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Problem Set # 2

This document contains multiple problems related to distillation column design and operation. It includes calculations for determining distillate and bottoms compositions and flow rates, number of theoretical plates, and tower diameter for columns performing benzene-toluene separation, heptane-octane stripping, ethanol-water stripping with steam injection, and hydrocarbon distillation with sieve trays. Parameters such as reflux ratio, vapor to feed ratio, steam injection rate, Murphree efficiency, tray spacing, and fraction of flooding are provided.

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Dharyl Flores
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1K views

Problem Set # 2

This document contains multiple problems related to distillation column design and operation. It includes calculations for determining distillate and bottoms compositions and flow rates, number of theoretical plates, and tower diameter for columns performing benzene-toluene separation, heptane-octane stripping, ethanol-water stripping with steam injection, and hydrocarbon distillation with sieve trays. Parameters such as reflux ratio, vapor to feed ratio, steam injection rate, Murphree efficiency, tray spacing, and fraction of flooding are provided.

Uploaded by

Dharyl Flores
Copyright
© © All Rights Reserved
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
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11.4-7 Enriching Tower for BenzeneToluene.

An enriching tower is fed 100 kg mol/h of a saturated vapor


feed containing 40 mol % benzene (A) and 60 mol % toluene (B) at 101.32 kPa abs. The distillate is to contain
90 mol % benzene. The reflux ratio is set at 4.0:1. Calculate the kg mol/h distillate D and bottoms W and their
compositions. Also, calculate the number of theoretical plates required.
11.4-8 Stripping Tower. A liquid mixture containing 10 mol % n-heptane and 90 mol % n-octane is fed at its
boiling point to the top of a stripping tower at 101.32 kPa abs. The bottoms are to contain 98 mol % n-octane.
For every 3 mol of feed, 2 mol of vapor is withdrawn as product. Calculate the composition of the vapor and
the number of theoretical plates required. The equilibrium data below are given as mole fraction n-heptane.
11.4-9 Stripping Tower and Direct Steam Injection. A liquid feed at the boiling point contains 3.3 mol %
ethanol and 96.7 mol % water and enters the top tray of a stripping tower. Saturated steam is injected directly
into liquid in the bottom of the tower. The overhead vapor which is withdrawn contains 99% of the alcohol in
the feed. Assume equimolar overflow for this problem. Equilibrium data for mole fraction of alcohol are as
follows at 101.32 kPa abs pressure (1 atm abs).

(a) For an infinite number of theoretical steps, calculate the minimum moles of steam needed per mole of
feed. (Note: Be sure and plot the q line.)
(b) Using twice the minimum moles of steam, calculate the number of theoretical steps needed, the
composition of the overhead vapor, and the bottoms composition.
11.5-1 Murphree Efficiency and Actual Number of Trays. For the distillation of heptane and ethyl benzene
in Problem 11.4-2, the Murphree tray efficiency is estimated as 0.55. Determine the actual number of trays
needed by stepping off the trays using the tray efficiency of 0.55. Also, calculate the overall tray efficiency
Eo .
11.5-3 Estimation of Tower Diameter of Sieve Tray. A distillation sieve-tray tower is being used to distill a
hydrocarbon feed. The vapor flow rate at the tower bottom is 21 000 kg/hr and the liquid flow rate is 19 500
kg/hr. The density of the liquid = 673 kg/m3 and = 3.68 kg/m3. Assume a tray spacing of 24 in. (0.610
m). Calculate the tower diameter assuming the tower operates at 80 % of flooding. Assume = 22.5 dyn/cm.

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