 15.47 15.51 15.55 370
380 15.55 15.60 15.64 15.68 15.72 15.76 15.81 15.85 15.89 15.93 15.98 380
390 15.98 16.02 16.06 16.10 16.14 16.19 16.23 16.27 16.31 16.36 16.40 390

400 16.40 16.44 16.48 16.52 16.57 16.61 16.65 16.69 16.74 16.78 16.82 400

410 16.82 16.86 16.91 16.95 16.99 17.03 17.07 17.12 17.16 17.20 17.24 410
420 17.24 17.29 17.33 17.37 17.41 17.46 17.50 17.54 17.58 17.62 17.67 420
430 17.67 17.71 17.75 17.79 17.84 17.88 17.92 17.96 18.01 18.05 18.09 430

“C 0 1 2 3 4 5 6 7 8 9 10 ‘C

6-16
- GC-17A Ver.2 SERVICE MANUAL
 : :.-;. I ~
: 6. i ‘6. ” Linear velocity and flow rate

Linear velocity and flow rate

The linear velocity indicates the distance (cm) that carrier gas trav-
els in the column in 1 second. The linear velocity indicated for the
GC-I 7A V2 is an average linear velocity speed in the column.
The average linear velocity can be obtained from the retention time
of methane in the following equation.

Average linear velocity V (cm/s) = Ltl<&\ ‘fs$i’

Where:

tx : Retention time of methane (min)

L : Length of column (m)

The column flow rate for the GC-17A V2 indicates the value that
has been converted to the under ambient temperature and atmo-
spheric pressure. It is equivalent to the value measured by a flow
meter connected the column outlet under ambient temperature.

Column flow rate (ml/min)

Carrier gas: Helium (20 ‘C )
(Column flow rate and the column length:
inverse proportion.)

i.D.=0.22mm

P
100Column inlet pressure
VW

If column inlet pressure is to be set, refer to the graph below.

x (PfPo)Z---PO2 x 103
Fc= rp$z PO

Where: Fc : Column flow rate [mlhninl

cl : Inside diameter of column hml
L : Length of column [ml
P : Column inlet pressure [kPal
PO : Column outlet pressure= atmospheric pressure [kPal
P : Coefficient of viscosity (19.4 ,0 Pa * s (helium, 20 “C) )

6-17
GC-17A Ver.2 SERVICE MANUAL I
 6.6 Linear velocity and flow rate

<=Sleference>> Method of obtaining the carrier gas flow rate (Fc) in the column
from the retention time (to) of methane.

r2L
Fc= rtoJ Unit of FC 1 ml/min

Therefore:

J+ (Pressure gradient correction factor)

p,pi Pi : Inlet pressure(absolutepressure),gauge pressure+ 1

PO PO: Outlet pressure (absolute pressure), normally 1

Y : Inside radius of column (cm)

L : Length of column (cm)
to 1 Retention time of methane (min)

Comparison of calculated results and actual measurements

CBPl - M25 - 025

.-X Inside diameter: 0.22 mm, length: 25 m

z
zi
4

4-18
- GC-77A Ver.2 SERVICE MANUAL
CB
3 Kanda-Nlshtktcho
SHIMADZU

SHIMAOZU COAPOAATIOW.International Marketinn Division

1-chome Chlyoda-ku
CORPORATION

Tokyo 101. Japan

SHIMADZU [ASIA PACIFICI PTE LTD.
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Phone 1(410)381-1227 Fax 1[410)381-1222 Toll Free 1 (800)477-1227 Phone 61(2)748-3233 Fax.61(2)748-3172
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